Oakton pH5 Operating Manual

Operating Manual
pHTestr 5 Pocket Testers
®
Model pH5 — Glass bulb probe for general liquid testing
Model pH5F — Flat probe for surface or micro-volume testing
Model pH5S — Spear-tip probe for testing semisolid and
solid materials
Thank you for purchasing an Oakton pHTestr
®
Please carefully read this operating manual before using the product
to obtain an accurate and reliable test result and avoid unnecessary
damage to the tester or
sensor/probe.
Features
• Large easy-to-read LCD with • Stability and battery status
3-color backlight icons
• Accuracy of ±0.01 pH ± 1 digit • Replaceable single-junction
sensor saves you money
• 1, 2, or 3 calibration points
• Auto power-off function
• Auto buffer recognition:
conserves battery life
US or NIST
• IP67 waterproof rating
Keypad Functions
Short press = <2 seconds Long press = >2 seconds
1. Short press to turn on the tester and long press to turn
off the tester.
MEAS 2. When turned off, long press to enter parameter setting mode.
3. In measurement mode, short press to turn on backlight.
1. In measurement mode, short press to switch parameter from
pH to ORP (Oxidation Reduction Potential); ORP probe sold
MODE
separately.
2. In parameter setting mode, short press to change parameter
(unidirectional).
1. Long press to enter calibration mode.
CAL
2. In calibration mode, short press to confirm calibration.
3. When measured value is locked (HOLD icon), short press to
<
unlock.
Preparation Before Use
Models pH5 and pH5F: If it is first-time use or the tester hasn't been
used for a long time, pour some 3M KCL solution to the Fill line in
the probe cap and soak the probe for about 15 to 30 minutes. Users
can store the probe in the 3M KCL solution in the probe cap when
1
pH Measurement
1. Short press /MEAS key to turn on the tester. Rinse the probe in
distilled water, and gently dab off excess water with tissue paper
(do not rub or wipe the glass sensor).
2. Dip the probe in sample solution, stir gently, and allow it to stand
until a stable reading is reached. Take readings after stability indi-
cator icon () appears and stays on the screen.
Notes
A. Applications of each model:
Model/Probe Application
Regular water solutions' pH measurement such as
pH5/Bulb probe hydroponics, aquaculture, pools and spas, water
treatment, brewing, etc.
Flat surface measurement such as skin, paper, fabric,
pH5F/Flat probe leather and so on; micro sample testing;
also works well for regular water solution.
Cheese, sushi rice, meat, fruit, bread, soil, solid
pH5S/Spear-tip
culture medium and semisolid medium measurement;
probe
also works well for regular water solution.
B. Model pH5F Flat probe tester is mostly for flat surface sample
testing.
• For skin test: skin should be without sweat or dirt, nor be overly
cleaned (do not use facewash products before testing) to avoid
affecting measurement results. Dampen skin with some distilled
water, slightly force flat probe onto the skin, get readings after
value stabilized.
• For paper, fabric and leather test: add 1 to 2 drops of distilled water
on surface, then perform measurements.
• For micro sample testing, use a container with an inner diameter
≤19 mm and a flat bottom. The tester can test volume ≥0.5 mL.
C. Model pH5S Spear-tip probe tester is widely used for solids
containing water or semisolid medium. When conducting such tests,
pay attention to insert probe evenly and be careful to prevent probe
from damage. If the medium is too hard (such as meat or fruits),
please bore a small hole with a knife before inserting the probe.
For pH measurement of any food (such as meat, cheese, sushi, etc.),
it should be a sampling test. That means test samples should no
longer be edible.
Special Notes
• The pH probe must be rinsed thoroughly after each use. Soap water
should be used to clean off any grease or other contaminants.
• These pH testers will NOT give accurate or stable pH readings
when testing distilled or deionized water. This is because distilled
or deionized water do not have enough ions present for the elec-
trode to function properly. To measure distilled or deionized water's
pH, users need to use a specialized instrument technique. When
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the tester is not in use to maintain the sensor's accuracy. To achieve
maximum accuracy, we recommend soaking the probe in the 3M
KCL storage solution overnight (12 hours) to activate the glass
membrane thoroughly.
Storing the pH5 and pH5F testers dry will NOT cause any permanent
damage. It will only temporarily cause the probe to lose its sensitivity,
which can always be restored by soaking in the storage solution.
Model pH5S: Never store the spear probe in a dry condition because
permanent damage can be caused. The spear probe should always
be stored in the 3M KCL soaking solution (potassium chloride).
One 10-mL bottle of storage solution comes with the tester kit. If the
soaking solution was contaminated, please replace immediately.
pH Calibration
Pocket pH Tester.
®
1. Short press
2. Rinse the probe in distilled water and use tissue paper
to gently dab off excess water.
3. Pour certain amount (about half volume of the calibration bottles)
of pH 7.00 pH and pH 4.00 buffer solutions in the corresponding
calibration bottles.
4. Long press CAL/ key to enter calibration
mode, short press
measurement mode.
5. Dip the probe in pH 7.00 buffer solution,
stir gently, and allow it to stand still in the
buffer solution until a stable reading is
reached. When measurement stability icon
() appears and remains on the screen
(see Fig 1); then short press CAL/ key to
complete the one-point calibration. The
tester returns to measurement mode and
indication icon "M" will appear at the
bottom left of the screen, indicating the
middle point of calibration has been completed.
6. For 2-point calibration, start with pH 7.00 buffer solution; once
confirmed then rinse the probe in distilled water and dry it with
tissue paper. Dip the probe into pH 4.00 buffer solution, follow the
steps above to complete 2-point calibration. Indication icons "L"
and "M" will appear on the bottom left of the screen.
7. If necessary to perform a 3-point calibration, rinse probe with
water, dip the probe into pH 10.01 buffer solution (sold sepa-
rately), and follow the steps above. Indication icons "L", "M",
and "H" will appear on the bottom left of the screen.
Notes
A. Tester can perform 1 to 3 points automatic calibration. Please note
that pH 7.00 (USA Standard) or pH 6.86 buffer solution (NIST Stan-
dard) must be used to conduct 1st point calibration. Then use other
testing purified water like spring water or drinking water, it will take
longer for the readings to get stabilized (typically 3 to 5 minutes)
because there are very few ions left to be detected by the sensor in
those purified water.
• Do NOT store probe in distilled or deionized purified water because
that will cause permanent damage to the pH probe. Purified water
is only recommended for rinsing the probe. The probe should be
stored in 3M KCL pH electrode storage solution (SKU 00653-04) for
best accuracy.
Setting the Parameters
When tester is turned off, long press
ter setting. Short press MODE/ key to switch from P1 to P2...P7.
Short press CAL/ key and parameter will flash, then short press
MODE/ key to choose desired parameter. Short press CAL/ key
to confirm parameter selection. Long press
to measurement mode.
Symbol
P1
P2 Set low measurement alarm
P3 Set high measurement alarm
P4 Select Automatic Lock (HOLD)
P5
P6
P7
Notes
A. Select standard pH buffer solution (P1)
There are two options of standard buffer solutions: USA series and
NIST series.
B. High and Low Measurement Heads-Up Examples (P1 and P2)
Alert when measured value ≤3.20 pH: Preset lowest value (P2) =
3.20 pH, highest value (P3) = 14.00 pH, when measured value is
≤3.20 pH (stability icon () displays on LCD), the red backlight
appears on display.
Alert when measured value ≥8.60 pH: Preset highest value (P3)
= 8.60 pH, lowest value (P2) = 0.00 pH, when measured value is
≥8.60 pH (stability icon () displays on LCD), the red backlight
appears on display.
Alert when measured value ≤3.20 pH or ≥8.60 pH: Preset lowest
value (P2) = 3.20 pH, highest value (P3) = 8.60 pH, when mea-
sured value is lower than 3.20 pH or higher than 8.60 pH (stabil-
ity icon () displays on LCD), the red backlight appears on
display.
C. Automatic Lock (P4)
Select "On" to activate auto lock function. When reading is stable for
more than 10 seconds, the tester will lock the value automatically,
and "HOLD" icon will appear on the bottom left of the screen. Press
CAL/ key to cancel HOLD on reading.
/MEAS key to turn on.
pH
6.6
/MEAS key to return to
☺
Figure 1
☺
2
/MEAS key to enter parame-
/MEAS key to return
Menu setting Selection
Select pH buffer solution USA – NIST
0 to 14.00 pH
0 to 14.00 pH
Off – On
Select backlight Off – 1 – On
Select temperature unit °C – °F
Restore to factory default No – Yes
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buffer solution to conduct 2nd or 3rd point calibration. Tester will
automatically recognize five kinds of pH buffer solutions. For details,
please refer to the following table:
Calibration USA series NIST series
1-point 7.00 pH
7.00 pH,
4.00 pH or 4.01 pH or
1.68 pH
2-point
7.00 pH,
10.01 pH or 9.18 pH or
12.45 pH
7.00 pH,
4.00 or 1.68 pH,
3-point
10.01 or 1.68 pH, 9.18
12.45 pH or 12.45 pH
B. pH 4.00 and pH 7.00 buffer solutions are included in the pH5S test
kit only but pH 10.01 is not. Users can purchase it separately if
needed. The buffer solutions poured into the calibration bottles
are NOT for one-time use. They can be used multiple times as
long as they are not contaminated, and the bottles are covered
when not in use. After that, we recommend replacing the buffer
solutions in the calibration bottles with new ones that are in the
buffer bottles (50 mL) to keep the accuracy of the standard buffer
pH
solutions. Do not pour used buffer solutions back into the buffer
7
bottles in case of contamination.
C. The tester has self-diagnostic functions:
Symbol Self-diagnostic information
Wrong pH buffer solution or
Er 1
the range of calibration
solution exceeds standard.
Press CAL/ key when
Er 2
reading is not stable during
measurement.
*If you find any air bubble in the glass bulb of the pH sensor, simply invert the
probe for a few times to remove it. The existence of an air bubble in the glass
bulb will significantly decrease the accuracy of measurement.
* The 1st point calibration must be 7.00 pH. Perform the 2nd point calibration
(4.00 pH) immediately after the 1st point. Do NOT turn off the meter before
you conduct 2nd point calibration. If the meter is turned off after 1st point
calibration, user will need to restart the calibration process with the 7.00 pH
first and the 4.00 pH following after. Calibrating directly in pH 4.00 after
turning meter off and back on will cause "Er1".
D. Backlight (P5)
Select "Off" to turn off backlight function, "On" to turn on backlight
function, or "1" to have backlight last for 1 minute.
E. Temperature Unit (P6)
Select °C or °F; the factory default is °C.
F. Factory Default Setting (P7)
Select "Yes" to recover instrument calibration to the theoretical
value (pH value in zero potential is 7.00 pH, slope is 100%), parame-
ter setting returns to initial value. This function can be used when
instrument does not work properly in calibration or measurement.
Calibrate and measure again after resetting the unit to factory default
status.
ORP Measurement
ORP stands for Oxidation-Reduction Potential. ORP is a measure of
the cleanliness of the water and its ability to break down contami-
Factory
nants. Note that ORP sensor module 35634-58 must be purchased
default
separately (see Ordering Information).
USA
Once ORP sensor probe is attached to tester, press MODE/ key to
0
enter ORP mode. Rinse the probe in distilled water and dry it. Dip
14.00
the probe in sample solution, stir gently, and allow it to stand still
Off
until a stable reading is reached. Get readings after measurement
stability icon () appears and remains on the screen.
1
°C
No
Indication
Recommended
icons
Accuracy:
6.86 pH M
≥0.1 pH
6.86 pH,
Range:
L M
<7.00 pH
1.68 pH
6.86 pH,
Range:
M H
<7.00 pH
12.45 pH
6.86 pH,
4.01 or Range:
L M H
0 to 14.00 pH
Checking and how to fix
1. Check whether pH buffer
solution is correct (1st point
calibration must be 7.00).
2. Check whether the probe is
damaged.
3. Check if there is any air
bubble in the glass bulb
sensor.
Wait for the measurement
stability icon () to appear and
stay, then press CAL/ key.
3
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