Set The Detector Parameters - Agilent Technologies 1260 Infinity User Manual

Set the Detector Parameters

1 Set peakwidth as close as possible to the width (at half height) of a narrow
Table 23
Peakwidth at half height
< 0.00125 minutes
0.00125 minutes
0.0025 minutes
0.005 minutes
0.01 minutes
0.025 minutes
0.05 minutes
0.1 minutes
0.2 minutes
0.4 minutes
* Values in the User Interface may be rounded.
2 Choose the sample wavelength.
3 Consider to use time-programming to further optimization.
Agilent 1260 Infinity Variable Wavelength Detector User Manual
peak of interest.
Peakwidth Settings
*
• at a longer wavelength than the cut-off wavelength of the mobile phase,
• at a wavelength where the analytes have strong absorptivity if you want
to get the lowest possible detection limit,
• at a wavelength with moderate absorptivity if you work with high
concentrations, and
• preferably where the spectrum is flat for better linearity.
Rise time [10.. 90%]
< 0.031 seconds
0.031 seconds
0.062 seconds
0.125 seconds
0.25 seconds
0.50 seconds
1 second
2 seconds
4 seconds
8 seconds
How to optimize the detector5
Data rate Module
54.96 Hz G1314C
27.48 Hz G1314C
13.74 Hz G1314C
13.74 Hz G1314B / G1314C
13.74 Hz G1314B / G1314C
13.74 Hz G1314B / G1314C
6.87 Hz G1314B / G1314C
3.43 Hz G1314B / G1314C
1.72 Hz G1314B / G1314C
0.86 Hz G1314B / G1314C
91