Related Manuals for Endress+Hauser KRFB
Summary of Contents for Endress+Hauser KRFB
- Page 1 BA02296C/66/EN/01.23 Products Solutions Services 70209490 Operating Instructions Raman flow assembly KRFB, KRFC...
- Page 2 Operating Instructions Raman flow assembly Endress+Hauser...
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Page 3: Table Of Contents
11.1 Micro flow bench ..........21 4.2 Product identification ......... 10 11.2 Micro flow cell ............22 4.3 Scope of delivery..........10 12 Supplementary documentation ..23 Installation ........11 13 Index ........... 24 5.1 Installing the micro flow bench ......11 Endress+Hauser... -
Page 4: About This Document
Table 2. Symbols U.S. export compliance The policy of Endress+Hauser is strict compliance with U.S. export control laws as detailed in the website of the Bureau of Industry and Security at the U.S. Department of Commerce. -
Page 5: Glossary
μin microinches μm micrometer millimeter milliwatt non-contact optic nanometer oct/min octaves per minute process development pounds per square inch WEEE Waste Electrical and Electronic Equipment Table 3. Glossary Endress+Hauser... -
Page 6: Basic Safety Instructions
The safety information in this section is specific to the flow cell that is compatible with the Raman Rxn-10 spectroscopic probe from Endress+Hauser. Refer to the Rxn-10 Raman spectroscopic probe Operating Instructions for additional information related to probe and laser safety. -
Page 7: Workplace Safety
The product is designed to meet all current safety requirements, and has been tested and shipped from the factory in a safe operating condition. The relevant regulations and international standards have been observed. Devices connected to an analyzer must comply with the applicable analyzer safety standards. Endress+Hauser... -
Page 8: Product Description
In most cases aqueous environments are an acceptable approximation; however, extension beyond these spaces is available. If a unique mounting solution is required, the micro flow bench can be configured with OEM-specific hardware to directly integrate into the unique environment. Endress+Hauser... -
Page 9: Micro Flow Cell
Endress+Hauser. Additionally, micro flow cells are configurable with a variety of fluid path thicknesses if the standard 2.5 mm option is not sufficient. -
Page 10: Incoming Product Acceptance And Product Identification
Wavelength • KMAT (product configuration code) Compare the information on the label/tag with the order. 4.2.2 Manufacturer address Endress+Hauser 371 Parkland Plaza Ann Arbor, MI 48103 USA Scope of delivery The scope of delivery comprises: • Raman micro flow bench •... -
Page 11: Installation
Installation Installing the micro flow bench The Endress+Hauser micro flow bench slips onto the Rxn-10 probe and is secured by a torque limiting thumb screw clamp. The thumb screw on the Rxn-10 probe should never be fully removed. When installing or removing optics, ensure the laser and emission shutter are in the closed position. -
Page 12: Inspecting The Micro Flow Cell
OEM-specific ports to enable unique applications. Tubing must be installed by trained and qualified personnel according to standard operating procedures (SOP). Endress+Hauser recommends that all tubing ports be inspected before installing tubing or sealing ferrules. All tubes should be cut square with approved cutting tools and techniques to ensure leak-free connections. When installing tubing and ferrules into the ports, ensure the tubing and ferrules are flush for the best performance. -
Page 13: Installing The Micro Flow Cell
3. Adjust the light shield forward until the plunger contacts and fixes the micro flow cell in place. 4. Confirm the beam dump is open or closed, according to the application requirements. 5. Close the light shield completely. Before collecting data, open the Rxn-10 shutter. Endress+Hauser... -
Page 14: Commissioning
The Raman RunTime software will not allow spectra to be collected without passing internal and probe calibrations. Passing the probe verification step is not required but is highly recommended. Raman Rxn analyzer operating instructions are available by searching the Downloads area of the Endress+Hauser website: https://endress.com/downloads. -
Page 15: Operation
Cleaning the micro flow cell window → Remove all residual moisture from the cell through a clean drying process such as bake-out. Endress+Hauser does not recommend a specific cleaning procedure as application SOPs may necessitate different parameters. Any bake- ... - Page 16 Operating Instructions Raman flow assembly A0053042 Figure 6. Shutter closure closed Endress+Hauser...
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Page 17: Diagnostics And Troubleshooting
Raman flow assembly Operating Instructions Diagnostics and troubleshooting Endress+Hauser Raman flow assemblies provide consistent and reliable long-term and repeated operation. Refer to the Rxn-10 Raman spectroscopic probe Operating Instructions (BA02160C) to troubleshoot issues with the Rxn-10 probe and accessory optics. - Page 18 Re-cut Flow cell tubing ends if necessary. ports are leaking Fittings incorrectly installed Confirm that fittings are for the correct tubing size and are compatible with the flow cell threads. Replace if necessary. Table 5. Diagnostics and troubleshooting Endress+Hauser...
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Page 19: Maintenance
Cleaning the micro flow cell window The optical surfaces of the micro flow cell must be clean before use. If cleaning is required, Endress+Hauser recommends the process below. Clean gloves are recommended whenever handling the micro flow bench and micro flow cell to minimize the transmission of oils or other film-type contamination to the exterior optical window surfaces. -
Page 20: Repair
To ensure swift, safe and professional product returns, please contact your service organization. For additional product return information, refer to the following site and select the applicable market/region: https://www.endress.com/en/instrumentation-services/instrumentation-repair. 10.2 User serviceable parts There are no user serviceable parts for the Raman flow assembly. Endress+Hauser... -
Page 21: Technical Data
Raman Rxn-10 probe Calibration 785 nm Calibration cell with calibration reference standard* method * See Raman flow assembly calibration and verification kit manual for details Verification 785 nm Verification cell with 70 % IPA method Table 7. Micro flow bench specifications Endress+Hauser... -
Page 22: Micro Flow Cell
15 mL/min* maximum volumetric flow rate * Maximum volumetric flow rate to ensure laminar flow specified for micro flow cell with water. Storage –20 °C to 60 °C < 90 % RH non-condensing Sterilization SIP, CIP Table 8. Micro flow cell specifications Endress+Hauser... -
Page 23: Supplementary Documentation
Operating Instructions Supplementary documentation All documentation is available: • On the Endress+Hauser Operations App for smartphone/tablet • In the Downloads area of the Endress+Hauser website: https://endress.com/downloads Part number Document type Document title BA02295C Operating Instructions Raman flow assembly calibration and verification kit... -
Page 24: Index
15, 16 laser power, 21 troubleshooting, 17 length, 21 wetted materials, 21 pressure, 21, 22 probe temperature, 21, 22 calibration, 14, 21 working distance, 21 verification, 14, 21 symbols, 4 Raman RunTime, 14 technical data, 21 repair, 20 Endress+Hauser... - Page 25 Raman flow assembly Operating Instructions www.addresses.endress.com Endress+Hauser...