Automatic Calibration From A Single Standard; Sips 10 - Agilent Technologies SIPS 10 User Manual

Operation
Make sure that you do not let too much air into the diluent tubing when you
NOTE
remove it from the Mariotte vessel. Allow sufficient time for the air to clear
before remeasuring.
4
If the nebulizer blocks, replace the diluent in the Mariotte vessel because
TIP
blocking causes the flow of sample to be reversed, towards the Mariotte vessel,
leading to contamination of the diluent and incorrect results.

Automatic Calibration from a Single Standard

Automatic calibration from a single standard can be performed using
either the single pump system of the SIPS 10 or the dual pump
system of the SIPS 20.

SIPS 10

To calibrate a method using the SIPS 10:
1
2
3
44
Observe the movement of the bubble in the diluent line. If it is
not travelling towards the nebulizer, slowly wind out the
nebulizer thimble until the bubble travels towards the nebulizer.
It should take approximately 25–30 seconds for the bubble to
travel 100 mm in the diluent tubing with the pump running at
100%.
Develop or modify a method (flame analysis) as per your
analytical requirements (refer to the online help for details).
To incorporate SIPS operation into the method, enable the Use
SIPS check box on the Type/Mode page (the first page in the
Edit Methods dialog).
On the SIPS page:
a
Set the Right Pump setting to None.
Agilent Sample Introduction Pump System SIPS 10/20 User's Guide