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Summary of Contents for Gilson CPC 100
- Page 1 User’s Guide Gilson CPC Systems...
- Page 2 Trademarks All product and company names are trademarks™ or registered® trademarks of their respective holders. Use of the trademark(s) in this document does not imply any affiliation with or endorsements by the trademark holder(s).
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Page 3: Table Of Contents
Requirements spacing storage and movement Sécurité symboles electroniques et de Dangers notes de sécurité Risques Chimiques Risques electriques solvants inflammables levage Pièces de Remplacement signes de Détérioration exigences du site espacement stockage et Déplacement Gilson CPC systems | UseR’s GUiDe... - Page 4 Abbreviations Customer service Installation CHAPTER 2 | Plumbing Connections inlet outlet Waste CPC system with PlC Purification system inlets electrical Connections Right side Panel Diagram Rs-232 Remote signals stop out Profinet external Power Power Connection tABle oF Contents Gilson CPC systems...
- Page 5 CHAPTER 4 | Helpful Hints Cleaning and Decontamination exterior Column and Fluid Path maintenance schedule Replace a seal in a Column Rotary seal Troubleshooting CHAPTER 5 | troubleshooting table error messages Repair and Return Policies Gilson CPC systems | UseR’s GUiDe...
- Page 6 Warranty APPENDIX A | General limited Warranty Fittings and tubing Valves Replacement Parts and Accessories APPENDIX B | Materials APPENDIX C | liquid Contact materials tABle oF Contents Gilson CPC systems...
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Page 7: Safety
Failure to comply with these precautions or with warnings described in the user’s guide violates safety standards of design, manufacture, and intended use of the instrument. Gilson assumes no liability for customers failing to comply with these requirements. -
Page 8: Electronic And Hazard Symbols
UV-Strahlung Gefahr radiation UV Caution, Two Person Lift Attention, Levage par deux Vorsicht, Zwei Personen Required personnes requis erforderlich Avertissement, Substances Achtung, Korrosiven Warning, Corrosive Chemical corrosives Chemikalien Caution, Hot Surface Attention, Surface chaude Vorsicht, Heiße Oberfläche saFety GIlSon CPC SyStEmS... -
Page 9: Safety Notices
The instrument exceeds the weight one person can lift safely. Two or more people are required to lift the instrument safely. Always lift the instrument from the base and follow any unpacking instructions provided with the instrument. Gilson CPC systems | USER’S GUIDE... -
Page 10: Replacement Parts
Run a clean solvent through the fluid path before storing the instrument. Do not leave buffer in the system, as it may cause blockages and damage the seals. Rinse the fluid path and prevent the liquids from flowing out by inlets and outlets before moving the instrument. saFety GIlSon CPC SyStEmS... -
Page 11: Sécurité
Gilson décline toute responsabilité en cas d’incapacité du client à se conformer à ces exigences. Veuillez lire toute la documentation et les informations relatives à la sécurité pour les accessoires, périphériques, et autres instruments pouvant être utilisés avec cet instrument avant de faire fonctionner le... -
Page 12: Symboles Electroniques Et De Dangers
UV-Strahlung Gefahr radiation UV Caution, Two Person Lift Attention, Levage par deux Vorsicht, Zwei Personen Required personnes requis erforderlich Avertissement, Substances Achtung, Korrosiven Warning, Corrosive Chemical corrosives Chemikalien Caution, Hot Surface Attention, Surface chaude Vorsicht, Heiße Oberfläche sÉCUritÉ GIlSon CPC SyStEmS... -
Page 13: Notes De Sécurité
Toujours soulever l’instrument par sa base et suivre les instructions de déballage fournies avec l’appareil. Pièces de Remplacement Utiliser exclusivement les pièces détachées mentionnées dans ce guide utilisateur. Gilson CPC systems Gilson CPC systems | USER’S GUIDE | USER’S GUIDE... -
Page 14: Signes De Détérioration
Ne pas laisser de tampon dans le système, cela pourrait causer des bouchages et endommager les joints. Faire passer un solvant propre dans les circuits hydrauliques avant de stocker l’appareil. Rincer les circuits hydrauliques et empêcher les liquides de s’écouler par les entrées et sorties avant de déplacer l’appareil. sÉCUritÉ GIlSon CPC SyStEmS... -
Page 15: Introduction
ChaPter 1 | in this ChaPter ● Description on page 10 ● Unpacking on page 11 ● Technical Specifications on page 14 ● Terms and Abbreviations on page 17 ● Customer Service on page 17 Gilson CPC systems | USER’S GUIDE... -
Page 16: Description
The combination of a CPC System and PLC 2050/2250/2500 Purification System, fully controllable with Gilson Glider CPC (GGC) software, creates a complete purification system for various applications. In this configuration, a detector measures the absorbance and sends the chromatogram to the onboard control software, after which fractions are collected via the integrated fraction collector.. -
Page 17: Unpacking
Carefully unpack the CPC System and its accessories. Verify that all parts are included and undamaged. Do this now, even if the CPC System will not be used immediately. Many carriers must receive concealed damage claims within seven days of delivery. Gilson CPC systems | USER’S GUIDE... - Page 18 If examination reveals that damage has occurred in shipment, notify the carrier and Gilson immediately. Refer to Customer Service on page WARNING Do not plug in the instrument if any damage is detected. Powering the instrument in a damaged state may result in serious injury and may damage internal components of the instrument.
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Page 19: Unpacking List
Unpacking List The following items are considered standard equipment and are provided with the Gilson CPC Systems. stanDarD eQUiPment After the instrument and the accessories have been unpacked, you should have the following: CPC 100, CPC 250, CPC 250 Pro, and CPC 1000 ●... -
Page 20: Technical Specifications
Technical Specifications Please be aware of the following before operating the CPC System. Changes or modifications to the CPC System not expressly approved by Gilson could void the NOTICE warranty. Des changements ou modifications sur l'instrument non formellement approuvés par Gilson AVIS peuvent annuler la garantie accordée. - Page 21 Vespel® 316 SS Tubing, fittings, sample loops, and unions PEEK / ETFE / PTFE System Pressure CPC 100, CPC 250, CPC 250 PRO 100 bar (1450 psi) Maximum Pressure CPC 1000, CPC 1000 PRO 80 bar (1160 psi) Specification Description Line voltage 110‑120 V~ or 220‑240 V~...
- Page 22 1 to 452 g System Range CPC 100 60 kg (132 lbs.) CPC 250 70 kg (154 lbs.) Weight CPC 250 PRO 65 kg (143 lbs.) CPC 1000 120 kg (264 lbs.) CPC 100 PRO 115 kg (253 lbs.) introDUCtion GIlSon CPC SyStEmS...
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Page 23: Terms And Abbreviations
If you need assistance, please contact your local Gilson representative. Specific contact information can be found at www.gilson.com. To help us serve you quickly and efficiently, please refer to Repair and Return Policies... - Page 24 This page intentionally left blank.
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Page 25: Installation
Chapter 2 installation ChaPter 2 | in this ChaPter ● Plumbing Connections on page 20 ● CPC System with PLC Purification System on page 21 ● Electrical Connections on page Gilson CPC systems | USER’S GUIDE... -
Page 26: Plumbing Connections
The column rotary seals are equipped with waste outlets for liquid outflow that may occur if the seals are damaged. All of these waste tubings are already connected to the system. Place them in a suitable waste receptacle. installation GIlSon CPC SyStEmS... -
Page 27: Cpc System With Plc Purification System
ASC Inlet DSC Inlet Figure 6 Inlet Tubing Connections (CPC) ASC outlet (Port 3) DSC outlet (Port 1) Figure 7 Outlet Tubing Connections (Automatic Backflush Valve on PLC Purification System) Gilson CPC systems | USER’S GUIDE... -
Page 28: Electrical Connections
Stop Out Not used. Profinet Intended for original equipment manufacturer (OEM) usage (program loading and upgrade). External Power Supplies power to external devices. Do not use unless instructed to do so by your local Gilson representative. installation GIlSon CPC SyStEmS... -
Page 29: Power Connection
Power Connection The Gilson CPC System is supplied with the appropriate fuses and is ready to operate at the line voltage of the destination country. To make the power connection, plug the AC power cord into the system power receptacle (POWER IN) and then make the connection between the system and the AC power source. -
Page 31: Operation
26 ● Start Up on page 29 ● Control the System on page 30 ● Loop Injection with Manual Valve on page 32 ● Change the Elution Mode (ASC/DSC) on page 33 Gilson CPC systems | USER’S GUIDE... -
Page 32: Front Panel
The front panel includes the power button with indicator light (lower, right corner), touchscreen (top, left side), four function keys for the touchscreen, and two momentarily illuminated push buttons for Run and Stop. Power Button (mAInS) and Power Indicator light Figure 9 Front Side Panel Diagram Display / touchscreen Figure 10 Front Panel Diagram oPeration GIlSon CPC SyStEmS... -
Page 33: Power Button And Power Indicator Light
When pressed, the speed setpoint (or the acceleration setpoint) automatically adjusts to the standard value for rotor loading: ● 500 rpm (or 20 g) for small columns (CPC 100, CPC 250, CPC 250 PRO) ● 500 rpm (or 55 g) for large columns (CPC 1000, CPC 1000 PRO) -
Page 34: Menu
Changing the advanced settings in this menu without Gilson authorization may damage the system and void the warranty. Seul un personnel de service qualifié ou un partenaire Gilson certifié peut avoir accès à l’écran AVIS Setup. Changer les réglages avancés dans ce menu sans l’autorisation de Gilson pourrait endommager le système et annulerait la garantie. -
Page 35: Start Up
Touch the screen. The Control Interface screen opens. Remote Control Do not touch the screen. Turn on the PLC Purification System with embedded Gilson Glider CPC (GGC) software, and wait for the GGC software to load. Ensure first that the software configuration is correct to establish communication. -
Page 36: Control The System
Control the System This section explains how to control a Gilson CPC System used as standalone unit. After the instrument is powered on and the control interface opened, use the built-in touchscreen and buttons to control the rotor. Start the Rotor... -
Page 37: Button Setpoints And Limits
System Button loading Button Elution Acceleration Range Acceleration Acceleration 500 rpm 1600 rpm 100 to 3000 rpm CPC 100 20 g 207 g 1 to 728 g 500 rpm 1600 rpm 100 to 3000 rpm CPC 250 19 g 195 g... -
Page 38: Loop Injection With Manual Valve
Manual Injection Valve - Needle Port la position INJECT à la ATTENTION position LOAD. Utiliser le bouchon du port de l’aiguille, attaché à la poignée, pour vous prémunir de cet éventuel spray. oPeration GIlSon CPC SyStEmS... -
Page 39: Change The Elution Mode (Asc/Dsc)
Refer to the “Operating Instructions” for more explanations of the manual sample injector. When the Gilson CPC System is coupled with a PLC Purification System, there is no injection valve on NOTE the CPC system. The injection process is performed on the PLC system, manually or automatically depending on the injection valve model, and managed by the GGC software. - Page 40 This page intentionally left blank.
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Page 41: Maintenance
ChaPter ● Helpful Hints on page 36 ● Cleaning and Decontamination on page 36 ● Maintenance Schedule on page 37 ● Replace a Seal in a Column Rotary Seal on page 38 Gilson CPC systems | USER’S GUIDE... -
Page 42: Helpful Hints
Helpful Hints To keep the system at optimal performance, Gilson recommends the following: ● Follow the preventative Maintenance Schedule on page 37. ● Do not start the rotor without fluid in the system as this may prematurely wear the seals. -
Page 43: Maintenance Schedule
Maintenance Schedule Gilson recommends performing periodic inspection and maintenance of components of CPC Systems to ensure operational performance. The recommended inspection and maintenance periods are listed below, but are only general guidelines. The frequency of the maintenance will vary depending on the system usage and type of sample injected. -
Page 44: Replace A Seal In A Column Rotary Seal
2. Switch off the system and disconnect the power cord. Reconnect only after replacing the panels. 3. Remove the side panel of the system by removing the four domed-head screws with a 2.5 mm Allen wrench. Rotary Rotor Seal Rotary module Domed- Head Screws Figure 26 Column Rotary Seal Access maintenanCe GIlSon CPC SyStEmS... - Page 45 9. Once the rotary seal head and cleaning disc are removed, loosen the four central M4 screws with a 3 mm Allen wrench to disassemble the head and the cleaning disc. Rotary Seal Head Rotary Seal Cleaning Disc Figure 28 Rotary Seal Assembly Gilson CPC systems | USER’S GUIDE...
- Page 46 12. Thoroughly clean the seal seat with Isopropyl Alcohol (IPA) or ethanol to remove possible worn seal particles, and then immerse the new seal in IPA for lubrication. 13. Align the new seal over the seal seat of the head or cleaning disc. maintenanCe GIlSon CPC SyStEmS...
- Page 47 16. Briskly push part D with the palm of your hand, inserting the seal into position. Figure 32 Column Seal Seating Instructions 17. Remove the tool and examine the seal to ensure it is properly placed. Gilson CPC systems | USER’S GUIDE...
- Page 48 Screws Figure 33 Rotary Seal Reassembly 24. Turn on the instrument, open the Menu screen and then the Hours Counters screen. Press Reset below the Seals field to reset the counter and close the Menu screen. maintenanCe GIlSon CPC SyStEmS...
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Page 49: Troubleshooting
Chapter 5 troUBleshootinG ChaPter 5 | in this ChaPter ● Troubleshooting Table on page 44 ● Error Messages on page 45 ● Repair and Return Policies on page 46 Gilson CPC systems | USER’S GUIDE... -
Page 50: Troubleshooting Table
Troubleshooting Table The following table details some basic symptoms, possible causes, and potential solutions for issues related to Gilson CPC Systems. If the problem persists after all remedies have been attempted, contact Gilson customer service. Refer to Customer Service on page 17. -
Page 51: Error Messages
When a Driver Error occurs, the red STOP button light flashes rapidly on the front panel of the instrument and the error number appears on the front panel display. For assistance with resolving an error, contact your local Gilson representative. Refer to the table below for the error text. Error... -
Page 52: Repair And Return Policies
Repair and Return Policies Before Calling Us your local Gilson representative will be able to serve you more efficiently if you have the following information: ● Serial number and model number of the instruments involved ○ the serial number is located on the left side of the CPC System ●... -
Page 53: Appendix A | Warranty
ChaPter 6 | General A Gilson CPC System is under warranty to be free from defects in material or workmanship under normal use within the instrument specifications indicated in this user’s guide and under conditions given below. The warranty period is one year from the date of initial shipment of the manufacturer. Note that it does not apply to the instrument if modified by the user or resold without permission from the manufacturer, nor to consumable parts after limited warranty expiration, nor to any failure of lifetime-expired parts. -
Page 54: Limited Warranty
● Use of clean solvents and containers ● Following the preventative maintenance schedule DamaGes not CoVereD ● Damaged threads or crushed internal parts caused by improper tightening ● Blocked flow paths caused by improper installation or unsuitable mobile phases Warranty GIlSon CPC SyStEmS... -
Page 55: Appendix B | Replacement Parts And Accessories
Parts anD ChaPter a | aCCessories All items listed must only be supplied by Gilson or an agent thereof. Use of alternate parts CAUTION may lead to improper operation of the system or failure to comply with safety or EMC regulations. - Page 56 Nut, SS for 1/8” tubing (qty. 10) 21041002 Plug, PEEK, 10-32 Miscellaneous Part Number Description 21041003 Fuse, 3.15 A, H 250 V~ 21040150 Fuse, 6.3 A, H 250 V~ 21040160 Serial RS-232 cable male/female rePlaCement Parts anD aCCessories GIlSon CPC SyStEmS...
- Page 57 PEEK, 1/16” OD, 0.75 mm ID, 1 meter 21041016 PEEK, 1/8” OD, 2.0 mm ID, 1 meter 21040171 SS, 1/16” OD, 1.0 mm ID, 1 meter 21040140 SS, 1/8” OD, 2.1 mm ID, 1 meter Gilson CPC systems | USER’S GUIDE...
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Page 59: Appendix C | Materials
Novaflon® 100 impressive adaptability enables it to compensate for minor damage or unevenness in the flange surface. Excellent media resistance makes it the ideal solution for use in the chemical industry. LIQUID CONTACT MATERIALS CONTINUED ON PAGE 54 Gilson CPC systems | USER’S GUIDE... - Page 60 800 deg. F, especially when corrosive conditions are severe. It is not recommended for use at high temperature. This grade can be highly polished with no surface blemishes. LIQUID CONTACT MATERIALS CONTINUED ON PAGE 55 materials GIlSon CPC SyStEmS...
- Page 61 100 description provided by Frenzelit-Werke GmbH (www.frenzelit.com), England Small tube Corporation (www.nesmalltube.com) and Valco Instruments Co. Inc. Stainless Steel, type 316l description provided by new England Small tube Corporation (www.nesmalltube.com) Zirconium oxide description provided by Ceramaret SA (www.ceramaret.ch) Gilson CPC systems | USER’S GUIDE...
- Page 64 LT309176-01...
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