Buchi S-300 Operation Manual

Buchi S-300 Operation Manual

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Mini Spray Dryer S-300
Operation Manual

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Summary of Contents for Buchi S-300

  • Page 1 Mini Spray Dryer S-300 Operation Manual...
  • Page 2 CH-9230 Flawil 1 E-Mail: quality@buchi.com BUCHI reserves the right to make changes to the manual as deemed necessary in the light of experience, especially with respect to structure, illustrations and technical details. This manual is copyrighted. Information from it may neither be reproduced, distributed, or used for competitive purposes, nor made available to third parties.
  • Page 3: Table Of Contents

    Installing the spray gas supply...................... 25 Installing peristaltic pump 2 (option) .................... 25 Installations for remote services (option) ...................  25 Installations for a spray drying mode .................... 26 Installing the outlet filter holder ...................... 26 Operation Manual Mini Spray Dryer S-300...
  • Page 4 7.11.3 Deleting a job list........................ 52 7.11.4 Deleting a job list entry...................... 53 7.11.5 Loading a job list ........................ 53 7.12 Editing an auto mode sequence (Advanced and Corrosive only)............ 53 7.13 Tagging table entries .........................  54 Operation Manual Mini Spray Dryer S-300...
  • Page 5 10.2 Nozzle does not atomize ........................ 70 10.3 Changing the fuse.......................... 70 10.4 Sending instrument data to BUCHI customer service ...............  71 10.5 No liquid delivery .......................... 71 Taking out of service and disposal.................... 72 11.1 Taking out of service..........................  72 11.2...
  • Page 6 Feeding tube ........................ 73 12.1.2 Drying gas hoses ......................... 73 12.2 Spare parts and accessories ...................... 74 12.2.1 Nozzles .......................... 74 12.2.2 Accessories.......................... 78 12.2.3 Glassware .......................... 80 12.2.4 Spare parts .......................... 84 12.2.5 Hoses and tubes ........................ 87 12.2.6 Documents........................... 88 Operation Manual Mini Spray Dryer S-300...
  • Page 7: About This Document

    1.3 Connected instruments In addition to this operation manual, follow the instructions and specifications in the documentation for the connected instruments. Operation Manual Mini Spray Dryer S-300 7/90...
  • Page 8: Safety

    The operator is responsible for damages or hazards that are caused by use other than that intended. Especially the following uses are not permitted: — Use of the instrument with non-BUCHI products. — Use of the instrument in closed mode with non-certified instruments. —...
  • Page 9: Personal Protective Equipment

    Safety-related incidents that occur while using the instrument should be reported to the manufacturer (quality@buchi.com). BUCHI service technicians Service technicians authorized by BUCHI have attended special training courses and are authorized by BÜCHI Labortechnik AG to carry out special servicing and repair measures.
  • Page 10: Warning Notices In This Document

    Indicates a danger that could result in damage to property. 2.6 Warning symbols The following warning symbols are displayed in this operation manual or on the instrument. Symbol Meaning General warning Instrument damage Dangerous electrical voltage Hot surface 10/90 Operation Manual Mini Spray Dryer S-300...
  • Page 11: Residual Risks

    Only use the instrument in well ventilated areas. If vapors escape from connections, check the seals concerned and replace them if necessary. Do not process any unknown fluids. Observe the safety data sheets for all substances used. Operation Manual Mini Spray Dryer S-300 11/90...
  • Page 12: Dangerous Particles

    Always visually inspect glass components for damage every time they are to be used. Do not continue to use glass components that are damaged. Always wear protective gloves when disposing of broken glass. 12/90 Operation Manual Mini Spray Dryer S-300...
  • Page 13: Malfunction Of A Connected Instrument (Option)

    Unauthorized modifications can affect safety and lead to accidents. Use only genuine BUCHI accessories, spare parts and consumables. Carry out technical changes only with prior written approval from BUCHI. Only allow changes to be made by BUCHI service technicians. BUCHI accepts no liability for damage, faults and malfunctions resulting from unauthorized modifications.
  • Page 14: Product Description

    Closed mode with Inert Loop and Dehu- between 20 % - 90 % organic solvent midifier (When using Ultrasonic Package acces- sory inert gas adapter is necessary) 3.2 Configuration 3.2.1 Front view Fig. 2: Front view 14/90 Operation Manual Mini Spray Dryer S-300...
  • Page 15 17 Connection piece with outlet tempera- 18 Separation flask ture sensor 19 Spray cylinder 20 Cylinder holder and sensor plugs See Chapter 3.2.4 "Cylinder holder and sensor plugs", page 17 21 On/Off master switch 22 Peristaltic pump 1 Operation Manual Mini Spray Dryer S-300 15/90...
  • Page 16: Rear View

    See Chapter 3.2.5 "Spray drying noz- zle (Two fluid nozzle)", page 18 Handle Spray gas connection Power supply connection Fuses Aspirator ventilation 10 Lower rear door 11 Ventilation slots 12 Upper rear door 13 Ventilation slots 16/90 Operation Manual Mini Spray Dryer S-300...
  • Page 17: Connections On The Side

    Product description | 3 3.2.3 Connections on the side Fig. 4: Connections RJ32 RJ32 3.2.4 Cylinder holder and sensor plugs Fig. 5: Adjustment and sensor plugs Outlet temperature sensor port Hight correction handle Product temperature sensor port Operation Manual Mini Spray Dryer S-300 17/90...
  • Page 18: Spray Drying Nozzle (Two Fluid Nozzle)

    The type plate identifies the instrument. The following type plate is an example with all possible information. For more details refer to the type plate on the instrument. The type plate is located at the rear of the instrument. 18/90 Operation Manual Mini Spray Dryer S-300...
  • Page 19: Scope Of Delivery

    220 - 240 ± 10 % Heating Control ± 3 °C ± 3 °C ± 3 °C Power consumption max. 2300 W max. 2300 W max. 2300 W Fuse 10 AT 10 AT 10 AT Overvoltage category Operation Manual Mini Spray Dryer S-300 19/90...
  • Page 20: Ambient Conditions

    Cover of the product collection vessel PA12 Seal of the product collection vessel Seal cyclone Silicone, Silicone with PTFE Drying gas tube TPR (Thermoplastic elastomers)/PTFE (Polytetrafluoroethylene) Acid resistant coated metal Stainless steel, PVA Acid resistant metal Titanium 20/90 Operation Manual Mini Spray Dryer S-300...
  • Page 21: Installation Site

    — The installation site meets the specifications according to the technical data (e.g. weight, dimension, etc.). See Chapter 3.5 "Technical data", page 19 — The installation site fits basic electromagnetic environment / Emission Class B. Operation Manual Mini Spray Dryer S-300 21/90...
  • Page 22: Transport And Storage

    Make sure that the ambient conditions are complied with (see Chapter 3.5 "Technical data", page 19). Wherever possible, store the device in its original packaging. After storage, check the device, all glass components, seals and tubing for damage and replace if necessary. 22/90 Operation Manual Mini Spray Dryer S-300...
  • Page 23: Lifting The Instrument

    Lift the instrument at the points indicated. NOTICE Dragging the instrument can damage the feet of the instrument. Lift the instrument when positioning or re-locating. Lift the instrument at the points indicated ((1) + (3) and (2) + (3)). Operation Manual Mini Spray Dryer S-300 23/90...
  • Page 24: Installation

    The installation site is as specified in the technical date. See Chapter 3.5 "Technical data", page 19. Connect the power supply cable to the connection on the instrument. See Chapter 3.2 "Configuration", page 14. Connect the mains plug to an own mains outlet socket. 24/90 Operation Manual Mini Spray Dryer S-300...
  • Page 25: Securing Against Earthquakes

    5.6 Installations for remote services (option) Navigation path: ➔ ➔ NOTE 2.4GHz Network frequency required to operate the instrument remotely. Instrument can only work on this frequency. If not applicable, use hotspot from device. Operation Manual Mini Spray Dryer S-300 25/90...
  • Page 26: Installations For A Spray Drying Mode

    5.7 Installations for a spray drying mode The installations for a spray drying mode, see separate installation manuals. — "Mini Spray Dryer S-300 in closed mode with Dehumidifier and Inert Loop" — "Mini Spray Dryer S-300 in closed mode with Inert Loop"...
  • Page 27 Büchi Labortechnik AG Installation | 5 Attach the filter holder to the instrument with the knurl nuts. Make sure that the warning sign is not visible anymore. Operation Manual Mini Spray Dryer S-300 27/90...
  • Page 28: Interface

    6.2 Navigation bar Icon Description Further information Menu bar Shows available menus. See Chapter 6.2.1 "Menu bar", page 29 Home panel Shows the home screen. See Chapter 10.4 "Sending instrument data to BUCHI customer service", page 71 28/90 Operation Manual Mini Spray Dryer S-300...
  • Page 29: Menu Bar

    Instrument tem. Calibrations See Chapter 9.2 "Calibrating the peri- staltic pumps", page 61 Shows counters and additional informa- tion. Shows the notification history. Logs Displayed when an update is available. Update Shows legal information. About Operation Manual Mini Spray Dryer S-300 29/90...
  • Page 30: Control Panel

    Setting the frequency for the nozzle cleaning. Shows the filter permeability in percent or mbar. See Chapter [Filter press.] "Customizing the control screen", page 32 6.3 Function buttons Icon Explanation [Load] button [Options] button 30/90 Operation Manual Mini Spray Dryer S-300...
  • Page 31: System Settings

    Setting the keyboard clicks to ON/OFF Navigation path ➔ ➔ [System] Navigate to the System submenu according to the navigation path. Select the Sound section. Carry out the changes according to your needs. Operation Manual Mini Spray Dryer S-300 31/90...
  • Page 32: Changing Date And Time

    Filter Pressure The pressure measured at the outlet of the filter in mbar Navigation path ➔ ➔ [Customize] Navigate to the Customize submenu according to the navigation path. Select the Control Panel section. 32/90 Operation Manual Mini Spray Dryer S-300...
  • Page 33: Customize The Report

    Select the graphic you wish to enter. [Company Address] Select the action action. ð The display shows a dialog with an alphanumeric input box. Enter the address. ð The entered values are changed. Operation Manual Mini Spray Dryer S-300 33/90...
  • Page 34: Changing The Measurement Units

    Temperature °C °F Pressure metric imperial Navigation path ➔ ➔ [Customize] Navigate to the Customize submenu according to the navigation path. Select the Localization section. Select the measurement units you wish to use. 34/90 Operation Manual Mini Spray Dryer S-300...
  • Page 35: Preparing For A Spray Drying Process

    Put the prepared filter body in the filter vessel. Secure the filter body in place with the cap nut. Put the filter in the filter holder. Make sure that the filter is attached to the filter holder. Operation Manual Mini Spray Dryer S-300 35/90...
  • Page 36: Preparing The Outlet Filter With Ptfe Membrane (Option)

    Pull the PTFE membrane on the filter body. Secure the filter bag in place with quick release fastener. ð For the initial installation it might be necessary to bend the hold of the fastener slightly towards the filter. 36/90 Operation Manual Mini Spray Dryer S-300...
  • Page 37 Secure the filter body in place with the cap nut. Put the filter in the filter holder. Make sure that the filter is attached to the filter holder. Connect the filter with the instrument. Operation Manual Mini Spray Dryer S-300 37/90...
  • Page 38: Preparing The Glass Assembly

    The filter is prepared. See Chapter 7.1 "Preparing the outlet filter", page 35 Open the hight correction handle. Attach the seal holder with the seal onto the instrument. Attach the separation flask to the spray cylinder. 38/90 Operation Manual Mini Spray Dryer S-300...
  • Page 39 Make sure, that the connection for the outlet temperature sensor shows in the direction indicated. Turn the spray cylinder that the coupling flange fits in the adjustment. Close the handle. Fix the hight correction handle. Operation Manual Mini Spray Dryer S-300 39/90...
  • Page 40: Preparing The Product Vessel

    Attach the cyclone to the spray cylinder. Attach the cyclone to the filter. 7.3 Preparing the product vessel NOTE Removing is done in reverse sequence. Prepare the product collection vessel. Attach the prepared product vessel to the cyclone. 40/90 Operation Manual Mini Spray Dryer S-300...
  • Page 41: Preparing The Spray Drying Nozzle

    Attach the spray gas tube in place with the union nut. Attach the de-block tube to the nozzle Attach the assembled feeding tube onto the FEED connection marked Attach the feed tube in place with the union nut. Operation Manual Mini Spray Dryer S-300 41/90...
  • Page 42: Preparing The Peristaltic Pump

    7.5.2 Preparing the peristaltic pump for auto mode (option) Precondition: The peristaltic pump bed is prepared. See Chapter 7.8 "Adjusting the peristaltic pump bed", page 45 The solvent is prepared. Sample is prepared. Prepare the Y-piece. 42/90 Operation Manual Mini Spray Dryer S-300...
  • Page 43: Preparing The Sensors

    7.6 Preparing the sensors 7.6.1 Preparing the product temperature sensor (option) (first time only) Remove the cap nut from the product collection vessel. (first time only) Remove the sealing from the fixing nut. Operation Manual Mini Spray Dryer S-300 43/90...
  • Page 44: Preparing The Outlet Temperature Sensor

    7.6.2 Preparing the outlet temperature sensor (first time only) Remove the cap nut from the sensor mounting. (first time only) Remove the sealing from the fixing nut. (first time only) Attach the sealing to the sensor. 44/90 Operation Manual Mini Spray Dryer S-300...
  • Page 45: Preparing The Grounding (If No Product Sensor Is Used)

    Attach the grounding cable to the product collection vessel. Connect the grounding cable to the instrument. 7.8 Adjusting the peristaltic pump bed Tools needed: Order no. Image Torx size 15 none Navigation path ➔ Operation Manual Mini Spray Dryer S-300 45/90...
  • Page 46: Preparing The Instrument For Remote Services (Option)

    There are two remote services available: Remote type Explanation [Remote Control] Carrying out the instrument functions from an remote de- vice. Monitoring all values from an remote device. [Monitoring] 46/90 Operation Manual Mini Spray Dryer S-300...
  • Page 47: Editing A Method (Advanced And Corrosive Only)

    Tap the button. ð The copy is created. 7.10.2 Deleting a method Navigation path ➔ Navigate to the Methods menu according to the navigation path. [Options] Tap the button. [Delete] Tap the action. Operation Manual Mini Spray Dryer S-300 47/90...
  • Page 48: Changing The Name Of A Method

    Select the method you wish to edit. Select the Method Parameters section. [Drying Gas] Select the action. ð The display shows a dialog box with a numeric input box. Enter the drying gas volume in m³/h. 48/90 Operation Manual Mini Spray Dryer S-300...
  • Page 49: Changing The Inlet Temperature For A Method

    Select the Method Parameters section. ð The display shows a dialog box with a numeric input box. [Pump] Select the action. Enter the pump volume in mL/min. [Save] Tab the button. ð The pump volume is saved. Operation Manual Mini Spray Dryer S-300 49/90...
  • Page 50: Changing The Outlet Temperature For A Method

    Enter the deblock speed in bpm (values from 0 to 60 are allowed). [Save] Tab the button. ð The deblock speed of the nozzle is saved. 7.10.12 Importing a method the following method format is possible: — .bdmf 50/90 Operation Manual Mini Spray Dryer S-300...
  • Page 51: Exporting A Method

    7.11 Editing a job list (Advanced and Corrosive only) NOTE It is not possible to enter a name twice. 7.11.1 Creating a new job list Navigation path ➔ Navigate to the Job Lists panel. [ + ] Tap the button. Operation Manual Mini Spray Dryer S-300 51/90...
  • Page 52: Adding An Entry To A Job List

    ➔ Navigate to the Job Lists panel. [Options] Tap the button. [Delete] Tap the action. Select the job list you wish to delete. [Delete] Tap the button. ð The job list is deleted. 52/90 Operation Manual Mini Spray Dryer S-300...
  • Page 53: Deleting A Job List Entry

    Navigate to the Auto sequence action according the navigation path. Enter the requested values. [Auto Mode State] Select the you wish to use. [Start] Tap the button. ð The instrument starts a spray drying process with the set parameters. Operation Manual Mini Spray Dryer S-300 53/90...
  • Page 54: Tagging Table Entries

    [ + ] Tap the button. ð The display shows a dialog with an alphanumeric input box. Enter a name for the tag. [Save] Tab the button. ð The list entry is tagged. 54/90 Operation Manual Mini Spray Dryer S-300...
  • Page 55: Carrying Out A Spray Drying Process

    Carrying out each parameter individually. ð With a method. See Chapter 7.10 "Editing a method (Advanced and Corrosive only)", page 47 ð With a job list. See Chapter 7.11 "Editing a job list (Advanced and Corrosive only)", page 51 Operation Manual Mini Spray Dryer S-300 55/90...
  • Page 56 If necessary, load a job list. See Chapter 7.11.5 "Loading a job list", page 53 Navigate to the Control panel according the navigation path. Tap the drying gas start button. ð The instrument starts the auto mode. 56/90 Operation Manual Mini Spray Dryer S-300...
  • Page 57: Tasks During Spray Drying (Manual Mode Only)

    Set the On/Off master switch to On. ð The instrument is starting up. Prepare pure solvent. Prepare the sample. Place sample and solvent on the sample place area. Prepare the peristaltic pump. See Chapter 7.5 "Preparing the peristaltic pump", page 42 Operation Manual Mini Spray Dryer S-300 57/90...
  • Page 58: Starting A Spray Drying Process In Closed Mode

    ð With a method. See Chapter 7.10 "Editing a method (Advanced and Corrosive only)", page 47 ð With a job list. See Chapter 7.11 "Editing a job list (Advanced and Corrosive only)", page 51 Navigation path ➔ 58/90 Operation Manual Mini Spray Dryer S-300...
  • Page 59: Tasks During Spray Drying (Manual Mode Only)

    Tap the heater stop button. If necessary save the run. Wait until the glassware is in ambient temperature. Tap the aspirator stop button. Set the air flow to 0. Remove the product from the product collection vessel. Operation Manual Mini Spray Dryer S-300 59/90...
  • Page 60: Shutting Down The Instrument

    Select the run you wish to delete. [Delete] Tap the button. ð The run is deleted. 8.6 Disconnecting the remote services Precondition: [Take Back Control] The display shows the button. [Take Back Control] Tap the button. 60/90 Operation Manual Mini Spray Dryer S-300...
  • Page 61: Cleaning And Servicing

    Do not carry out any servicing and cleaning operations that involve opening the housing. Use only genuine BUCHI spare parts in order to ensure correct operation and preserve the warranty. Carry out the service and cleaning operations described in this section to extend the lifetime of the instrument.
  • Page 62: Cleaning The Aspirator

    The aspirator is starting up. Wait until the aspirator is dry. 9.4 Opening and closing the lower rear door. Push the snap lock down and pull the door. Remove the exhaust air hose. 62/90 Operation Manual Mini Spray Dryer S-300...
  • Page 63: Opening And Closing The Upper Rear Door

    Check if the outlet filter pressure is not more than 20 mbar relative to the clean filter. If necessary, clean or replace the filter. See Chapter 7.1 "Preparing the outlet filter", page 35 9.8 Cleaning the heater NOTE Installing is done in reverse sequence. Operation Manual Mini Spray Dryer S-300 63/90...
  • Page 64: Cleaning The Glass Components And Temperature Sensors

    Clean all coated temperature sensors (outlet and product) with a soft towel. Use small amounts of solvent is recommended. 9.10 Cleaning the nozzle NOTICE Sharp cleaning tools Sharp cleaning tools can damage the surface. Do not use any sharp cleaning tools. 64/90 Operation Manual Mini Spray Dryer S-300...
  • Page 65 Remove the nozzle cap. Remove the nozzle tip. Clean the nozzle with a small cleaning brush, cleaning agent and water. Clean the nozzle pipe and needle with a damp cloth, cleaning agent and water. Operation Manual Mini Spray Dryer S-300 65/90...
  • Page 66: Cleaning And Servicing The Warning And Directive Symbols

    If they are dirty, clean them. 9.12 Cleaning the housing Wipe down the housing with a damp cloth. If heavily soiled, use ethanol or a mild detergent. Wipe down the display with a damp cloth. 66/90 Operation Manual Mini Spray Dryer S-300...
  • Page 67: Help With Faults

    If necessary, replace the seals. Product drips in No spray flow. Open spray gas valve. spray cylinder. Check pressure of the spray Insufficient spray flow. gas in the supply tube (5–8 bar). Operation Manual Mini Spray Dryer S-300 67/90...
  • Page 68: Troubleshooting Heater

    Contact BUCHI Customer (Faulty flow direction or no Service. flow in the heating system). Outlet temperature Sensor not inserted. Place outlet sensor in coupling does not rise. element. Fault in tubing system. Check tubing system. 68/90 Operation Manual Mini Spray Dryer S-300...
  • Page 69 Hose not dipped into sample Dip hose into sample vessel. vessel. Change of sample concen- Agitate the sample (magnetic tration. agitator) to obtain uniform concentration. No feed of product. Switch on peristaltic pump. Operation Manual Mini Spray Dryer S-300 69/90...
  • Page 70: Troubleshooting Aspirator

    Make sure the O-ring on the fuse carrier is not damaged. Replace the defective fuse (1). Screw in the fuse carrier. Connect the power supply cable. If the fuse brakes repeatedly contact the Contact BUCHI Customer Service. 70/90 Operation Manual Mini Spray Dryer S-300...
  • Page 71: Sending Instrument Data To Buchi Customer Service

    Büchi Labortechnik AG Help with faults | 10 10.4 Sending instrument data to BUCHI customer service Navigation path ➔ Precondition: A data storage device is connected to the instrument. Navigate to the Home menu according the navigation path. [Support] Tap the button.
  • Page 72: Taking Out Of Service And Disposal

    When disposing, observe the disposal regulations of the materials used. Materials used see Chapter 3.5 "Technical data", page 19. 11.3 Returning the instrument Before returning the instrument, contact the BÜCHI Labortechnik AG Service Department. https://www.buchi.com/contact 72/90 Operation Manual Mini Spray Dryer S-300...
  • Page 73: Appendix

    Dichloromethane Methanol Ethanol Acetone Toluene Acetonitrile Tetrahydrofuran Ethyl acetate Hexane Hydrochloric acid Sulfuric acid Acetic acid Formic acid Sodium hydroxide Ammonia Water (+) = resistant, (-) = non-resistant, (/) = no information available Operation Manual Mini Spray Dryer S-300 73/90...
  • Page 74: Spare Parts And Accessories

    Nozzle cleaning 0.7 mm acid proof, complete 11059876 Cleaning brush for nozzle 044782 Screw connection product tube 044628 Screw connection air and cooling 044629 O-ring for nozzle cleaner, FKM (black), 2× 3.00 x 044469 1.50 mm 74/90 Operation Manual Mini Spray Dryer S-300...
  • Page 75 Order no. Image Needle 0.5 mm 11056864 Needle 0.7 mm 044618 Needle 1.4 mm 046372 Needle 2.0 mm 046373 Needle 0.7 mm titanium 11056315 Needle 1.4 mm titanium 11056417 Needle 2.0 mm titanium 11056422 Operation Manual Mini Spray Dryer S-300 75/90...
  • Page 76 Nozzle tip 2.0 mm 046377 Nozzle tip 0.7 mm titanium 11056317 Nozzle tip 1.4 mm titanium 11056419 Nozzle tip 2.0 mm titanium 11056424 Nozzle caps Order no. Image Nozzle cap 1.4 mm 044649 76/90 Operation Manual Mini Spray Dryer S-300...
  • Page 77 O-ring nozzle cap silicone (red), 2× 16.00 × 2.00 002103 O-ring for needle and nozzle tip, FKM (green), 4 004222 × 6.00 × 1.50 mm O-ring for nozzle cleaner, FKM (black), 2× 3.00 × 038348 1.50 mm Operation Manual Mini Spray Dryer S-300 77/90...
  • Page 78: Accessories

    Dehumidifier S-396 230 V 11073814 Dehumidifier S-396 240 V 11073815 Inert Loop S-395 200V 50Hz 11074620 Inert Loop S-395 220-240V 50Hz 11074621 Inert Loop S-395 200V 60Hz 11074622 Inert Loop S-395 220V 60Hz 11075174 78/90 Operation Manual Mini Spray Dryer S-300...
  • Page 79 Only for open mode. Replacement filter with seal 011238 Spray cylinder chrome steel, complete 11064367 Adapter USB-Wi-Fi/Bluetooth 11072500 Oil-free compressor, 230V 50Hz 027907 Oil-free compressor, 230V 60Hz 11055737 Compressed air maintenance unit 004366 Operation Manual Mini Spray Dryer S-300 79/90...
  • Page 80: Glassware

    Glass assembly S-300, complete 11071071 Glass assembly S-300 brown, complete 11073658 Glass assembly corrosive S-300, complete 11071420 Glass assembly S-300 HP cyclone, complete 11074494 Glass assembly S-300 HP cyclone brown, com- 11074495 plete Cyclones Order no. Image Standard cyclone 11071060...
  • Page 81 044673 Spray cylinder brown 044726 Spray cylinder vertical outlet 044697 Spray cylinder vertical outlet, brown 044728 Cylinder insulation 040058 Collection vessels Order no. Image Product collection vessel 044678 Product collection vessel brown 044727 Operation Manual Mini Spray Dryer S-300 81/90...
  • Page 82 Cover for large collection vessel HP cyclone 11056901 Screw cap SVL 30 005223 Flange screw coupling 034139 Other glassware related spare parts Order no. Image Angle tube 11070485 Angle tube brown 11073660 82/90 Operation Manual Mini Spray Dryer S-300...
  • Page 83 Cover product vessel corrosive 11071425 Coupling flange 11073537 Coupling flange corrosive 11071421 Set flange screw coupling 1 pcs. 11074579 O-ring FKM for screw coupling 001535 Tension spring 032017 Knurled handle with recess 11071059 Operation Manual Mini Spray Dryer S-300 83/90...
  • Page 84: Spare Parts

    Separation flask brown 004343 Quick connector Nozzle Ø6 11071105 Spray cylinder holder 044710 Screw for spray cyclinder holder 044712 O-ring to spray cylinder 044711 12.2.4 Spare parts Order no. Image Set O-ring Plastiperfl. S-300 11074501 84/90 Operation Manual Mini Spray Dryer S-300...
  • Page 85 Gasket SVL 42x35 PTFE 11071325 Outlet filter, complete 11071410 Outlet filter corrosive, complete 11071411 PTFE membrane filter with clamp 11075115 Polyester filter bags (6 units) 035004 Quick release clamp 11071080 Filter holder grounded 11073770 Operation Manual Mini Spray Dryer S-300 85/90...
  • Page 86 Metal tube connector 004251 Silicone tube for nozzle cooling, 4 m 004139 Compressed gas hose, complete 11073584 Tygon tube MH2375 transparent (per m) 046314 Tygon tube F 4040 A yellow (per m) 046315 86/90 Operation Manual Mini Spray Dryer S-300...
  • Page 87: Hoses And Tubes

    Hose Inert Loop TPR conf. 11071076 Tube Dehumidifier TPR conf. 11074039 Tube filter FEP conf. corr. 11072988 Hose TPR 0.7 m conf. 11071051 Hose TPR 1.0 m conf. 11071053 Hose PTFE 0.7 m conf. 11071054 Operation Manual Mini Spray Dryer S-300 87/90...
  • Page 88: Documents

    Hose PTFE 1.0 m conf. 11071056 Hose PTFE 0.7 m conf. coated 11071606 Hose PTFE 1.0 m conf. coated 11071608 12.2.6 Documents Order no. Set IQ/OQ S-300 en 11074567 Repeating OQ S-300 en 11074568 88/90 Operation Manual Mini Spray Dryer S-300...
  • Page 90 We are represented by more than 100 distribution partners worldwide. Find your local representative at: www.buchi.com...

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