Shodex IC SI-90 4E Operation Manual

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(Please read this manual carefully to achieve the best and consistent column performance for a long time)
Important Handling Instructions
Caution!
· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column
and understand their proper handling methods to prevent potential health hazards or death
from occurring.
· Please wear appropriate personal protective equipment such as lab goggles and gloves
when handling organic solvents and acid and alkaline reagents. Avoid any direct physical
contact to prevent chemical injuries.
Before Using the Column
(1) Please visually inspect the package and outside of the column for any damage.
(2) Please check if product name and serial number written on the column package, column name tag, and
enclosed Certificate of Analysis (CoA) are matching and correct.

1. Introduction

Thank you for purchasing the Shodex product. Shodex IC SI-90 4E is a suppressor type ion chromatography
column for analysis of anions, using sodium carbonate eluents. The column is suitable for the separations of
standard inorganic anions including fluoride, chloride, nitrite, bromide, nitrate, phosphate, and sulfate, as well
as organic acid anions such as acetate and formic acid.

2. Column Components

3. Column Specifications

Product
Product Name
Code
F6995244
IC SI-90 4E
F6709620
IC SI-90G
Base Material
: Spherical porous particles of polyvinyl alcohol modified with quaternary ammonium group
Column Housing : PEEK
Screw Type
: Internally-threaded type No.10-32 UNF
Shipping Solvent : 1.8 mM Sodium Carbonate Solution + 1.7 mM Sodium Bicarbonate Solution
Operation Manual
Shodex
IC SI-90 4E
Column Size (mm)
I.D.
Length
4.0
4.6
SHOWA DENKO K.K. (https://www.shodex.com/)
Particle Size
(μm)
250
9
10
9
ver.211013E
Theoretical Plate
Number
(Per Column)
≥ 5,000
(Guard Column)
1

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Summary of Contents for Shodex IC SI-90 4E

  • Page 1 Certificate of Analysis (CoA) are matching and correct. 1. Introduction Thank you for purchasing the Shodex product. Shodex IC SI-90 4E is a suppressor type ion chromatography column for analysis of anions, using sodium carbonate eluents. The column is suitable for the separations of standard inorganic anions including fluoride, chloride, nitrite, bromide, nitrate, phosphate, and sulfate, as well as organic acid anions such as acetate and formic acid.
  • Page 2 Range Recommended Maximum Recommended Range (Per Column) IC SI-90 4E 3 - 12 20 - 60 IC SI-90G Usable solvents are listed below. (1) In general, a mixture of sodium carbonate solution and sodium bicarbonate solution is used. (2) The standard eluent is 1.8 mM sodium carbonate solution and 1.7 mM sodium bicarbonate solution.
  • Page 3 · It is recommended to set the pump limiter to avoid exceeding the maximum pressure. 7.3 Solvent Exchange When replacing the solvent, start the system at less than 0.5 mL/min. Recommended solvent volume to introduce at each step is 3 to 5 times of the column volume. SHOWA DENKO K.K. (https://www.shodex.com/)
  • Page 4 (a cool and dark space is recommended). Refer to section 7.3 Solvent Exchange for how to replace the eluent. Attention! · Never allow inside of the column to dry. It can damage the column. SHOWA DENKO K.K. (https://www.shodex.com/)
  • Page 5 (2) Do not make a strong impact on the column. Do not drop or hit the column on a hard surface. Refer to the Shodex™ website (https://www.shodex.com/) for product details and their applications. For additional assistance, contact the distributor from whom you purchased the column or contact your regional Shodex...
  • Page 6 11. Warranty (Ver. 4COLUMN) (1) Showa Denko K. K. warrants that the Shodex product, at the time of delivery to the user, will conform to the specification of the attached CERTIFICATE OF ANALYSIS, if the Shodex product is used in accordance with the attached operating manual.

This manual is also suitable for:

Ic si-90gF6995244F6709620

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