Shodex IC SI-36 4D Operation Manual

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(Please read this manual carefully to achieve the best and consistent column performance for a long time)
Important Handling Instructions
Caution!
· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column
and understand their proper handling methods to prevent potential health hazards or death
from occurring.
· Please wear appropriate personal protective equipment such as lab goggles and gloves
when handling organic solvents and acid and alkaline reagents. Avoid any direct physical
contact to prevent chemical injuries.
Before Using the Column
(1) Please visually inspect the package and outside of the column for any damage.
(2) Please check if product name and serial number written on the column package, adhesive label, and
enclosed Certificate of Analysis (CoA) are matching and correct.

1. Introduction

Thank you for purchasing the Shodex product. Shodex IC SI-36 4D is a
chromatography column for analysis of anions. The column is used with hydroxide eluents such as
potassium hydroxide and sodium hydroxide. The column is suitable for the separations of standard anions
including fluoride, chloride, nitrite, bromide, nitrate, sulfate, and phosphate, as well as sulfite.

2. Column Components

3. Column Specifications

Product
Product Name
Code
F6999361
IC SI-36 4D
F6709620
IC SI-90G
Base Material
: Spherical porous particles of polyvinyl alcohol modified with quaternary ammonium group
Column Housing : PEEK
Screw Type
: Internally-threaded type No.10-32 UNF
Shipping Solvent : 10 mM Sodium Sulfate Solution (SI-36 4D)
: 1.8 mM Sodium Carbonate Solution + 1.7 mM Sodium Bicarbonate Solution (SI-90G)
Operation Manual
Shodex
IC SI-36 4D
Column Size (mm)
I.D.
Length
4.0
150
4.6
SHOWA DENKO K.K. (https://www.shodex.com/)
Particle Size (μm)
3.5
10
9
ver.200603E
suppressor type ion
Theoretical Plate
Number
(Per Column)
≥ 8,500
(Guard Column)
1

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Summary of Contents for Shodex IC SI-36 4D

  • Page 1 1. Introduction suppressor type ion Thank you for purchasing the Shodex product. Shodex IC SI-36 4D is a chromatography column for analysis of anions. The column is used with hydroxide eluents such as potassium hydroxide and sodium hydroxide. The column is suitable for the separations of standard anions including fluoride, chloride, nitrite, bromide, nitrate, sulfate, and phosphate, as well as sulfite.
  • Page 2 Range Recommended Maximum Recommended Range (Per Column) IC SI-36 4D 3 - 14 20 - 60 IC SI-90G Usable solvents are listed below. (1) In general, either potassium hydroxide or sodium hydroxide is used. (2) The standard eluent is 25-mM potassium hydroxide. The higher the concentration of potassium hydroxide, the faster the elution of ions will be.
  • Page 3 · If using a manually prepared eluent, keep the eluent in a solvent reservoir with a carbonate trap cartridge. Note · Use of on-line degasser is recommended. · It is recommended to set the pump limiter to avoid exceeding the maximum pressure. SHOWA DENKO K.K. (https://www.shodex.com/)
  • Page 4 · When reusing the column stored in a refrigerator, first wait for the column temperature to be ambient, and then remove the end caps and install the column on the system. SHOWA DENKO K.K. (https://www.shodex.com/)
  • Page 5 (2) Do not make a strong impact on the column. Do not drop or hit the column on a hard surface. Refer to the Shodex™ website (https://www.shodex.com/) for product details and their applications. For additional assistance, contact the distributor from whom you purchased the column or contact your regional Shodex...
  • Page 6 User’s exclusive remedy and Showa Denko K.K.‘s exclusive liability for such claim are limited to the replacement of the Shodex product in question. In no event is Showa Denko K.K. liable for any indirect, incidental or consequential damage arising out of in connection with the Shodex product, whether or not such damage is allegedly based on breach of warranty, negligence or otherwise.

This manual is also suitable for:

Ic si-90gF6999361F6709620

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