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Summary of Contents for Bruker Fourier 300
- Page 1 Fourier Fourier 300 Quick Start Installation Guide Version Innovation with Integrity...
- Page 2 © December 20, 2011: Bruker Corporation Rheinstetten, Germany P/N: Z33048 DWG-Nr.: Z4D11877 For further technical assistance on the Fourier unit, please do not hesitate to contact your nearest BRUKER dealer or contact us directly at: BRUKER Corporation am Silberstreifen D-76287 Rheinstetten...
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Page 3: Table Of Contents
Table of Contents Contents Getting Started....................5 This Manual......................5 Before You Begin ..................... 5 Unpacking the Console .................... 5 Console Connections ....................6 External Filters ......................6 Adjusting the Air Pressure..................7 Switching On the Console the First Time ..............7 1.7.1 Verifying That the Console Has Booted .............. - Page 4 Table of Contents Z33048_00_01...
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Page 5: Getting Started
This manual is intended to be a quick-start reference guide for Bruker service techni- cians. It provides basic information for installing and setting up the Fourier 300 system. Carefully read the information in this manual, as well as, the safety information... -
Page 6: Console Connections
Getting Started Console Connections Figure 1.1 Console Connections External Filters Some earlier models come with three external filters: • Z13383 is connected to the 1H connector on the rear of the console. • Z14331 is connected to the C13 connector on the rear of the console. •... -
Page 7: Adjusting The Air Pressure
To access any of the Web server sites, the following password and user name are required: User: root Password: BRUKER (in capitals!) If you are not sure the DHCP Server is running, you can check by opening: Control Panel -> Administrative Tools -> Services -> Bruker DCHP Server Figure 1.2 Bruker DCHP Server Z33048_00_01... -
Page 8: Copying The Probe Data To The Pc System
Getting Started If you are not sure what addresses have been assigned, you can check by opening the following file: Bruker\Diskless\dchpd.leases lease 149.236.99.254 { starts 4 2010/08/19 11:08:55; ends 2 2038/01/19 03:14:06; tstp 2 2038/01/19 03:14:06; binding state active; next binding state free;... -
Page 9: Setting The Magnet To The Correct Field
Getting Started Setting the Magnet to the Correct Field The magnet is designed to be operated at 300.18 MHz, with the current in the H0 field coil of the shim system set to zero. At this frequency the synthesizers are “cleanest” and least likely to create spurious problems. -
Page 10: Figure 1.3 Setting The Spin Safety Threshold
Getting Started Figure 1.3 Setting the Spin Safety Threshold Remove the sample, or activate the sample lift, and annotate the “empty” spin volt- age. Insert, or lower the sample, and switch on the spin (either from the BSMS panel or from the Web server). -
Page 11: Initial Shimming
Getting Started 1.11 Initial Shimming First level shimming is done in the usual way by first setting the currents given in the magnet manual and then seeing if the base shim can be improved in the GS mode. Once the cryo-shims are set, continue adjusting the lower orders of the BOSS1 shim system in the GS mode until your FID half height has reached approximately 100 ms. -
Page 12: Manual Shimming To Lineshape
Converting the Parameter Set to the Actual BF1 Before converting the parameter set, make a backup copy of the PAR directory, e.g: C:\Bruker\TopSpin3.1.b.12\exp\stan\nmr\par This can be done using CF, followed by “expinstall”. However, the preferred way is to use CF, followed by the command “paracon”, since it also converts parameter sets in the user directory. -
Page 13: Creating A Shim Map For Gradshim
Getting Started Figure 1.6 Parameter Set Conversion NOTE: If the BF1 has been changed, you will need to restart the console after perform- ing CF, or paracon has been carried out. Otherwise, the lock frequency will not be updated. 1.15 Creating a Shim Map for Gradshim Gradshim works best when the shim map was made using a well shimmed magnet. -
Page 14: Atp Tests And Customer Acceptance
1.16 ATP Tests and Customer Acceptance The required Hardware Tests (HWT) for the Fourier 300 are carried out during console end testing and are not intended to be repeated at the customer site. The following ATP tests are relevant for the Fourier: •... - Page 15 Getting Started • Lineshape test for 1H with rotation • Resolution test for 1H • Sensitivity test for 1H • Lineshape Test for 13C with rotation • Resolution test for 13C • Sensitivity test for 13C (ASTM) • Sensitivity test for 13C (EB) •...
- Page 16 Getting Started and 2D spectra. If this part contains spectral information, simply increase the spec- tral width. Note: If you obtain reproducible “spurious spikes” in 1H spectra it may be due to an unfavorable BF1 frequency. The Fourier DDS are “clean” for at least 200 ppm at around 300.18 MHz.
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Page 17: Appendix
Appendix Appendix Main Differences Between Fourier and AVANCE The main differences between the Fourier and AVANCE are that with the Fourier: • The lock works at 1 kHz instead of 6 kHz, which means that sidebands are closer together. Also, the lock parameters have different units for BSMS values. Table 1.1. - Page 18 Main Differences Between Fourier and AVANCE Z33048_00_01...
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Page 19: Figures
Figures Figures Figure 1.1 Console Connections................6 Figure 1.2 Bruker DCHP Server................7 Figure 1.3 Setting the Spin Safety Threshold ............10 Figure 1.4 Results of the AU Program FLOCK ............. 11 Figure 1.5 Updating the BSMS Field Value in the edlock Table ......12 Figure 1.6... - Page 20 Figures Z33048_00_01...
- Page 22 Bruker Corporation info@bruker.com www.bruker.com Order No: Z33048...
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