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Bruker D8 Series User Manual

Bruker D8 Series User Manual

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D8 Series
User Manual
Instrument Performance Verification Booklet
D8 ADVANCE / D8 DISCOVER / D8 ENDEAVOR
Original Instructions
XRD
Innovation with Integrity

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Summary of Contents for Bruker D8 Series

  • Page 1 D8 Series User Manual Instrument Performance Verification Booklet D8 ADVANCE / D8 DISCOVER / D8 ENDEAVOR Original Instructions Innovation with Integrity...
  • Page 2 All configurations and specifications are subject to change without notice. Order no. DOC-M88-EXX157 V17 . Updated: April 12, 2019. © 2009 - 2019 Bruker AXS GmbH, Karlsruhe, Germany. All trademarks and registered trademarks are the sole property of their respective owners.

  • Page 3: Table Of Contents

    Declaration of Conformity .................... 31 Bragg-Brentano Geometry with Cobalt Anode.............. 31 Part I: Instrument Details (D8 Series) ................ 33 Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series).... 39 C. Factory Acceptance Test Protocol..................... 41 Declaration of Conformity .................... 41 Parallel Beam Geometry with Copper Anode .............. 41 Part I: Instrument Details .................... 43...
  • Page 4 Declaration of Conformity .................... 67 Bragg-Brentano Geometry with Cobalt Anode.............. 67 Part I: Instrument Details (D8 Series) ................ 69 Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series).... 75 G. Customer Acceptance Test Protocol.................. 77 Declaration of Conformity .................... 77 Parallel Beam Geometry with Copper Anode .............. 77 Part I: Instrument Details .................... 79...

  • Page 5: Introduction

    Introduction This guidance outlines procedures recommended by Bruker AXS for instrument verification. The procedures described apply to all Bruker AXS D8  ADVANCE, D8  DISCOVER, and D8  ENDEAVOR diffraction systems used for X-ray powder diffraction analysis in reflection mode and fully cover the functionality of all validation relevant components of these diffraction systems as provided in the following table.

  • Page 6: Performance Verification Levels

    Introduction Bragg-Brentano Systems Parallel Beam Systems Diffractometer D8 ADVANCE D8 ENDEAVOR D8 ADVANCE D8 DISCOVER D8 DISCOVER Detector Scintillation counter LYNXEYE XE Scintillation counter Solid state detector LYNXEYE XE‑T Solid state detector (SOL‑XE) (SOL‑XE) LYNXEYE‑2 Linear detector VÅNTEC‑1 Linear detector VÅNTEC‑1 SSD160‑2 Linear detector LYNXEYE / Linear detector LYNXEYE / LYNXEYE‑2 /...

  • Page 7: Performance Verification In Gxp Regulated Areas

    (EQ) process as defined by GxP regulations. If your laboratory is not required to comply with GxP regulations you may skip this section. For instrument qualification Bruker AXS recommends the adaptation of the specifications and procedures provided in this booklet into your in-house EQ system according to the following schema: Table 1.2: Instrument performance verification as part of equipment qualification...
  • Page 8 Introduction 8 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 9: Procedures

    An instrument passing all tests with respect to line position, intensity and shape is automati- cally fit for all kinds of X-ray analysis. For GxP regulated laboratories Bruker AXS recommends to use the procedures provided in this chapter as a base for the creation of in-house SOPs.
  • Page 10 Procedures Table 2.1: Instrument parameters for Bragg-Brentano systems (incl. TWIN / TRIO Bragg-Brentano setting) Instrument Parameter Value Value (with air scatter screen) 3) 5) 3) 5) Generator settings Cu: 40 kV / 40 mA Cu: 40 kV / 40 mA 3) 5) 3) 5) Co: 35 kV / 40 mA Co: 35 kV / 40 mA Divergence slit 0.3°...

  • Page 11: Measurement Parameters

    Procedures Table 2.2: Instrument parameters for parallel beam systems with 40 mm Göbel mirrors in primary TWIN / TRIO optics Instrument Parameter Value 1), 2) Generator settings Cu: 40 mA / 40 kV 1),2) Co: 35 mA / 40 kV Radiation safety slit holder 1 mm Göbel mirror with axial Soller slit 2.5°...

  • Page 12: Evaluation Procedures And Data Interpretation

    Procedures Table 2.5: Measurement parameters for Co radiation Reflection Scan angles 2θ [°] Step width 2θ [°] Step time [s] 0 1 2 29.2 - 30.4 0.005 1 0 4 40.3 - 41.8 0.005 3 0 0 80.8 - 81.9 0.01 2 2 6 117.2 - 119.4 0.02...

  • Page 13: Instruments Without Focusing Monochromator

    Procedures 2.4.2 Instruments Without Focusing Monochromator For instruments without primary beam monochromator the impact of the K component of the α2 radiation emitted by the X-ray source has to be taken into account. In order to achieve line in- tensities as accurate as possible, the complete K doublet must be used.
  • Page 14 Procedures 14 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 15: Reference Values

    NIST SRM1976c origin to fit to a large variety of sample stages, as it is very stable, robust, long lasting, and does not require any preparation. The certificate is dedicated to Cu-radia- tion. However, Bruker AXS uses the d-spacing of this standard also for verifying angular ac- curacy (line-position and FWHM) for Co-radiation.

  • Page 16: Basic Setup (Bragg-Brentano, Dedicated And Twin / Trio Optics)

    Reference Values Table  3.1: Reference values for line positions and relative intensities for Cu-radiation (CuK α1 λ = 0.154059 nm) Reflection Line position 2θ [°] Line position 2θ [°] Relative intensity (Net area rounded Bragg-Brentano Parallel Beam to 2 decimal place) 0 1 2 25.575 25.561 23.88...

  • Page 17: Factory And Customer Acceptance Test Protocol

    Reference Values 3. The deflection angle must be saved to data base of the MEASUREMENT SUITE by the Save configuration to data base of the Configuration plugin. ´ The software will ask for a name for this configuration. The name is Instrument Verification Factory.
  • Page 18 Reference Values Table 3.4: Maximum allowed values for the line shape in terms of FWHM (Co-radiation). SC: scintillation counter, SOL‑XE: energy dispersive solid state detector, position sensitive detector VÅNTEC‑1, SSD160, LYNXEYE / LYNXEYE XE / LYNXEYE XE‑T, LYNXEYE-2, SSD160-2 and EIGER2 R 500K Reflection Bragg-Brentano Parallel Beam (Göbel Mirror) SC / SOL‑XE VÅNTEC‑1...

  • Page 19: References - Glossary - Appendices A To I

    (for installations outside North America) D8 DISCOVER User Manual Vol. 2 DOC-M88-EXX162 D8 DISCOVER Supplement Folder DOC-M88-EXX163 D8 Series IQ OQ PQ for D8 ADVANCE / D8 DISCOVER DOC-M88-EXX160 D8 ENDEAVOR IQ OQ PQ DOC-M88-EXX265 LYNXEYE and SSD160 User Manual DOC-M88-EXX095 LYNXEYE XE User Manual...
  • Page 20 References – Glossary – Appendices A to I Glossary Certified reference material A reference material, accompanied by a certificate, one or more of whose property values are certified by a procedure, which establishes its traceability to an accurate realization of the unit in which the property values are expressed, and for which each certified value is accompanied by an uncertainty at a stated level of confidence.

  • Page 21: Factory Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in Bragg-Brentano reflection geometry. The factory acceptance test proce- dure consists in full-profile measurements of the certified NIST standard reference material SRM1976c.
  • Page 22 A. Factory Acceptance Test Protocol Comments 22 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 23: Part I: Instrument Details (D8 Series)

    A. Factory Acceptance Test Protocol Part I: Instrument Details (D8 Series) Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractome- D8 ADVANCE Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes)
  • Page 24 A. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector (SOL‑XE) SOL‑XE User Manual DOC-M88-EXX113 VÅNTEC‑1...
  • Page 25 A. Factory Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractometer D8 DISCOVER Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV /  30 mA (for FF tubes) TXS Power: 50 kV / 100 mA (for 0.3x3 mm filament, line and spot focus) TXS Power: 50 kV / 22 mA (for 0.1x1 mm filament, spot focus) Vertical...
  • Page 26 A. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Slits Fixed divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Fixed antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Variable divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Variable antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Motorized air scatter screen Automatic mode Primary axial Soller slit...
  • Page 27 A. Factory Acceptance Test Protocol Instrument Configuration D8 ENDEAVOR Instrument Details Set Values for Validation Diffractometer D8 ENDEAVOR Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer Height: Radius: 200,5 Rotating...
  • Page 28 A. Factory Acceptance Test Protocol Comments 28 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 29: Part Ii: Angular Accuracy, Instrument Response And Resolution (D8 Series)

    Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series) Anode: Cu Bragg-Brentano Geometry Angular Accuracy: Difference Reference Position corr Instrument Response: I Instrument Resolution Maximum allowed 2θ deviation depends on height Maximum allowed intensity deviation for point detectors ± 10% FWHM <...
  • Page 30 Comments...

  • Page 31: Factory Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in Bragg-Brentano reflection geometry. The factory acceptance test proce- dure consists in full-profile measurements of the certified NIST standard reference material SRM1976c.
  • Page 32 B. Factory Acceptance Test Protocol Comments 32 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 33: Part I: Instrument Details (D8 Series)

    B. Factory Acceptance Test Protocol Part I: Instrument Details (D8 Series) Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV / 30 mA (for FF tubes)
  • Page 34 B. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector SOL‑XE User Manual DOC-M88-EXX113 (SOL‑XE)
  • Page 35 B. Factory Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractometer D8 DISCOVER Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Theta/2Theta Height: Radius: Primary radius ....[mm] Secondary radius ....[mm] Horizontal...
  • Page 36 B. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Slits Fixed divergence Divergence slit: 0.3° (approx. 0.6 mm) Fixed antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Variable divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Variable antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Motorized air scatter screen Automatic mode Primary axial Soller slit...
  • Page 37 B. Factory Acceptance Test Protocol Instrument Configuration D8 ENDEAVOR Instrument Details Set Values for Validation Diffractometer D8 ENDEAVOR Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Height: Radius: 200,5 Rotating Sample position A1 Monochroma- Kβ-Filter tisation...
  • Page 38 B. Factory Acceptance Test Protocol Comments 38 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 39: Part Ii: Angular Accuracy, Instrument Response And Resolution (D8 Series)

    Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series) Anode: Co Bragg-Brentano Geometry Angular Accuracy: Difference Reference Position corr Instrument Resolution Maximum allowed 2θ deviation depends on height FWHM < FWHM 2θ Difference 2θ Difference 2θ FWHM FWHM [°]...
  • Page 40 Comments...

  • Page 41: Factory Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in parallel beam reflection geometry (Göbel mirror systems). The factory ac- ceptance test procedure consists in full-profile measurements of the certified NIST standard reference material NIST SRM1976c .
  • Page 42 C. Factory Acceptance Test Protocol Comments 42 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 43: Part I: Instrument Details

    C. Factory Acceptance Test Protocol Part I: Instrument Details Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer...
  • Page 44 C. Factory Acceptance Test Protocol Instrument Details Set Values for Validation VÅNTEC‑1 VÅNTEC‑1 User Manual DOC-M88-EXX072 EIGER2 R 500K EIGER2 R 500K User Manual DOC-M88-EXX293 including D8 ADVANCE ECO 40 kV / 25 mA in case of D8 ADVANCE ECO Comments 44 / 96 DOC-M88-EXX157_V17_04.2019...
  • Page 45 C. Factory Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractome- D8 DISCOVER Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV /  30 mA (for FF tubes) TXS Power: 50 kV / 100 mA (for 0.3x3 mm filament, line and spot focus) TXS Power: 50 kV / 22 mA (for 0.1x1 mm filament, spot focus) Vertical...
  • Page 46 C. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Slits Primary axial Soller slit 2.5° Secondary equatorial Soller slit 0.2° Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2...

  • Page 47: Part Ii: Angular Accuracy, Instrument Response And Resolution

    Part II: Angular Accuracy, Instrument Response and Resolution Anode: Cu Parallel Beam Geometry Angular Accuracy: Difference Deflection angle corr Instrument Response: I Instrument Resolution Maximum allowed 2θ deviation depends on height Maximum allowed intensity deviation for point detectors ± 10% FWHM <...
  • Page 48 Comments...

  • Page 49: Factory Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in parallel beam reflection geometry (Göbel mirror systems). The factory ac- ceptance test procedure consists in full-profile measurements of the certified NIST standard reference material NIST SRM1976c .
  • Page 50 D. Factory Acceptance Test Protocol Comments 50 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 51: Part I: Instrument Details

    D. Factory Acceptance Test Protocol Part I: Instrument Details Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer...
  • Page 52 D. Factory Acceptance Test Protocol Instrument Details Set Values for Validation VÅNTEC‑1 VÅNTEC‑1 User Manual DOC-M88-EXX072 EIGER2 R 500K EIGER2 R 500K User Manual DOC-M88-EXX293 1) including D8 ADVANCE ECO 2) 35 kV / 28 mA in case of D8 ADVANCE ECO Comments 52 / 96 DOC-M88-EXX157_V17_04.2019...
  • Page 53 D. Factory Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractome- D8 DISCOVER Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Theta/2Theta Height: Radius: Primary radius ....[mm] Secondary radius ....
  • Page 54 D. Factory Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector (SOL‑XE) SOL‑XE User Manual DOC-M88-EXX113 VÅNTEC‑1...

  • Page 55: Part Ii: Angular Accuracy, Instrument Response And Resolution

    Part II: Angular Accuracy, Instrument Response and Resolution Anode: Co Parallel Beam Geometry Angular Accuracy: Difference Deflection angle corr Instrument Resolution Maximum allowed 2θ deviation depends on height FWHM < FWHM 2θ Difference 2θ Difference 2θ FWHM FWHM [°] Deflection Deflection [°] [°]...
  • Page 56 Comments...

  • Page 57: Customer Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in Bragg-Brentano reflection geometry. The factory acceptance test proce- dure consists in full-profile measurements of the certified NIST standard reference material SRM1976c.
  • Page 58 E. Customer Acceptance Test Protocol Comments 58 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 59: Part I: Instrument Details (D8 Series)

    E. Customer Acceptance Test Protocol Part I: Instrument Details (D8 Series) Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractome- D8 ADVANCE Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes)
  • Page 60 E. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector (SOL‑XE) SOL‑XE User Manual DOC-M88-EXX113 VÅNTEC‑1...
  • Page 61 E. Customer Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractometer D8 DISCOVER Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV /  30 mA (for FF tubes) TXS Power: 50 kV / 100 mA (for 0.3x3 mm filament, line and spot focus) TXS Power: 50 kV / 22 mA (for 0.1x1 mm filament, spot focus) Vertical...
  • Page 62 E. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Slits Fixed divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Fixed antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Variable divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Variable antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Motorized air scatter screen Automatic mode Primary axial Soller slit...
  • Page 63 E. Customer Acceptance Test Protocol Instrument Configuration D8 ENDEAVOR Instrument Details Set Values for Validation Diffractometer D8 ENDEAVOR Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer Height: Radius: 200,5 Rotating...
  • Page 64 E. Customer Acceptance Test Protocol Comments 64 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 65: Part Ii: Angular Accuracy, Instrument Response And Resolution (D8 Series)

    Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series) Anode: Cu Bragg-Brentano Geometry Angular Accuracy: Difference Reference Position corr Instrument Response: I Instrument Resolution Maximum allowed 2θ deviation depends on height Maximum allowed intensity deviation for point detectors ± 10% FWHM <...
  • Page 66 Comments...

  • Page 67: Customer Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in Bragg-Brentano reflection geometry. The factory acceptance test proce- dure consists in full-profile measurements of the certified NIST standard reference material SRM1976c.
  • Page 68 F. Customer Acceptance Test Protocol Comments 68 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 69: Part I: Instrument Details (D8 Series)

    F. Customer Acceptance Test Protocol Part I: Instrument Details (D8 Series) Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV / 30 mA (for FF tubes)
  • Page 70 F. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector SOL‑XE User Manual DOC-M88-EXX113 (SOL‑XE)
  • Page 71 F. Customer Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractometer D8 DISCOVER Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Theta/2Theta Height: Radius: Primary radius ....[mm] Secondary radius ....[mm] Horizontal...
  • Page 72 F. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Slits Fixed divergence Divergence slit: 0.3° (approx. 0.6 mm) Fixed antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Variable divergence slit Divergence slit: 0.3° (approx. 0.6 mm) Variable antiscatter slit Antiscatter slit: 0.3° (approx. 0.6 mm) Motorized air scatter screen Automatic mode Primary axial Soller slit...
  • Page 73 F. Customer Acceptance Test Protocol Instrument Configuration D8 ENDEAVOR Instrument Details Set Values for Validation Diffractometer D8 ENDEAVOR Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Height: Radius: 200,5 Rotating Sample position A1 Monochroma- Kβ-Filter tisation...
  • Page 74 F. Customer Acceptance Test Protocol Comments 74 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 75: Part Ii: Angular Accuracy, Instrument Response And Resolution (D8 Series)

    Part II: Angular Accuracy, Instrument Response and Resolution (D8 Series) Anode: Co Bragg-Brentano Geometry Angular Accuracy: Difference Reference Position corr Instrument Resolution Maximum allowed 2θ deviation depends on height FWHM < FWHM 2θ Difference 2θ Difference 2θ FWHM FWHM [°]...
  • Page 76 Comments...

  • Page 77: Customer Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in parallel beam reflection geometry (Göbel mirror systems). The factory ac- ceptance test procedure consists in full-profile measurements of the certified NIST standard reference material NIST SRM1976c .
  • Page 78 G. Customer Acceptance Test Protocol Comments 78 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 79: Part I: Instrument Details

    G. Customer Acceptance Test Protocol Part I: Instrument Details Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer...
  • Page 80 G. Customer Acceptance Test Protocol Instrument Details Set Values for Validation EIGER2 R 500K EIGER2 R 500K User Manual DOC-M88-EXX293 including D8 ADVANCE ECO 40 kV / 25 mA in case of D8 ADVANCE ECO Comments 80 / 96 DOC-M88-EXX157_V17_04.2019...
  • Page 81 G. Customer Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractome- D8 DISCOVER Tube Power: 40 kV / 40 mA (for FL tubes) Tube Power: 40 kV /  30 mA (for FF tubes) TXS Power: 50 kV / 100 mA (for 0.3x3 mm filament, line and spot focus) TXS Power: 50 kV / 22 mA (for 0.1x1 mm filament, spot focus) Vertical...
  • Page 82 G. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter (See User LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 Manuals) LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector (SOL‑XE) SOL‑XE User Manual DOC-M88-EXX113 VÅNTEC‑1...

  • Page 83: Part Ii: Angular Accuracy, Instrument Response And Resolution

    Part II: Angular Accuracy, Instrument Response and Resolution Anode: Cu Parallel Beam Geometry Angular Accuracy: Difference Deflection angle corr Instrument Response: I Instrument Resolution Maximum allowed 2θ deviation depends on height Maximum allowed intensity deviation for point detectors ± 10% FWHM <...
  • Page 84 Comments...

  • Page 85: Customer Acceptance Test Protocol

    Serial Number: SAP Number (Sales Order Number): This protocol details the results of the factory acceptance test procedure for Bruker AXS dif- fraction systems in parallel beam reflection geometry (Göbel mirror systems). The factory ac- ceptance test procedure consists in full-profile measurements of the certified NIST standard reference material NIST SRM1976c .
  • Page 86 H. Customer Acceptance Test Protocol Comments 86 / 96 DOC-M88-EXX157_V17_04.2019...

  • Page 87: Part I: Instrument Details

    H. Customer Acceptance Test Protocol Part I: Instrument Details Instrument Configuration D8 ADVANCE Instrument Details Set Values for Validation Diffractometer D8 ADVANCE Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV / 30 mA (for FF tubes) Vertical Theta/Theta goniometer...
  • Page 88 H. Customer Acceptance Test Protocol Instrument Details Set Values for Validation VÅNTEC‑1 VÅNTEC‑1 User Manual DOC-M88-EXX072 EIGER2 R 500K EIGER2 R 500K User Manual DOC-M88-EXX293 1) including D8 ADVANCE ECO 2) 35 kV / 28 mA in case of D8 ADVANCE ECO Comments 88 / 96 DOC-M88-EXX157_V17_04.2019...
  • Page 89 H. Customer Acceptance Test Protocol Instrument Configuration D8 DISCOVER Instrument Details Set Values for Validation Diffractome- D8 DISCOVER Tube Power: 35 kV / 40 mA (for FL tubes) Tube Power: 35 kV /  30 mA (for FF tubes) Vertical Theta/Theta goniometer Theta/2Theta Height: Radius: Primary radius ....[mm] Secondary radius ....
  • Page 90 H. Customer Acceptance Test Protocol Instrument Details Set Values for Validation Detector Scintillation counter LYNXEYE, SSD160 LYNXEYE User Manual DOC-M88-EXX095 LYNXEYE XE LYNXEYE XE User Manual DOC-M88-EXX240 LYNXEYE XE‑T LYNXEYE XE‑T User ManualDOC-M88-EXX239 LYNXEYE‑2 LYNXEYE‑2 User Manual DOC-M88-EXX305 SSD160-2 SSD160-2 User Manual DOC-M88-EXX306 Solid state detector (SOL‑XE) SOL‑XE User Manual DOC-M88-EXX113 VÅNTEC‑1...

  • Page 91: Part Ii: Angular Accuracy, Instrument Response And Resolution

    Part II: Angular Accuracy, Instrument Response and Resolution Anode: Co Parallel Beam Geometry Angular Accuracy: Difference Deflection angle corr Instrument Resolution Maximum allowed 2θ deviation depends on height FWHM < FWHM 2θ Difference 2θ Difference 2θ FWHM FWHM [°] Deflection Deflection [°] [°]...
  • Page 92 Comments...

  • Page 93: Daily Check Protocol

    I. Daily Check Protocol I. Daily Check Protocol System No.: Sample: Anode: Reflection (hkl): 2θ : Maximum allowed FWHM : Maximum allowed 2θ deviation: ± 0.01° FWHM (< FWHM Date Line Line Intensity Line Shape Pass / Fail Operator Signature Postion DOC-M88-EXX157_V17_04.2019 93 / 96...
  • Page 94 I. Daily Check Protocol Date Line Line Intensity Line Shape Pass / Fail Operator Signature Postion 94 / 96 DOC-M88-EXX157_V17_04.2019...
  • Page 95 DOC-M88-EXX157_V17_04.2019 95 / 96...
  • Page 96 ● Bruker Corporation info.baxs@bruker.com www.bruker.com Order No: DOC-M88-EXX157 V17 - 04.2019...

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