Related Manuals for Ametek TRACE ANALYTICAL ta5000R
Summary of Contents for Ametek TRACE ANALYTICAL ta5000R
- Page 1 TRACE ANALYTICAL MODEL ta5000R User Manual Process Instruments Western Research 455 Corporate Boulevard Newark, DE 19702 PN: T900-017 Rev. A...
- Page 2 If the instrument or procedures are used for purposes over and above the ca- pabilities specified herein, confirmation of their validity and suitability should be obtained; otherwise, AMETEK does not guarantee results and assumes no obligation or liability.
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Page 3: Table Of Contents
Contents About This Document ..................5 Safety Notes ......................5 Grounding ......................6 Important Safety Information ................6 Warning Labels ...................... 7 Electromatic Compatibility (EMC) ..............8 General Safety Considerations ................9 Electric Hazard ..................9 UV Light ....................9 Mercury Vapor .................. - Page 4 Connect AC Power and Communication Cables ........... 30 Start Up and Operation 31 Power Up ....................31 Using the Menu Keys ..................32 Operator state diagram ..................33 Warm Up....................... 33 Main Menu Screens .................... 35 Page Screens ......................36 Systems Settings Page ..................
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Page 5: About This Document
About This Document This manual is intended as a guide for operation of the ta5000R. This manual is notintended as a service guide and does not contain service information. The ta5000R should only be operated by personnel who have been properly trained in the procedures required for safe operation of the ta5000R. -
Page 6: Grounding
Grounding Instrument grounding is mandatory. Performance specifications and safety protection are void if instrument is operated from an improp- erly grounded power source. WARNING Verify ground continuity of all equipment before applying power. Important Safety Information Before working on the ta5000R, read and understand the following Notes, Warnings, and Cautions, regarding safety and other required information. -
Page 7: Warning Labels
Achtung - Heiße Oberfläche Environmental Information (WEEE) This AMETEK product contains materials that can be reclaimed and recycled. In some cases the product may contain materials known to be hazardous to the environment or human health. In order to prevent the release of harmful substances into the environment and to conserve our natural resources, AMETEK recommends that you arrange to recycle this product when it reaches its “end of life.”... -
Page 8: Electromatic Compatibility (Emc)
Electromagnetic Compatibility (EMC) Read and follow the recommendations in this section to avoid perfor- mance variations or damage to the internal circuits of this equipment when installed in harsh electrical environments. CAUTION The various confi gurations of the Heater should not produce, or fall victim to, electromag- netic disturbances as specifi... -
Page 9: General Safety Considerations
General Safety Considerations Components and Functions The following safety items must be observed to avoid personal injury and to prevent damage to the RGD analyzer. All personnel involved in instal- lation, operation or service of the analyzer should be thoroughly familiar with these items. -
Page 10: Warranty And Claims
(90) days from date of shipment. Resale items warranty is limited to the transferable portion of the original equipment manufacturer’s warranty to AMETEK. If you are returning equipment from outside the United State, a statement should appear on the documentation ac- companying the equipment being returned declaring that the goods being returned for repair are American goods, the name of the firm who purchased the goods, and the shipment date. -
Page 11: Overview
The system consists of a microprocessor controlled gas chro- matograph utilizing the Unique Reduction Gas Detector (RGD) designed by Ametek’s Trace Analytical. Functional Overview In order to achieve specified performance, the ta5000R performs these... -
Page 12: Reduction Gas Detection
Reduction Gas Detection Species eluting from the RGD column set pass immediately into the heated bed of mercuric oxide (HgO) and the photometric detector. Within the HgO bed, the general reaction occurs: X + HgO (solid) => XO + Hg (vapor) where X is any appropriate reducing gas. - Page 13 Data is presented via the front display panel. Alternatively data may be obtained through an RS232 serial computer interface and HP parallel printer interface located on the rear panel. With optional interface kits, two components may be assigned to separate trend channels to provide a continuous signal proportional to the con- centration of the assigned component.
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Page 15: Specifications
SPECIFICATIONS Model designation and detection limit specifications Lower detection limits may vary depending on application, contact manufacturer for information about your specific model or applica- tion. Not all models and applications are listed below. CAUTION Sample Gas Model Lower Detection Limit H2 ppb CO ppb Nitrogen... -
Page 16: Sample Gas Supplies
Sample Compatibility Specific models available for various applications Resolution, Display 0.1 ppb Resolution, Communication Ports 0.01 ppb Carrier Gas Supplies (On -Line Installation) Inlet Pressure Range 70 to 90 psig (4.8 to 6.1 bar) Inlet Pressure Stability ± 2%, regulator required Return Pressure Atmospheric vent is optimal, ±... -
Page 17: Gases
Sample Gas Inlet Fitting 1/16-inch VICI compression fitting Flow Rate 20 - 100 sccm minimum Inlet pressure stability ± 2%, UHP regulator required Vent pressure Atmospheric pressure vent is optimal, ± 0.5 psig maximum Actuator Gas Inlet Fitting 1/16-inch VICI compression fitting (Uses Sample Inlet) Inlet Pressure Range 70 to 150 psig (4.8 to 10.2 bar) -
Page 18: Outputs
Outputs Display LCD graphics, backlit, 100mm x 150mm Printer Port Concentration, chromatogram, and diagnos -tic reports Serial PLC Port Concentration data and general alarm via RS232 4 to 20ma (optional) Concentration signals ta5000 PLC Output Format The concentration data, status, and other detail information is sent from port 2 of the ta5000 automatically at the end of every run. -
Page 19: Com Ports
The following defi nes each fi eld: DDDD-DD-DD TT:TT:TT,#,R,S,A,EEEEEEEE,NNNNN,C, … DDDD-DD-DD = Date (2000-03-23) TT:TT:TT = Time (12:23:44) = Analyzer Serial Number = Run or Maintenance (Calibration) Mode = EDL or Single Analysis Mode = Stream Number EEEEEEEE = Eight digits of error status (0 = Not Error, 1 = Er- ror) General Alarm (MSD) Spare... -
Page 20: Paralle Printer Ports(Lpti)
The Parallel Printer Port uses a standard 25-pin female D-type connector. The printer port follows standard parallel printer protocols. The analyz- ers are compatable with Hewlett Packard printers model numbers HP-6xx, HP-7xx, and HP-8xx. Ametek’s Trace Analytical recommends using one of these suggested models. Parallel Printer Port LPT1... -
Page 21: Analyzer Description
ANALYZER DESCRIPTION Front Panel and User Interface The front panel of the ta5000R is where the user interface is found. The user interface is a combinationof the display screen and menu keys. The display screen shows information andoptions for running the ta5000R. The Menu Keys correlate to menu labels on the display screen and are used for all input to the operating system. -
Page 22: Display Screen
Rear Panel Display Screen The display screen is where the instrument displays all current informa- tion and options.The display is separated into three sections. The top section of the screen is the Status Bar. This is where the instru- ment displaysthe current status. This bar will also display which screen is currently selected, the time and date and other important Status informa- tion. - Page 23 Display screen User Manual | 23...
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Page 24: Installation
• Operating Manual • Accessories purchased with the ta5000R If any evidence of damage exists, immediately contact the shipping com- pany, save the original shipping container, and notify Ametek as soon as possible for consultation. Location and Environment 1. The area where the ta5000R Gas Analyzer is to be operated should be clean with minimum particulate matter and dust in the air. -
Page 25: Electrical Preparations And Connections
2. Support gases for the instrument should be located near the analyzer. A uniform temperature environment for cylinders and regulators is es- sential in order to keep constant pressure and flow rate. Always keep gas containers inside the building where temperature fluctuations are at a minimum. -
Page 26: Regulators And Plumbing
Use Cajon VCR fittings with gaskets to connect to UHP regulators. Do not use pipe thread fittings since they are not clean and are not CAUTION leak-tight for Ametek’s trace gas analysis. Suggested Hardware for Gas Connections UHP Regulators for Carrier and Sample Gases Dual stage stainless steel, 0 to 150 psig outlet with gauges and 1/16-inch VICI female fittings. -
Page 27: Damage Prevention
Tubing, 1/16-inch OD x 0.03-inch ID, Stainless Steel 4 each approximately 72” lengths for gas supply umbilical. Tubing, 1/8-inch OD, for pneumatic (Actuator gas) line 1 each approximately 72” length for gas supply umbilical. Guidelines for prevention of damage PLEASE STUDY THIS MANUAL THOROUGHLY BEFORE IN- STALLING OR OPERATING THE INSTRUMENT. -
Page 28: Installation Instructions
CAUTION If any inconsistencies are encountered during installation, stop im- mediately. do not continue the installation without direction from Ametek customer service. CAUTION Tools Suggested for Installation All connections are made using U.S. standard size conectors. -
Page 29: View Of Gas And Power Connections
Connect Sample Gas - without Front Injection Panel option The ta5000 analyzer can be used for process or single gas sample analysis. On-line process sample line should be connected to the “SAMPLE IN” 1/16 “ VICI fitting on the rear panel. Optimal results are achieved with constant flow rates (20-100 sccm). -
Page 30: Connect Ac Power And Communication Cables
Connecting AC Power and Communications Cables IMPORTANT: Verify that the operating voltage of the instrument matches the available AC power. The analyzer does not auto select for CAUTION varying power line voltages. Correct instrument operating voltage is labeled on the rear panel directly above the DIN connector / power switch. -
Page 31: Start Up And Operation
If any of these does not oc- cur, turn the power off immediately and contact Ametek service or your local authorized service agent. -
Page 32: Using The Menu Keys
Using the Menu Keys The analyzer displays a set of labels across the bottom of the display screen. The set is called a menu because it presents the user with choices. Each choice on the menu will either lead to another menu or will perform a function. -
Page 33: Operator State Diagram
Menus Operator State Diagram Power-up Warmup Warmup Edit Edit Edit System Temperatures Aux Box Page Warm-up Page Page and Status Settings Settings Cool Optional Aux Box Installed? Page Return to Source Calibration Page Idle Settings Page Edit Blank Calib State Diagram for Normal User Mode. This chart illustrates how the menus are arranged in Normal User Mode. - Page 34 After pressing Warmup the instrument will perform a series of system tests and will begin heating critical zones. The results from these tests will appear on the Warm-up screen. The Warmup menu item will also change to Cool. If you wish to stop the Warm-up process, press the Cool key and the instrument will start to cool down.
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Page 35: Main Menu Screens
Main Menu After warm-up has completed successfully the main menu will be dis- played. The main menu is a set of primary choices leading to other menu options. The following table shows the choices available from the main menu. 12:34:25 Idle Mode CO = Page... -
Page 36: Page Screens
Page Screens Each time Page is pressed another user setup screen will be displayed. The following table shows a summary of information available from each page. If a page allows input, the cursor will be displayed and arrow keys will be available as menu items. Some fields have a selection of pre-programmed settings that the user can select. -
Page 37: Systems Settings Page
System Settings Page The first Page Screen is for general configuration settings. The following list shows the function of each option for this screen Idle Mode 12:34:25 System Settings Ver. 2.70 Clock: 10-Jan-03 12:34:25 Print Chromatograms: -------------------- System Errors -------------------- Edit Print Page... -
Page 38: Diagnostic Print Key
Diagnostic Print Key The Print key appears when setting the clock. Pressing the Print key from this page will print a complete report of all system settings, calibration settings, temperatures and status and the chromatogram from the last run of the analyzer. This is a system diagnostic tool which can be used to troubleshoot problems with the analyzer. -
Page 39: Calibration
Calibration Screen Pressing page again will exit the page screens. It is recommended to use the Ametek’s Trace Analytical MGB1000 Micro Gas Blender to blend the calibration gas to the desired level when calibrating the ta5000R User Manual | 39... -
Page 40: Run Screen
From the Run Screen press Run and automatic operation of the analyzer will begin. The ta5000R will display the time left, in seconds, for the cur- rent cycle in the status window. The results will be updated in the screen as the concentration is determined. -
Page 41: Super User Mode
How to enter Super User mode Please contact Ametek Service about entering the Super User Mode. Once you have accessed this mode, you will see the Super User mode name appear in the left corner of the screen. If “Normal User” appears in the left corner you were already in Super User. -
Page 42: Temperature And Status Page
Super User Temperature & Status Page Depressing the “Zero” key will manually zero the detector. Depressing the “Lamp” key will toggle the lamp on and off. Depressing the “Edit” key will provide a new menu of options above the keys to: 1. -
Page 43: System Settings
2. With the asterisk on the top line, one can toggle between single, cycle and rerun as analysis options. Single will run one event if the “Run” key is depressed. Cycle will continuously run the loaded event program until IDLE is depressed. Pressing IDLE in Super User Mode will immediately stop the cycle. -
Page 44: Operator State Diagram
State Diagram for Super User Mode This chart illustrates how the menus are arranged in Super User Mode. Each large circle represents a screen that is displayed on the instrument. The names printed above each arrow represent a menu label and menu key. -
Page 45: Description Of Internal Components
DESCRIPTION OF INTERNAL COMPONENTS Front Panel Main Processor Display Module Chassis Controller Chrom Detector Module Controller Photometer Power Supply Mercury Bed Module Mercury Scrubber Rear Panel User Manual | 45... -
Page 46: Error Messages
ERROR MESSAGES Error Messages Error Messages are viewed and acknowledged on the System Settings screen. When the Status LED on the front panel is red this indicates that there are system errors or the status of the analyzer has changed. The System Status page displays error messages that the system has encoun- tered. - Page 47 Analog Signal Zeroing Error The instrument has failed to zero the detectors analog signal. Vsig Minimum Voltage Limit This fault will occur if the RGD detector does not have the minimum Vsig (1000mv) for proper analysis. Typical Values are 1750-2250. Vsig cannot be above 2500.
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Page 48: Dimensional Drawings
Dimensional Drawings ta5oooR 3-D View 48 | Model ta5000R Gas Purity Monitor... - Page 49 ta5oooR Side View User Manual | 49...
- Page 50 ta5oooR Top View 50 | Model ta5000R Gas Purity Monitor...