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TRACE ANALYTICAL
MODEL ta3000F
Gas Purity Monitor
User Manual
Process Instruments
Western Research
455 Corporate Boulevard
Newark, DE 19702
PN T900-015 Rev. A

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Table of Contents
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Summary of Contents for Ametek ta3000F

  • Page 1 TRACE ANALYTICAL MODEL ta3000F Gas Purity Monitor User Manual Process Instruments Western Research 455 Corporate Boulevard Newark, DE 19702 PN T900-015 Rev. A...
  • Page 2 © 2004 AMETEK Process & Analytical Instruments Division This document contains Information for the use of the Model ta3000F Gas Purity Monitor. Data herein has been verified and validated and is believed adequate for the intended use of this instrument. If the instrument or procedures are used for purposes over and above the ca- pabilities specified herein, confirmation of their validity and suitability should be obtained;...
  • Page 3: Table Of Contents

    Contents About This Document ..................5 Safety Notes ......................5 Grounding ......................6 Important Safety Information ................6 Warning Labels ...................... 7 Electromatic Compatibility (EMC) ..............8 General Safety Considerations ................9 Electric Hazard ..................9 UV Light ....................9 Mercury Vapor ..................
  • Page 4 Super User Run Screen ..................41 Super User Menus ....................42 Super User State Diagram .................. 42 Shut Down ......................43 Description of Internal Components 44 Error Messages ..................45 Dimensional Drawings ................ 47 4 | Model ta3000F Gas Purity Monitor...
  • Page 5: About This Document

    About This Document This manual is intended as a guide for operation of the ta3000F. This manual is notintended as a service guide and does not contain service information. The ta3000F should only be operated by personnel who have been properly trained in the procedures required for safe operation of the ta3000F.
  • Page 6: Grounding

    Verify ground continuity of all equipment before applying power. Important Safety Information Before working on the ta3000F, read and understand the following Notes, Warnings, and Cautions, regarding safety and other required information. Additional Notes, Warnings, and Cautions included in individual proce- dures in this manual indicate special conditions to consider during instal- lation, before opening the heater and while working on it.
  • Page 7: Warning Labels

    Achtung - Heiße Oberfläche Environmental Information (WEEE) This AMETEK product contains materials that can be reclaimed and recycled. In some cases the product may contain materials known to be hazardous to the environment or human health. In order to prevent the release of harmful substances into the environment and to conserve our natural resources, AMETEK recommends that you arrange to recycle this product when it reaches its “end of life.”...
  • Page 8: Electromatic Compatibility (Emc)

    Heater or the overall system. Examples of electrical events and devices known for the gen- eration of harmful electromagnetic disturbances include motors, capacitor bank switching, storm related transients, RF welding equipment, static, and walkie-talkies. 8 | Model ta3000F Gas Purity Monitor...
  • Page 9: General Safety Considerations

    Components and Functions The following safety items must be observed to avoid personal injury and to prevent damage to the ta3000F analyzer. All personnel involved in installation, operation or service of the analyzer should be thoroughly familiar with these items. These considerations are in addition to all site specific safety procedures.
  • Page 10: Warranty And Claims

    (90) days from date of shipment. Resale items warranty is limited to the transferable portion of the original equipment manufacturer’s warranty to AMETEK. If you are returning equipment from outside the United State, a statement should appear on the documentation ac- companying the equipment being returned declaring that the goods being returned for repair are American goods, the name of the firm who purchased the goods, and the shipment date.
  • Page 11: Overview

    OVERVIEW Model ta Gas Purity Monitor Introduction The ta3000F Process Gas Analyzer is a trace level gas chromatograph capable of detecting ppb concentrations of contaminants in sample gas matrices. The system consists of a microprocessor controlled gas chro- matograph utilizing the Trace Analytical Flame Ionization Detector (FID).
  • Page 12: Operating System

    External signal outputs for a data collection system or host computer are located at the rear panel. The microprocessor control system allows complete unattended operation of the ta3000F. This onboard system performs necessary operational and analytical functions such as: •...
  • Page 13: Specifications

    Specifications Model designation and detection limit specifications Sample Gas Model Lower Detection Limit CO2 ppb CH4ppb NMHCppb Nitrogen ta3000F-N2 Argon ta3000F-Ar Helium ta3000F-He Oxygen ta3000F-O2 Hydrogen ta3000F-H2 ta3000F Performance Accuracy Greater of +1 x LDL or + 10% of readingg...
  • Page 14: Carrier Gas Supplies

    Inlet pressure stability + 2%, UHP regulator required Vent pressure Atmospheric pressure vent is optimal, + 0.5 psig maximum Fid Hydrogen Inlet Fitting 1/16-inch VICI compression fitting Inlet Pressure Range 30 psig (2.0 bar) 14 | Model ta3000F Gas Purity Monitor...
  • Page 15: Fid Air

    Inlet pressure stability + 2%, UHP regulator Flow rate 30 cc/min Purity Hydrocarbons, CO, C O , Moisture < 1 ppm FID Air Inlet Fitting 1/16-inch VICI compression fitting Inlet pressure range 20 psig (1.4 bar) Inlet pressure stability + 2%, regulator required Flow rate 230 cc/min Purity...
  • Page 16 Spare Spare Spare Spare Spare (LSD) NNNNN = Name of impurity = Concentration in ppb x 100 The following is an example of this output string: 2001-08-16 14:54:13,54,R,S,1,10000000,CH4 ,441,CO2 ,5332,NMHC,172, , , , 16 | Model ta3000F Gas Purity Monitor...
  • Page 17: Com Ports

    Com Ports - COM 1, COM 2, and COM 3 All three of these ports are 9-pin male D-type connectors. Pin 2 is used to transmit data to other equipment. The analyzer uses Pin 3 to receive data. Pin 5 is a common ground. All other pins are unused. COM PORTS User Manual | 17...
  • Page 18 The printer port follows standard parallel printer protocols. The analyz- ers are compatable with Hewlett Packard printer’s model numbers HP- 6xx, HP-7xx, and HP-8xx. Trace Analytical recommends using one of these suggested models. Parallel Printer Port LPT1 18 | Model ta3000F Gas Purity Monitor...
  • Page 19: Analyzer Description

    ANALYZER DESCRIPTION Front Panel and User Interface The front panel of the ta3000F is where the user interface is found. The user interface is a combination of the display screen and menu keys. The display screen shows information and options for running the ta3000F.
  • Page 20 Gas Connections A/C Power Connector Printer Port FID Exhaust FID Shut-Off Communication Ports Rear Panel 20 | Model ta3000F Gas Purity Monitor...
  • Page 21: Display Screen

    Display Screen The display screen is where the instrument displays all current informa- tion and options.The display is separated into three sections. The top section of the screen is the Status Bar. This is where the instru- ment displays the current status. This bar will also display which screen is currently selected, the time and date and other important Status informa- tion.
  • Page 22: Installation

    • Do not discard the shipping container until installation is complete. Upon receipt of the ta3000F analyzer, check the interior of the shipping container for the following items: • ta3000F Analyzer and Power Cord •...
  • Page 23: Electrical Preparations And Connections

    This allows for flexibility when moving or turning the instrument for service and routine maintenance. 7. Situate the ta3000F in such a way that there is always access to the rear panel for easy hook up of the gases, as well as ease of service components.
  • Page 24: Regulators And Plumbing

    UPS will supply power instantly from batteries when the main power is interrupted. Proper power will be supplied for minutes or hours depend- ing upon the size of the battery. Since the ta3000F needs less than 5A of current, the UPS battery pack can be relatively small.
  • Page 25: Damage Prevention

    Guidelines for prevention of damage PLEASE STUDY THIS MANUAL THOROUGHLY BEFORE IN- STALLING OR OPERATING THE INSTRUMENT. CAUTION Carrier gas Detectors can be permanently damaged if operated at temperature with- out flow. The carrier gas should remain flowing until all heated zones are below 50o C (2 to 3 hours).
  • Page 26: Installation Instructions

    The ta3000 analyzer can be used for process or single gas sample analysis. On-line process sample line should be connected to the “SAMPLE IN” 1/16 “ VICI fitting on the rear panel. Optimal results are achieved with constant flow rates (20-100 sccm). 26 | Model ta3000F Gas Purity Monitor...
  • Page 27: View Of Gas And Power Connections

    Connect FID Air FID Air quality can dramatically affect instrument performance. The ta3000F analyzer requires “Purified” dry air for FID oxidizer gas. See gas specifications for FID Air in Section 6.0, Specifications for details. The instrument connection is made at the “FID AIR” 1/16” VICI port on rear panel.
  • Page 28: Connect Ac Power And Communication Cables

    Confirm the instrument power switch is OFF (“O” is Depressed) Connect DIN power cord to instrument Connect DIN power cord to AC voltage source CONNECT COMMUNICATIONS CABLES (if applicable) COM1, COM2, COM3 port, PARALLEL PRINTER port 28 | Model ta3000F Gas Purity Monitor...
  • Page 29: Start Up And Operation

    If any of these does not oc- cur, turn the power off immediately and contact Ametek customer service or your local authorized service agent.
  • Page 30: Using The Menu Keys

    The six keys are called menu keys; the text labels are called menu labels. All operator input to the analyzer occurs through the 6 menu keys. Status Bar Main Window Menu Labels Menu Keys ta3000 Gas Analyzer Status LED Menu Labels 30 | Model ta3000F Gas Purity Monitor...
  • Page 31: Operator State Diagram

    Operator State Diagram Power-up Warmup Warmup Edit Edit System Temperatures Page Warm-up Page Page and Status Settings Cool Page Return to Source Calibration Idle Settings Page Edit Blank Calib State Diagram screenm. This chart illustrates how the menus are arranged. Each large circle rep- resents a screen that is displayed on the instrument.
  • Page 32: Warm Up

    If any errors occur during the warm-up process, proceed to Page 45 to review error messages. Warmup Mode 12:35:25 WARM-UP Module Electronics: Pass Detector System: Detector Temperatures: Carrier Pressure: Cool Page Warmup Mode Screen 32 | Model ta3000F Gas Purity Monitor...
  • Page 33: Main Menu Screens

    The Warm-up process typically takes 20 to 30 minutes. When the warm-up process has completed succesfully a Run munu label will appear. Pressing the Run key will take the user to the main screen where the Main menu will be available.
  • Page 34: Page Screens

    An Edit menu label appears if there are fields that allow the user to enter information Screen What Information is available Page 1 System Settings. Page 2 Temperatures and Status Page 3 Calibration Page Screens 34 | Model ta3000F Gas Purity Monitor...
  • Page 35: Systems Setting Page

    System Settings Page The first Page Screen is for general configuration settings. The following list shows the function of each option for this screen Idle Mode 12:34:25 System Settings Ver. 2.70 Clock: 10-Jan-03 12:34:25 Print Chromatograms: EDL mode: -------------------- System Errors -------------------- Edit Print Page...
  • Page 36: Setting The Clock

    The instrument must be in “Idle” mode to accept the changes. Any change made will be lost if the instrument is turned off before the changes have been accepted on the System Settings page. 36 | Model ta3000F Gas Purity Monitor...
  • Page 37: Saving Changes Non Volatile Ram

    Temperatures and Status Page Press the Page key to display the Temperatures and Status page. This page shows status information about the critical heated zones and status of the detector. No user input is allowed on this page in normal user mode. Idle Mode Temperatures &...
  • Page 38: Run

    From the Run Screen press Run and automatic operation of the analyzer will begin. The ta3000F will display the time left, in seconds, for the cur- rent cycle in the status window. The results will be updated in the screen...
  • Page 39: Run Screens

    How to enter Super User Mode Please contact Ametek Service about entering the Super User Mode. Once you have accessed this mode, you will see the Super User mode name appear in the left corner of the screen. If “Normal User” appears in the left corner you were already in Super User.
  • Page 40: Super User Mode

    Concentration Factor must be 1 for proper operation. Concentration and Response Factor Calculation RF = AREA / CONC GAS_CONC = AREA / RF = Response Factor CONC = Concenration (or blend) of Calibration Gas Cylinder in ppb 40 | Model ta3000F Gas Purity Monitor...
  • Page 41: Super User Run Screen

    Super User Run Screen The run screen in Super User mode is very different than the functionality and appearance of Normal User mode. 1. The top line provides current mode, current viewable time, current at- tenuation, and current time respectively. 2.
  • Page 42: Super User Menus

    Page Idle Idle Calib Single (Return to Source) Cycle Blank ReRun Calib Edit Sequence Blank Calib Zere V1 Load ANAL Event Sequencer Manual V1 Inject V2-CW V2-CCW Edit Edit Edit Operator State Diagram 42 | Model ta3000F Gas Purity Monitor...
  • Page 43: Shut Down

    Shut Down System shut down for maintenance or for any other reason is very sim- ple. If shut down is due to an emergency or for any safety reason, simply switch the instrument off using the A/C DIN Switch located on the rear panel of the analyzer (0 depressed is off).
  • Page 44: Description Of Internal Components

    DESCRIPTION OF INTERNAL COMPONENTS Front Panel Main Processor Display Module Chassis Controller Electrometer Chrom Detector Module Controller Power Supply Module Rear Panel Front and Rear Panels 44 | Model ta3000F Gas Purity Monitor...
  • Page 45: Error Messages

    ERROR MESSAGES Error Messages Error Messages are viewed and acknowledged on the System Settings screen. When the Status LED on the front panel is red this indicates that there are system errors or the status of the analyzer has changed. The System Status page displays error messages that the system has encoun- tered.
  • Page 46 The most common system paramaters that are changed are the response factor due to performing a calibration run. This fault can only be updated during warmup or Idle. (See Saving Changes into Non-Volatile RAM in the Run Section of this manual, page 36). 46 | Model ta3000F Gas Purity Monitor...
  • Page 47: Dimensional Drawings

    DIMENSIONAL DRAWINGS Outer Dimensions - 3D View User Manual | 47...
  • Page 48 Side View 48 | Model ta3000F Gas Purity Monitor...
  • Page 49 ta3oooF Top View User Manual | 49...
  • Page 50 This Page intentionally left blank 50 | Model ta3000F Gas Purity Monitor...

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