Page 1 Bruker BioSpin SampleXpress Sample Changer User Manual Version NMR Spectroscopy think forward...
Page 2 © July 15, 2010: Bruker Biospin GmbH Rheinstetten, Germany P/N: Z31900 DWG-Nr.: Z4D11037 For further technical assistance on the SampleXpress unit, please do not hesitate to contact your nearest BRUKER dealer or contact us directly at: BRUKER BioSpin GMBH am Silberstreifen D-76287 Rheinstetten...
Page 3: Table Of Contents
Table of Contents Contents About ......................7 This Manual......................7 Policy Statement ...................... 7 Symbols and Conventions..................7 Introduction....................9 Concept ........................9 Limitation of Liability ....................10 Copyright ........................ 10 Warranty Terms...................... 10 Customer Service....................10 EC Declaration of Conformity................. 11 EG-Konformitätserklärung..................
Page 4 Table of Contents Sample Usage ......................34 Design and Function ...................35 Overview......................... 35 Brief Description ..................... 36 Unit Description ...................... 37 5.3.1 Base Unit ........................ 37 5.3.2 Cassette ......................... 42 5.3.3 Control Panel......................43 Connections......................44 Indicator Lamp......................46 Work and Danger Zones ..................47 Accessories ......................
Page 5 Device Report File....................99 10.8 Cleaning ....................... 101 10.8.1 Before Cleaning....................101 10.8.2 Cleaning the Outside of the SampleXpress Chassis and Units ......102 10.8.3 Cleaning the Outer Shell of the Device ..............102 10.8.4 Cleaning the Magazine Light Barrier ..............102 10.8.5 Cleaning the Cassette ..................
Page 6 Table of Contents 12.1 List of Error Codes....................111 Dismantling and Disposal.................117 13.1 Safety ........................117 13.2 Dismantling......................118 13.3 Disposal........................ 118 Contact .......................121 Appendix A ......................123 Safety Notices ...................... 123 Avertissements De Sécurité ................. 133 Sicherheitshinweise....................145 Appendix B ......................157 Repair Declaration....................
Page 7: About
Illustrations in this manual are intended to facilitate basic understanding, and may differ from the actual design. This SampleXpress user manual must be kept with the device. In addition to the Sam- pleXpress user manual, instructions concerning labor protection laws, operator regula- tions tools and supplies must be available and adhered to.
Page 8: Caution
About WARNING This combination of symbol and signal word indicates a potentially hazardous situa- tion which could result in death or serious injury unless avoided. CAUTION This combination of symbol and signal word indicates a possibly hazardous situation which could result in minor or slight injury unless avoided. NOTICE This combination of symbol and signal word indicates a possibly hazardous situation which could result in damage to property or the environment unless avoided.
Page 9: Introduction
Introduction The new Bruker sample changer SampleXpress allows automatic measurement of NMR samples with Bruker NMR spectrometers. It is the successor of the B-ACS sample changer system. Its compact, exceptionally integrated design, drastically reduces sam- ple transfer distances, delivering exchange times of just a few seconds, making Sam- pleXpress ideal for optimizing throughput in standard NMR service laboratories running 30-200 samples per day.
Page 10: Limitation Of Liability
Introduction Limitation of Liability All specifications and instructions in this manual have been compiled taking account of applicable standards and regulations, the current state of technology and the experience and insights we have gained over the years. The manufacturer accepts no liability for damage due to: •...
Page 11: Ec Declaration Of Conformity
Introduction EC Declaration of Conformity Z31900_00_01...
Page 12: Eg-Konformitätserklärung
Introduction EG-Konformitätserklärung Z31900_00_01...
Page 13: Safety
The device has been designed and constructed solely for the intended use described here. The SampleXpress must only be used for keeping NMR samples in a cassette module, inserting them into the NMR spectroscopy magnet and ejecting them after measurement back into the magazine.
Page 14 • All personnel who work with, or in the close proximity of the SampleXpress device, need to be informed of all safety issues and emergency procedures as outlined in this user manual.
Page 15: Personnel Requirements
Personnel Requirements 3.3.1 Qualifications Note: Only trained Bruker personnel are allowed to mount, retrofit, repair, adjust and dis- mantle the unit! This manual specifies the personnel qualifications required for the different areas of work, listed below: Laboratory Personnel...
Page 16: Unauthorized Persons
Safety 3.3.2 Unauthorized Persons WARNING Risk to life for unauthorized personnel due to hazards in the danger and working zone! Unauthorized personnel who do not meet the requirements described in this manual will not be familiar with the dangers in the working zone. Therefore, unauthorized per- sons face the risk of serious injury or death.
Page 17: Basic Dangers
Safety Basic Dangers The following section specifies residual risks which may result from using the device and have been established by means of a risk assessment. In order to minimize health hazards and avoid dangerous situations, follow the safety instructions specified here as well as in the following chapters of this manual. 3.5.1 Position of the Safety Devices EMERGENCY STOP Button...
Page 18: General Workplace Dangers
Working in Heights CAUTION Accident hazard from falling from ladder! It is possible to fall from a ladder when it is used to reach the SampleXpress on some magnets. Do not use a ladder. Use an approved platform to reach the device on the magnet.
Page 19: Dangers From Electric Power
NOTICE Material damage hazard due to impacting the magnet! Impacting the magnet may result in a quench. Mount the SampleXpress carefully on the magnet. Avoid banging the magnet during installation and operation, e.g. when replacing the sample cassette. Genuine Samples...
Page 20: Danger To Life From Residual Electrostatic Potentials
Safety Electric Current WARNING Electrical hazard from electrical shock! A life threatening shock may result when the housing is open during operation. Disconnect the device from the electrical power supply before opening the device. Use a voltmeter to verify that the device is not under power! Be sure that the power supply cannot be reconnected without notice.
Page 21: Mechanical Dangers
CAUTION Accident hazard from movement of mechanical parts! The fingers or hand may be pinched due to movement of mechanical parts. Shut off the SampleXpress before accessing the device. Falling Objects CAUTION Accident and material damage hazard from falling objects! Equipment may fall down during assembly, retrofitting, or dismantling.
Page 22: Dangers From Gases Under Pressure
A break in the pneumatic hose may result in the uncontrolled exit of nitrogen into the laboratory. An oxygen warning device should be present in the laboratory if the device is operated with nitrogen. Note that leakage from the main supply line cannot be stopped by the SampleXpress! Z31900_00_01...
Page 23: Dangers From Radiation
Keep storage media, credit cards etc. away from the magnetic source. Data could be erased. Note: The magnetic field of the SampleXpress does not cause any personal injuries or property damage. For further information see the manual of the magnet used.
Page 24: Dangers Due To High Or Low Temperatures
Material damage may result from the overflow of cryogens. Turn off the SampleXpress during magnet servicing. Cover the SampleXpress with a protective cover to avoid contact with cold gases. Be sure to use sufficient transfer line and Teflon evacuation hose for nitrogen and helium refills based on recommendations in the magnet manual.
Page 25: Danger From Chemical Substances
Safety 3.5.9 Danger from Chemical Substances Glass Tube Breakage DANGER Danger of injury from glass tube breakage! Broken glass tubes may cause minor injuries or material damage, but may also result in a life threatening situation if hazardous substances are used. If a glass tube breaks, refer to the corresponding precautions and cleaning/disin- fection instructions.
Page 26: Material Damage Hazard From Heavy Samples
Material damage may result when the device comes in contact with NMR solvents. Follow instructions provided in the manual for correct handling of solvents. Follow the sensor cleaning procedures described in this manual. If surface damage should occur, contact Bruker for repair of damaged parts. NOTICE Material damage hazard from heavy samples! Samples may be damaged due to incorrect sample lift pressure adjustment.
Page 27: Environmental Protection
Safety Protective Earth Conductor WARNING Danger to life from contact voltage! Absent or faulty protective earth conductor may result in contact voltage. This may pose a risk of injury or death. Before the initial commissioning of the appliance, connect the main power supply to the socket and verify the complete functionality of the protective earth conduc- tor.
Page 28: Signage
Safety The following pollutants are used: Helium inert gas Helium inert gas may cause suffocation at high concentra- tions. Disposal of the empty gas cylinders must be performed by a specialized disposal company. Nitrogen gas Nitrogen gas may cause suffocation at high concentrations. Disposal of the empty gas cylinders must be performed by a specialized disposal company.
Page 29 Safety Danger Spot Warning indicating a danger spot in work rooms. Hand Injury Keep hands away from areas bearing this warning sign. There is a danger that hands could be crushed, drawn in or other- wise injured. Maximum Sample Height There is a danger that the sample breaks, if the sample exceeds the maximum sample height.
Page 30: Spare Parts
Safety Spare Parts NOTICE Material damage hazard from glass tube breakage or sample blockage in the BST. Material damage from glass breakage or samples becoming stuck in the BST may result if non-OEM replacement parts are used. Replacement parts must meet OEM standards. Loss of Guarantee If non-approved spare parts are used the manufacturer's guarantee is invalidated.
Page 31: Technical Data
Technical Data General Information Data Value Unit Weight without cassette Weight with 60s cassette (without any sample) Length Width Height Table 4.1 Technical Data: General Information Connection Values Electrical Data Value Unit Voltage 208 - 230 Apparent power consumption, maximum Circuit protection 2 x 1.0 Slow Blow...
Page 32: Operating Conditions
Decreasing linear till relative humidity < 50% at 40 < 50 °C, maximum Table 4.4 Operating Environment For the appropriate temperature see also the Bruker site planning guides on the BASH CD (Bruker Advanced Service Handbook): Manual Bruker Part Number...
Page 33: Rating Plate
Technical Data Rating Plate Figure 4.1 Rating Plate The rating plate is located at the power input and includes the following information: • Manufacturer • Type • Voltage • Frequency • Apparent power consumption, maximum • Year of Production • PN: Part Number •...
Page 34: Sample Usage
Technical Data Sample Usage SampleXpress can handle any type of sample with standard spinner geometry: • Standard NMR tubes (3-10 mm). • Melted reference samples. • Match spinner (1, 1.7, 2, 2.5, 3, 4, 4.25, 5 mm). • Shuttle POM for sample tubes 1-1.7 mm.
Page 35: Design And Function
Design and Function Overview Status Light Base Unit NMR Access Position Cassette Guide Emergency Stop Touch Panel Control Panel Magnet Base Plate Figure 5.1 Overview Z31900_00_01...
Page 36: Brief Description
The samples are inserted into the magnet by the SampleXpress, and are stored in a removable cassette. Thereby it is possible to remove the cassette for filling/removing samples. The cassette has a capacity of 60 samples.
Page 37: Unit Description
Design and Function Unit Description 5.3.1 Base Unit Figure 5.3 Base Unit Mounted on Base Plate The base unit contains all of the actuators and most of the sensors. It is placed on top of the base plate and fixed with 4 screws on the bottom side, and 2 screws on the top side of the base plate.
Page 38: Figure 5.4 Clamp Closed
Design and Function Conveyor Chain Motor The SampleXpress uses an electric DC motor to drive the sample conveyor chain in the cassette. To minimize the influence on the NMR measurement, this motor is mounted with special vibration damping parts. As an option for very strong magnetic fields, the motor can be placed outside the 5 Gauss line.
Page 39: Figure 5.6 Sample Guide
Design and Function Sample Guide The sample guide serves to guide the samples into the magnet. As the samples drop down from the cassette into the mag- net, they have to be safely led into the proper position. The sample guide is driven by a pneu- matic cylinder placed in the base unit.
Page 40: Figure 5.8 Sample Guide
Design and Function Guide inactivated Guide activated Figure 5.8 Sample Guide Another function of the sample guide is to mechanically lock the conveyor chain. When a conveyor chain link is positioned in proximity of the NMR access position above the BST, the chain link contains a lot of deliberate play which makes it easier for the unit to align on the correct position.
Page 41: Figure 5.10 Base Unit
Design and Function Sample Release Lever Sample Release Lever Figure 5.10 Base Unit Each conveyor chain link has its own sample release lever (Figure 5.11/1) to hold the sample in place. This lever is pressed to its home position by a spring which is placed inside each conveyor chain link.
Page 42: Cassette
Design and Function Sample Brake The sample brake slows down the sample on its way back from the BST tube. Figure 5.12 Sample Brake 5.3.2 Cassette The removable cassette has a capacity of 60 samples, which can be filled individually, or can be removed from the base unit and all the conveyor chain links can be filled at once.
Page 43: Control Panel
Design and Function 5.3.3 Control Panel The control panel is the central operating control for the device. It is mounted on a swivel arm on the front side of the device. The control panel is equipped with a touch screen, which controls the application software.
Page 44: Connections
Design and Function Connections BST Interface Cable from SLCB BSMS BST Interface Cable to BST Gas Interrupt (future feature) Lift Adjustment Knob Status and Control Pressure Gauge Air Supply Adjustment Knob Air Supply External R232 (future feature) 10. Console RS232 11.
Page 45: Figure 5.15 Connections Right Side
Design and Function Power Control from Control Panel Fuse Cartridge DC In (future feature) Power Supply Figure 5.15 Connections Right Side Z31900_00_01...
Page 46: Indicator Lamp
Design and Function Indicator Lamp Indicator Lamp The indicator lamp indicates the various operating status using different colored light sig- nals. Figure 5.16 Indicator Lamps Pos. Light Signal Description Fault event (red) The red indicator lamp is illuminated when an internal error occurs.
Page 47: Work And Danger Zones
Design and Function Work and Danger Zones NMR Access Position The arrow indicates the danger zone. When no cassette is present it is pos- sible that the device operator may be caught in the gripper claws. Figure 5.17 NMR Access Position Z31900_00_01...
Page 48: Figure 5.18 Cassette And Control Panel
Cassette and Control Panel The arrow indicates the danger zones. It may be possible that the device oper- ators bang their heads against the SampleXpress, due to the height of the control panel or the cassette. Figure 5.18 Cassette and Control Panel...
Page 49: Accessories
Part Number Stair with 2 steps Z106255 Stair with 4 steps Z106254 Cover During magnet maintenance it is recommended to cover the SampleXpress with the fol- lowing cover: Accessory Part Number BACS2 Protective Cover Magnet Service 1804420 Barcode Collar Set...
Page 50: Figure 5.19 External Control Panel
Design and Function Cryofit Mounting Kit Accessory Part Number Cryofit Mounting Kit HZ16826 External Control Panel Accessory Part Number External Control Panel H118947 Figure 5.19 External Control Panel Z31900_00_01...
Page 51: Transport, Packaging And Storage
Transport, Packaging and Storage Installation, initial commissioning, retrofitting, repairs, adjustments or dismantling of the device must only be carried out by employees of the manufacturer or persons authorised by the manufacturer. Symbols on the Packaging The following symbols are affixed to the packaging material. Always observe the sym- bols during transport and handling.
Page 52 Transport, Packaging and Storage Attach Here Lifting gear (lifting chain, lifting strap) must only be attached to points bearing this symbol. Center of Gravity Marks the center of gravity of packages. Note the location of the center of gravity when lifting and trans- porting.
Page 53: Inspection At Delivery
Transport, Packaging and Storage Component Sensitive to Electrostatic Charge The packaging contains components which are sensitive to an electrostatic charge. Only allow packaging to be opened by trained personnel. Establish potential equalisation before opening. Protect from Heat Protect packages against heat and direct sunlight. Protect from Heat and Radioactive Sources Protect packages against heat, direct sunlight and radioactive sources.
Page 54: Packaging
Transport, Packaging and Storage Packaging About Packaging The individual packages are packaged in accordance with anticipated transport condi- tions. Only environmentally friendly materials have been used in the packaging. The packaging is intended to protect the individual components from transport damage, corrosion and other damage prior to assembly.
Page 55: Installation And Initial Commissioning
Installation and Initial Commissioning Installation, initial commissioning, retrofitting, repairs, adjustments or dismantling of the device must only be carried out by employees of the manufacturer or persons authorised by the manufacturer. Z31900_00_01...
Page 56 Installation and Initial Commissioning Z31900_00_01...
Page 57: Operation Overview
Operation Overview Safety Improper Operation WARNING Danger of injury from improper operation! Improper operation can result in serious injury and significant damage to property. Carry out all operating steps in accordance with the specifications and instruc- tions in this manual. Before starting work, ensure that all covers and safety devices are installed and functioning properly.
Page 58: General Operating Guidelines
Temperature Changes When the ambient temperature changes significantly (for example, after moving the SampleXpress from the stock room before mounting), wait at least 1 hour until the device has achieved room temperature before turning on the device. Contamination of Samples Reusing NMR glass tubes may result in contamination of a new NMR sample from the old substance.
Page 59: Switching On The Device
Switching On the Device Press the Power button on the control panel. Bruker screen appears. If a cassette is inserted, the SampleXpress starts initialization. The device checks if a sample is in the cassette. The indicator lamp switches over to blue (see...
Page 60: Sample Adjustment And Maximum Sample Height
8.2/2) is under the maximum sample height. The glass tube must be below the yellow line, otherwise it will break. (Figure 8.2/1). If the sample is too long, do not use it in the SampleXpress! 1. Maximum Sample Height 2. Sample 3. Spinner Figure 8.2...
Page 61: Operation
Operation The SampleXPress is operated via the application control software or by the TopSpin/ Icon-NMR. In this chapter the application control software is described. The application control software consists of a main screen and four touch screen but- tons. This chapter provides an overview of the different displays and the operating steps to be performed.
Page 62: Main Display
Operation Main Display The main display screen shows all the information necessary during processing. Main Screen in Single Access Mode Position Function Message display. Displays the cassette with its 60 positions. • Gray positions are empty positions. • White positions are loaded with samples. Information about Operator Access Position and Sample Down.
Page 63 Operation Main Screen in Random Access Mode Position Function Message display. Displays the cassette with its 60 positions. Only gray positions are displayed. The system does not show which positions are empty or filled. No information is displayed in Random Access Mode. Touch screen buttons.
Page 64: Figure 9.2 Cassette
Operation Cassette The cassette in the main screen displays the sample numbers and their positions. The Operator Access Position (Figure 9.2/1) is the position where the spinner can be inserted when a cover is used. When no cover is used, the spinner can be inserted in any empty position.
Page 65: Main Menu Touch Screen Buttons In Single Access Mode
Operation 9.2.1 Main Menu Touch Screen Buttons in Single Access Mode Screen Submenu Function Main „Info“ Displays all positions occupied with samples. „Add“ For adding samples to the cassette. „Remove“ For removing samples or the cassette. „Settings“ For device configuration. See also chapter "The Settings Window"...
Page 66: Starting The Application Software
The initialization display appears: Figure 9.4 SampleXpress Device Initialization 9.3.1 Program Start After starting the program several messages are displayed in the message display.
Page 67: Displaying Position Information
Operation Figure 9.7 Message Display: Insert cassette When a new cassette has been inserted, all 60 positions are rescanned. The device detects filled positions and displays them as white. Empty positions are displayed as gray. Displaying Position Information The Info button in the main menu opens a screen showing all the positions which are filled with a sample.
Page 68: Add Or Remove Samples In Single Access Mode
Operation Press the Previous or Next button to see the details of the previous or next loaded position. Press the Back button to return to the information screen. The previous menu is displayed. Add or Remove Samples in Single Access Mode With this function it is possible to add or remove samples from the cassette.
Page 69: Adding Samples
Operation 9.5.1 Adding Samples Press the Add button. The Add selection window appears displaying 3 buttons: When no empty position is left, the Go to free button is disabled and grayed. Figure 9.10 The Add Selection Window Press the Go To Position button to choose the sample position. The Position selection screen appears: Figure 9.11 Position Selection Screen Select an empty gray position to insert the sample into (white positions are loaded...
Page 70: Figure 9.12 Going To The Operator Access Position
Operation Figure 9.12 Going to the Operator Access Position When the operator access position is reached the following message is displayed: Figure 9.13 Insert Sample Screen Insert the sample into the Operator Access Position (Figure 9.14/1). Figure 9.14 Operator Access Position Note: Make sure the sample height is within the limits set in "Sample Adjustment and Maximum Sample Height"...
Page 71: Adding Samples - Go To Free Position
Operation To finish this function, press the Back button, To add another sample, press a gray position, To replace a sample, press a white position. The following message is displayed: Figure 9.15 Replacing a Sample 9.5.1.1 Adding Samples - Go to Free Position When samples do not need to be in any specific order, it is faster to add a sample in the nearest free position: Press the Add button in the main screen.
Page 72: Figure 9.18 Waiting For A Free Position
Operation Press the Go to free button. The chain rotates to the next free position: Figure 9.18 Waiting for a free position Insert a new sample, or press the Skip position button to continue to the next avail- able position: Figure 9.19 Inserting the Sample When a sample has been inserted, the chain rotates automatically to the next free position.
Page 73: Adding/Replacing Samples In Sequence
Operation When all samples have been inserted, press the Back button to return to the main menu. 9.5.1.2 Adding/Replacing Samples in Sequence This functions allows samples to be added or replaced sequentially in ascending order, until the Back button is pressed. Figure 9.21 Removing Samples in Sequence from Position Press the Add button (Figure...
Page 74: Removing Samples
Operation 9.5.2 Removing Samples Press the Remove button (Figure 9.16) in the main screen. The Remove selection screen is displayed: Figure 9.22 Remove Selection Screen Press the Go to position button to choose the sample position. The Position selection screen appears: Figure 9.23 Position Selection Screen Select a white (loaded) position for removing (gray positions are empty positions).
Page 75: Removing All The Samples
Operation When the sample arrives at the Operator Access Position the following message is displayed: Figure 9.25 Remove Sample Screen Remove the sample from the Operator Access Position. Figure 9.26 Operator Access Position The selection screen (Figure 9.11) will be displayed again. To finish this function: Press the Back button, To remove another sample,...
Page 76: Figure 9.27 Remove All
Operation Figure 9.27 Remove All Press the All button. The chain rotates to the next position filled with a sample and a message is dis- played: Figure 9.28 Removing the sample Remove the sample. The chain rotates to the next position filled with a sample. This procedure will be repeated, until all samples are removed from the cassette.
Page 77: Remove Measured Samples From The Cassette
Operation 9.5.2.2 Remove Measured Samples from the Cassette It is possible to remove just the measured samples from the cassette. The measured sample positions are green colored, their state is Finished. Figure 9.30 Finished Samples To remove all measured samples individually through the Operator Access Position: Press the Remove button (Figure 9.16) in the main screen.
Page 78: Figure 9.33 Removing Finished Samples
Operation When the measured sample arrives in the Operator Access Position, a message is displayed: Figure 9.33 Removing finished samples Remove the sample. The chain rotates to the next position filled with a measured sample. This procedure will be repeated, until all measured samples are removed from the cas- sette.
Page 79: Removing Samples In Sequence
Operation 9.5.2.3 Removing Samples in Sequence This functions allows the removal of samples sequentially in ascending order from a selected position, until the next empty position is reached. Figure 9.35 Removing Samples in Sequence from Position Press the Remove button (Figure 9.16) in the main screen.
Page 80: Removing And Inserting The Cassette
Operation Removing and Inserting the Cassette This function enables the cassette to be removed from the device. This allows the cas- sette to be filled outside of the unit. 9.6.1 Removing the Cassette To remove the cassette Press the Remove button in the main menu. Figure 9.36 Main Screen The Remove selection screen is displayed.
Page 81: Figure 9.38 Information Screen
Operation Press Yes. The cassette will be released and a message will be displayed: Figure 9.38 Information Screen Lift the cassette using the hand holds. You should feel a slight resistance. Remove the cassette carefully. The buttons will no longer be accessible (gray colored) and a message is displayed: Figure 9.39 Message Screen Z31900_00_01...
Page 82: Inserting The Cassette
Inserting the Cassette Lift the cassette using its hand holds. Fit the cassette into the cassette guide. Push the cassette carefully into the SampleXpress. Avoid banging it into the Sam- pleXpress unit or the magnet. The engagement will be clearly audible.
Page 83: Figure 9.41 Touch Screen
Operation Press the General button on the user tab. The Settings -> General Touch Screen screen will appear. Figure 9.41 Touch Screen The Settings - General window has 3 tabs: • Touch Screen • Date & Time • About the device Select the Touch Screen tab and press the Start Calibration button.
Page 84: Date And Time Setting
Operation 9.7.2 Date and Time Setting The date and time of the device can be adjusted from the user settings screen. Press the touch screen Settings button in the main menu. The Settings -> User screen will appear: Figure 9.43 Settings Screen Press the General button on the User tab.
Page 85: About The Device
Operation 9.7.3 About the Device This screen displays the following information about the device: • Device Identification Device type Model number Serial number ECL: Engineering Change Level • Software & Others Firmware Network Press the Settings button in the main menu. The Settings screen will appear: Figure 9.45 Settings Screen Press the General button on the User tab.
Page 86: Figure 9.46 About Device Screen
Operation Figure 9.46 About Device Screen Press the Back button to return to the previous screen. Z31900_00_01...
Page 87: Working In Random Access Mode
Operation Working in Random Access Mode When the cover is not used, the sample does not need to be added at the Operator Access Position, but can be added to any empty position. In this Random Access Mode, the main screen is different than the menu in Single Access Mode. Figure 9.47 Main Menu in Random Access Mode Use the Left and Right buttons to move the conveyor chain left or right.
Page 88: Working In Manual Mode
Operation Working in Manual Mode The SampleXpress can be used without a cassette, but the spectroscopy magnet has to be loaded manually. Inserting the sample manually into the magnet: Wait until the outstanding job is completed. The lamp indicator switches to green.
Page 89: 10 Maintenance
10 Maintenance 10.1 Safety Samples DANGER Danger of injury from glass tube breakage! Broken glass tubes may cause minor injuries or material damage, but may also result in a life threatening situation if hazardous substances are used. If a glass tube breaks, refer to the corresponding precautions and cleaning/disin- fection instructions.
Page 90: Accident Hazard From Movement Of Mechanical Parts
Switch off all power supplies before starting work and make sure they cannot be switched on again. Moving Parts CAUTION Accident hazard from movement of mechanical parts! The fingers or hand may be pinched due to movement of mechanical parts. Shut off the SampleXpress before accessing the device. Z31900_00_01...
Page 91: Replacement Parts
Replacement parts must be exchanged by Bruker Service staff! The only exception is the cassette. Only original parts from Bruker are to be used for the SampleXpress. Use of any parts other than from Bruker invalidates all warranty. Parts which are returned to Bruker for repair or disposal must be accompanied by a repair declaration (see "Repair Declaration"...
Page 92: Lift Adjustment
Maintenance 10.4 Lift Adjustment NOTICE Material damage hazard from heavy samples! Samples may be damaged due to incorrect sample lift pressure adjustment. Adjustment is valid only for 1 sample configuration and weight. Personal must be trained. BST Interface Cable from SLCB BSMS BST Interface Cable to BST Gas Interrupt (future feature)
Page 93: Magnet Service
After a Quench Disconnect the SampleXpress from the power supply. Contact Bruker service immediately. In the event of a quench it is possible that the SampleXpress may be damaged. In this case the SampleXpress should be returned to Bruker for repair.
Page 94: Software
10.7 Software The SampleXpress logs all information in a file. With the help of this file customer ser- vice can diagnose the system. In case of troubleshooting as a result of an unknown error, the customer service may ask you to send the log files and the system data. From these files the customer service can obtain additional debugging information.
Page 95: Figure 10.2 Service File
Note the name and the path of the log file in the information window. The file is saved in the directory \Bruker\Automation\logs\ on the USB stick. The file name consists of device name, model number, serial number, date (YYYYMMDD) and time (hhmmss), e.g.
Page 96: Firmware Upgrade
Maintenance If the Information screen (Figure 10.3) does not appear, send the new file on the USB memory stick back to the customer service. The file contains information about the device. 10.7.2 Firmware Upgrade Note: Make sure that the power supply will not be cut off during the entire procedure. Otherwise you will have to send for a service technician.
Page 97: Figure 10.5 Firmware Versions
Figure 10.5 Firmware Versions Several firmware versions may be displayed. Select the firmware version which you want to update on the device. If you are not sure which to use contact Bruker service. The selected firmware is highlighted purple. Figure 10.6 Firmware Versions Press the Update button.
Page 98: Figure 10.7 Confirm Screen
Maintenance Figure 10.7 Confirm Screen Press the Yes button. Firmware is being updated and a notice appears on the touch screen. After the update is finished disconnect the USB memory stick from the device. Z31900_00_01...
Page 99: Device Report File
Maintenance 10.7.3 Device Report File In case of problems with the device, a report can be sent to the customer service. Note: Make sure that the power supply will not be cut off during the entire procedure. Otherwise you will have to send for a service technician. Make sure that the USB memory stick has enough free space and is FAT32 formatted.
Page 100: Figure 10.9 Export Device Report
When the process is finished write down the name and the path of the log file (Fig- 10.10). The file is saved in the directory \Bruker\Automation\logs\ on the USB stick. The file name consists of device name, model number, serial number, date (YYYYMMDD) and time (hhmmss), e.g.
Page 101: Cleaning
10.8 Cleaning 10.8.1 Before Cleaning Stop the submitted jobs in the IconNMR automation mode. Stop the SampleXpress from doing any actions. Switch the power off (see "Switching Off the Device" on page 59). Disconnect the power supply (Figure 10.11/3).
Page 102: Cleaning The Outside Of The Samplexpress Chassis And Units
Usage of volatile cleaners like thinner or benzine may damage the surface of the unit. • Clean the outside of the SampleXpress chassis and units with a soft, lint-free cloth dampened in water. Wait until the unit is completely dry before you reconnect the power cable.
Page 103: Cleaning The Cassette
It may be necessary to send in the device for a cleaning service. No special precautions have been taken in SampleXpress to avoid contamination from a leaking sample tube. Bruker accepts no responsibility for any damage which may occur when samples are used containing radioactive or other hazardous materials.
Page 104 Maintenance Z31900_00_01...
Page 105: 11 Troubleshooting
On the touch screen an error message is displayed, i. e. a code number with a corre- sponding text. Write down the code number and complete error message. Also note the following information: • Part number and serial number of the SampleXpress. • Spectrometer type and order number. •...
Page 106: Figure 11.1 Sample Stuck In Magnet
Troubleshooting Securing to Prevent Restart WARNING Danger to life from an uncontrolled restart! An uncontrolled restart may cause serious injuries or death. Before a restart, ensure that the cause of the emergency stop has been rectified and that all safety devices are fitted and completely functional. Do not unlock the EMERGENCY STOP button until the danger is no longer pres- ent.
Page 107: Danger Of Injury From Improper Troubleshooting
CAUTION Accident hazard from movement of mechanical parts! The fingers or hand may be pinched due to movement of mechanical parts. Shut off the SampleXpress before accessing the device. Behavior in the Event of Faults The following principles apply: Immediately initiate an emergency stop in the event of faults posing an immediate danger to people or property.
Page 108: Fault Indicators
Contact Bruker customer service! In the event of a fault, an error message may appear on the touch screen. Do not use the device anymore. Contact the customer service of Bruker (see "Contact" on page 121 for contact details) and follow the instructions of the customer service.
Page 109: Indicator Lamp
Contact Bruker customer service! In the event of a fault an information about a device failure may appear on the touch screen. Contact the customer service of Bruker (see "Contact" on page 121 for contact details) and follow the instructions of the customer service.
Page 110: Start-Up Following Fault Rectification
Troubleshooting 11.3 Start-up Following Fault Rectification After rectifying the fault, perform the following steps to restart the system: Acknowledge the fault at the controller. Ensure that no persons are in the danger zone. Reset the emergency stop devices. Screens appear on the touch screen. A new initialization will begin.
Page 111: 12 Error Codes
12 Error Codes All the actors named below (cassette clamp, guide, release and sample chain block) have two sensors for detecting the real system state: one sensor detects the inactive state and the other the active state of the corresponding actor. Physically it is never pos- sible that both sensors are active at the same time, but during a malfunction the Sam- pleXpress may produce errors.
Page 112 The cassette was searched for • Activate Sample Down Detection tion for security eject. an empty position for executing Mode (Bruker service only). 117.310.126 a security eject attempt. But the cassette is completely filled. This allows a completely filled cas- sette to be added to the SampleX- press.
Page 113 Inserting further in the magnet. 103.310.144 samples is prohibited. • Adjust sample detection sensor threshold (Bruker service only). 103.310.148 Tube ID changed The Tube ID for this position • Check barcode collar Tube ID; unexpected for posi- was read in the past and has •...
Page 114 • Clean sensor surfaces. • Adjust sample detection sensor threshold (Bruker service only). 117.410.011 Sensor Error: Cas- The internal plausibility check of Contact Bruker for replacing the sette: both sensors the sensors failed. The system defective parts. active! stopped to avoid any damage to the equipment.
Page 115 Error Codes 117.410.012 Sensor Error: Clutch: The internal plausibility check of Contact Bruker for replacing the both sensors active! the sensors failed. The system defective parts. stopped to avoid any damage to the equipment. 117.410.013 Sensor Error: Cas- The internal plausibility check of...
Page 116 Error Codes Z31900_00_01...
Page 117: 13 Dismantling And Disposal
13 Dismantling and Disposal Following the end of its useful life, the device must be dismantled and disposed of in accordance with the environmental regulations. Installation, initial commissioning, retrofitting, repairs, adjustments or dismantling of the device must only be carried out by employees of the manufacturer or persons authorised by the manufacturer.
Page 118: Dismantling
Dismantling and Disposal Improper Dismantling WARNING Danger of injury due to improper dismantling! Stored residual energy, angular components, points and edges on and in the device or on the tools needed can cause injuries. Ensure sufficient space before starting work. Handle exposed, sharp-edged components with care.
Page 119 Dismantling and Disposal NOTICE Danger to the environment from incorrect handling of pollutants! Incorrect handling of pollutants, particularly incorrect waste disposal, may cause seri- ous damage to the environment. Always observe the instructions below regarding handling and disposal of pollut- ants.
Page 120 Dismantling and Disposal Z31900_00_01...
Page 121: 14 Contact
NMR Hotlines Contact our NMR service centers. Bruker BioSpin NMR provide dedicated hotlines and service centers, so that our special- ists can respond as quickly as possible to all your service requests, applications ques- tions, software or technical needs.
Page 122 Contact Z31900_00_01...
Page 123: Safety Notices
Infection, contamination, or other health endangerment as a result of contact with biological or chemical substances, e.g. from broken samples. Clean the device before maintenance work and/or returning to Bruker for repair. Prepare a list of materials in which the device came into contact with or measured.
Page 124 Safety Notices CAUTION Accident and material damage hazard from falling objects! Equipment may fall down during assembly, retrofitting, or dismantling. This may result in personal injury or equipment damage. If necessary, assembly/disassembly the device in multiple parts. Use a platform with railings instead of a ladder to reach the assembly area. Avoid working over the head.
Page 125 Safety Notices NOTICE Material damage hazard due to impacting the magnet. Impacting the magnet may result in a quench. Mount the device carefully on the magnet. Avoid banging the magnet during installation and operation, e.g. when replacing the sample cassette. NOTICE Material damage hazard from unsafe assembly practices! Material damage may result from falling from the ladder during assembly, retrofitting,...
Page 126 Safety Notices NOTICE Material damage hazard from overflow of cryogens! Material damage may result from the overflow of cryogens. Turn off the device during magnet servicing. Cover the device with a protective cover to avoid contact with cold gases. Be sure to use sufficient transfer line and Teflon evacuation hose for nitrogen and helium refills based on recommendations in the magnet manual.
Page 127 Material damage may result when the device comes in contact with NMR solvents. Follow instructions provided in the manual for correct handling of solvents. Follow the sensor cleaning procedures described in this manual. If surface damage should occur, contact Bruker for repair of damaged parts. Z31900_00_01...
Page 128 Safety Notices CAUTION Accident hazard from falling from ladder! It is possible to fall from a ladder when it is used to reach the device on some mag- nets. Do not use a ladder. Use an approved platform to reach the device on the magnet. Wear non-slip shoes.
Page 129 Safety Notices CAUTION Danger of injury from tripping over dirt and scattered objects! Dirt and scattered objects may cause people to slide or trip. A fall may result in inju- ries. Always keep the work area clean. Remove objects which are no longer required from the work area and particularly from the floor.
Page 130 Safety Notices WARNING Danger to life from strong magnetic fields! Strong magnetic fields may cause serious injuries or death and significant damage to property. Persons fitted with heart pacemakers must be kept away from the appliance. The functionality of the heart pacemaker could be compromised. Persons with metal implants must be kept away from the appliance.
Page 131 Safety Notices WARNING Danger to life from an uncontrolled restart! An uncontrolled restart may cause serious injuries or death. Before a restart, ensure that the cause of the emergency stop has been rectified and that all safety devices are fitted and completely functional. Do not unlock the EMERGENCY STOP button until the danger is no longer pres- ent.
Page 132 Safety Notices WARNING Danger of injury from improper operation! Improper operation can result in serious injury and significant damage to property. Carry out all operating steps in accordance with the specifications and instructions in this manual. Before starting work, ensure that all covers and safety devices are installed and functioning properly.
Page 133: Avertissements De Sécurité
Préparez une liste des matières avec lesquelles l'appareil a été en contact ou pour lesquelles l'appareil a effectué des mesures. Le client est tenu de faire parvenir à Bruker une confirmation dûment visée attes- tant que les opérations de nettoyage/ désinfection ont été correctement effec- tuées.
Page 134 Avertissements De Sécurité ATTENTION Risque d'accident et d'endommager le matériel si des objets tombent! L'équipement peut tomber par terre au cours de l'assemblage, de la rénovation "ret- rofit" ou du désassemblage, entraînant un risque de blessures aux personnes ou de dommages à...
Page 135 Avertissements De Sécurité MISE EN GARDE Risque d'endommager le matériel à cause d'une erreur logicielle ! Les échantillons ou l'appareil peuvent être endommagés à cause d'une erreur logicielle ayant provoqué un dysfonctionnement du système de commande. L'utilisa- teur peut également être commotionné à cause d'un dysfonctionnement abrupt ou de la mise en route inopinée du système.
Page 136 Un détecteur d'oxygène doit être installé dans le laboratoire si l'appareil est desti- né à fonctionner à l'azote. Veuillez noter qu'une fuite au niveau du circuit principal d'alimentation ne peut pas être stoppée à l'aide du SampleXpress !! MISE EN GARDE Risque d'endommager le matériel à cause d'un débordement de cryo- gènes !
Page 137 Avertissements De Sécurité ATTENTION Risque d'accident à cause du mouvement des parties mécaniques ! Les doigts ou la main peuvent se retrouver pincés par le mouvement des pièces mécaniques de l'appareil. Eteignez l'appareil avant d'intervenir dessus. ATTENTION Risque d'accident à cause de vêtements trop amples ou de cheveux longs pris dans la chaîne du magasin ! Vous risquez d'être blessé...
Page 138 Avertissements De Sécurité DANGER Danger de blessure à cause d'un tube en verre brisé ! Les éclats de verre des tubes brisés peuvent non seulement causer des blessures mineures et endommager le matériel mais aussi créer une situation sanitaire extrêmement sérieuse si les substances utilisées sont dangereuses. Si un tube en verre se casse, référez-vous aux précautions de sécurité...
Page 139 Suivez les instructions fournies dans le manuel pour savoir comment manipuler correctement les solvants. Respectez les procédures de nettoyage de la sonde décrites dans ce manuel. Dans l'éventualité d'un dégât de surface, contactez Bruker qui se chargera de réparer les parties endommagées. ATTENTION Risque d'accident pour cause de chute de l'escabeau ! Sur certains aimants, il est nécessaire d'utiliser un escabeau pour atteindre l'appar-...
Page 140 Avertissements De Sécurité AVERTISSEMENT Danger de mort pour les personnes non autorisées, à cause des ris- ques encourus dans la zone de danger et la zone de travail ! Le personnel non autorisé qui ne satisfait pas aux exigences décrites dans ce man- uel ne peut pas être averti des dangers inhérents à...
Page 141 Avertissements De Sécurité AVERTISSEMENT Danger de blessure dû aux mouvements causés par des forces pneu- matiques emmagasinées ! Des composants à commande pneumatique peuvent bouger de façon inopinée à cause de forces résiduelles emmagasinées, causant ainsi des blessures graves. Les opérations réalisées sur le système pneumatique ne doivent être effectuées que par des techniciens en pneumatique dûment formés.
Page 142 Avertissements De Sécurité AVERTISSEMENT Danger de blessure à cause de la formation de vapeur ! Au cours du processus opératoire, des vapeurs peuvent se former et provoquer des blessures graves par inhalation. Avant d'installer cet appareil, vérifiez que la salle qui l'accueille est bien ventilée ou équipée d'un extracteur.
Page 143 Avertissements De Sécurité AVERTISSEMENT Danger de mort à cause d'une tension de contact ! L'absence ou la défaillance d'une terre de protection peut susciter l'apparition d'une tension de contact, qui peut elle-même engendrer un danger de blessure ou de mort. Avant la mise en service initiale de l'appareil, raccordez l'alimentation électrique principale à...
Page 144 Avertissements De Sécurité Z31900_00_01...
Page 145: Sicherheitshinweise
Kontakt mit biologischen oder chemischen Substanzen, z.B. bei zerbrochenen Probenbehältern. Reinigen Sie das Gerät vor allen Wartungsarbeiten bzw. bevor Sie es zur Repara- tur an Bruker einsenden. Erstellen Sie eine Liste der Stoffe, mit denen das Gerät in Berührung gekommen ist oder an denen Messungen vorgenommen worden sind.
Page 146 Sicherheitshinweise VORSICHT Gefahr von Unfällen und Sachschäden durch herabfallende Objekte! Beim Zusammenbau, bei Nachrüstungen sowie beim Zerlegen des Geräts können Teile herabfallen. Dadurch können Personen- oder Sachschäden verursacht werden. Falls erforderlich, sollten Sie das Gerät in mehreren Teilen montieren bzw. zerle- gen.
Page 147 Sicherheitshinweise HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch Softwarefehler. Die Proben oder das Gerät können durch Softwarefehler, die zu Funktionsstörungen des Steuersystems führen, beschädigt werden. Außerdem können plötzlich auftre- tende Funktionsstörungen oder ein unerwartetes Anlaufen des Systems bei den Bedienern zu Schreckreaktionen führen. Während der Installation und der Wartung dürfen nur Dummy-Proben verwendet werden.
Page 148 Wenn das Gerät mit Stickstoff betrieben wird, sollte das Labor mit einer Warnein- richtung für den Sauerstoffgehalt der Atemluft ausgestattet sein. Beachten Sie, dass der Austritt von Stickstoff an der Hauptversorgungsleitung von Seiten des SampleXpress nicht abgestellt werden kann! HINWEISE ZUM BETRIEB Gefahr von Sachschäden durch überlaufendes Kühlmittel! Gefahr von Sachschäden durch überlaufendes Kühlmittel.
Page 149 Sicherheitshinweise VORSICHT Unfallgefahr durch sich bewegende Teile! Es besteht die Gefahr von Quetschungen an Hand oder Fingern durch sich beweg- ende Teile. Schalten Sie das Gerät ab, bevor Sie hinein greifen. VORSICHT Unfallgefahr durch Verfangen lose hängender Kleidungsstücke oder langer Haare in der Magazinkette! Falls in der Nähe der Magazinkette mit lose herabhängenden Kleidungsstücken oder langen Haaren gearbeitet wird, besteht Verletzungsgefahr dadurch, dass Haare oder Kleidungsstücke in die Magazinkette geraten.
Page 150 Sicherheitshinweise GEFAHR Verletzungsgefahr durch zerbrochene Glasbehälter! Zerbrochene Glasbehälter können zu geringfügigen Sachschäden oder Verletzun- gen, ebenso aber auch zu lebensbedrohlichen Situationen führen, wenn Gefahrstoffe freigesetzt werden. Falls ein Glasbehälter zerbricht, beachten Sie bitte die entsprechenden Anweisungen zu Vorsichtsmaßregeln und zur Reinigung bzw. Desinfektion. Tragen Sie geeignete Schutzausrüstung.
Page 151 Lösungsmittel. Beachten Sie die Beschreibung zur Reinigung des Sensors im Handbuch. Falls Oberflächen beschädigt werden, sollten Sie sich zur Reparatur der beschä- digten Teile an Bruker wenden. VORSICHT Unfallgefahr durch Sturz von der Leiter! Beim Versuch, das Gerät an einigen Magneten mit einer Leiter zu erreichen, besteht Sturzgefahr.
Page 152 Sicherheitshinweise WARNUNG Lebensgefahr für nicht autorisiertes Personal durch verschiedene Risiken im Gefahren- und Arbeitsbereich! Nicht autorisiertes Personal, das die in diesem Handbuch beschriebenen Bedingun- gen nicht erfüllt, ist mit den Gefahren im Arbeitsbereich nicht vertraut. Daher besteht für nicht autorisiertes Personal die Gefahr von Unfällen mit schweren Verletzungen oder Todesfolge.
Page 153 Sicherheitshinweise WARNUNG Verletzungsgefahr durch Bewegungen von Teilen auf Grund gespeich- erter pneumatischer Energie! Pneumatisch angetriebene Komponenten können sich wegen noch im System befindlicher Druckluft unerwartet bewegen und so zu schweren Verletzungen führen. Arbeiten an den Druckluftsystemen dürfen nur von geschulten Pneumatiktechni- kern ausgeführt werden.
Page 154 Sicherheitshinweise WARNUNG Lebensgefahr durch nicht funktionierende Sicherheitseinrichtungen! Falls Sicherheitseinrichtungen nicht funktionieren oder außer Funktion gesetzt werden, besteht die Gefahr schwerer oder sogar tödlicher Verletzungen. Prüfen Sie vor Beginn der Arbeit, dass alle Sicherheitseinrichtungen korrekt installiert sind und einwandfrei arbeiten. Sicherheitseinrichtungen dürfen in keinem Fall blockiert oder umgangen werden. Sorgen Sie dafür, dass alle Sicherheitseinrichtungen ständig zugänglich sind.
Page 155 Sicherheitshinweise HINWEISE ZUM BETRIEB Gefährdung der Umwelt bei nicht sachgemäßer Handhabung von Gefahrstoffen! Die unsachgemäße Handhabung von Gefahrstoffen, insbesondere die nicht sach- gemäße Entsorgung, kann zu schwerwiegenden Umweltschäden führen. Beachten Sie grundsätzlich die nachstehende Anweisungen, bevor Sie Gefahrst- offe handhaben oder entsorgen. Ergreifen Sie sofort die erforderlichen Maßnahmen, wenn Gefahrstoffe unbeabsi- chtigt in die Umwelt gelangen.
Page 156 Sicherheitshinweise Z31900_00_01...
Page 157: Repair Declaration
Appendix B Repair Declaration The Equipment Clearance Form on the following page needs to be used for Service, Repair, Disposal or Transfer of the SampleXpress. Z31900_00_01...
Page 159: Warning Signs
Danger of injury from glass tube breakage! ............. 25, 89 Note Only trained Bruker personnel are allowed to mount, retrofit, repair, adjust and dis- mantle the unit! ...................... 15 The identification and placement of warning labels should be included in the manual.
Page 160 Warning Signs Z31900_00_01...
Page 161: Figures
Main Screen Example in Single Access Mode ........62 Figure 9.2 Cassette....................64 Figure 9.3 Main Menu Touch Screen Buttons............65 Figure 9.4 SampleXpress Device Initialization ............66 Figure 9.5 Message Display: Adapting cassette ........... 66 Figure 9.6 Message Display: Scanning all samples..........66 Figure 9.7 Message Display: Insert cassette ............
Page 162 Figures Figure 9.8 Information Screen................67 Figure 9.9 Main Menu Touch Screen Buttons............68 Figure 9.10 The Add Selection Window ..............69 Figure 9.11 Position Selection Screen ..............69 Figure 9.12 Going to the Operator Access Position ..........70 Figure 9.13 Insert Sample Screen................
Page 163 Figures Figure 9.44 Date and Time Screen ................. 84 Figure 9.45 Settings Screen..................85 Figure 9.46 About Device Screen ................86 Figure 9.47 Main Menu in Random Access Mode ..........87 Figure 9.48 Sample Transfer Position..............88 Figure 10.1 Connections Left Side................92 Figure 10.2 Service File ..................
Page 164 Figures Z31900_00_01...
Page 165: Tables
Electrical Connection Values .............. 31 Table 4.3 Pneumatic Connection Values ............32 Table 4.4 Operating Environment ............... 32 Table 4.5 Bruker Site Planning Guides............... 32 Table 5.1 Indicator Lamps .................. 46 Table 9.1 Cassette Color Symbols and Their Meanings........64 Table 10.1 Bruker Replacement Parts ..............
Page 166 Tables Z31900_00_01...
Page 167: Glossary
Glossary Glossary BSMS Bruker Smart Magnet Control System Bruker Sample Transport Nuclear Magnetic Resonance SLCB Sample Level Control Board Z31900_00_01...
Page 168 Glossary Z31900_00_01...
Page 169: Index
Index Index Actuators ..........57 Adjusting the spinner ........ 60 Air pressure ..........113 insufficient Application control software ..... 61 Application software ........... 66 booting Barcode collars ......... 58 Barcode reader ........... 9 Base Plate ..........35 Base Unit ..........35 Cassette ..........
Page 170 Index ICON-NMR ..........9 Icon-NMR ..........61 IconNMR ..........101 Indicator lamp ..........46 colors used Laboratory Personnel ......15 Personnel qualifications Laboratory personnel ........15 Maintenance intervals .......93 Motors ............57 Needle valves ...........92 Nitrogen towers ........93 NMR Access Position ......64 NMR access position ........40 NMR glass tubes ........58 NMR measurement ..........38 Influence on...
Page 171 Index SampleTrack ..........9 Security Eject ........... 64 Sensor error ........... 114 Settings ............ 65 Single Access Mode ......... 61 Site Planning ..........32 Skip a sample ........... 76 Spare parts ..........30 Standard Operating Procedure ....14 Storage temperature ........ 54 Strong magnetic fields ......
Page 172 Index Z31900_00_01...
Page 174 With more than 40 years of experi ence meeting the professional scientific sector’s needs across a range of disciplines, Bruker BioSpin has built an enviable rapport with the scientific community and various specialist fields through understanding specific demand, and providing attentive and responsive service.

Bruker SampleXpress User Manual

Table of Contents

1 About

2 Introduction

3 Safety

4 Technical Data

5 Design and Function

6 Transport, Packaging and Storage

7 Installation and Initial Commissioning

8 Operation Overview

9 Operation

10 Maintenance

11 Troubleshooting

12 Error Codes

13 Dismantling and Disposal

14 Contact

Appendix A

Appendix B

Appendix C

Quick Links

Chapters

Troubleshooting

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Questions and answers

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Summary of Contents for Bruker SampleXpress

Table of Contents