Checkout Chromatograms Fid Checkout Conditions And Chromatogram - Agilent Technologies 6890 Series Service Manual

610 Checkout Chromatograms
FID checkout conditions and chromatogram
FID checkout conditions and chromatogram
Column and sample
Type
Sample
Injection volume
Inlet
Temperature
Inlet pressure
Split/Splitless Only
Mode
Purge flow
Purge time
PTV—Splitless Mode
Inlet temperature
Initial time
Rate 1
Final temp 1
Final time 1
Rate 2
Final temp 2
Final time 2
Inlet pressure
Mode
Purge time
Purge flow
Detector
Temperature
H flow
2
Air flow
Makeup flow, N
Offset
2 of 26
HP-5 30 m × 0.32 mm × 0.25 µm PN 19091J-413
FID Checkout PN 18710-60170
1 µL
250°C
Oven Track
25 psi
Splitless
60 mL/min
0.75 min
40°C
0.1 min
350°C
2 min
250°C
0 min
0.75 min
60 mL/min
300° C
30 mL/min
400 mL/min
25 mL/min
2
Should be < 20 pA
Performance Verification
Agilent 6890 Gas Chromatograph Service Manual
Purged/Packed or Split/Splitless
Cool On-Column
(Constant pressure for EPC inlets,
helium)
720°C/min
100°C/min
25 psi (const. press. for EPC inlets)
Splitless
Jun 2001