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Thermo Scientific Orion 2111XP Manual

Thermo Scientific Orion 2111XP Manual

Sodium analyzer
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Thermo Scientific
Orion 2111XP
Sodium Analyzer
UM-263639-005
•
Revision B
•
January 2017

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Summary of Contents for Thermo Scientific Orion 2111XP

  • Page 1 Thermo Scientific Orion 2111XP Sodium Analyzer UM-263639-005 • Revision B • January 2017...

  • Page 2: Table Of Contents

    Contents Section 1 General Information........1 Introduction .
  • Page 3 Calibration Abort Steps ..........62 Calibration Error Codes .

  • Page 4: Section 1 General Information

    S E C T I O N 1 This user guide covers the operation, maintenance and troubleshooting for the Thermo Scientific Orion 2111XP sodium analyzer, which offers unmatched reliability in monitoring critical sample streams throughout the power/steam generation and industrial water industry.

  • Page 5: Features And Benefits

    High acid samples  Features and Benefits The Thermo Scientific Orion 2111XP sodium analyzer features an expandable platform design that incorporates over 30 years of expertise in sodium measurements combined with innovative Thermo Scientific Orion technologies for superior performance. Choice of application/reagent packages: ...

  • Page 6: Application Packages

    Section Application Packages The Thermo Scientific Orion 2111XP sodium analyzer is ideally suited to meet the demanding needs of high purity water measurements and high acid-cation exchange applications, all in one system and all from one of the most trusted names in sodium monitoring.

  • Page 7: Principles Of Operation

    General Information Principles of Operation The sample enters the Thermo Scientific Orion 2111XP sodium analyzer and passes through the inlet valve, bypass/needle valve, inlet filter, pressure regulator, flow meter and into the restrictor tubing. The sample then passes through the flow cell manifold into a reagent bottle and through a diffusion tubing assembly where pH adjustment takes place.

  • Page 8: Principles Of Calibration

    Principles of Calibration Calibration procedures for analytical instruments are important and must be performed carefully. The calibration procedure used in the Thermo Scientific Orion 2111XP analyzer is a variation of Double Known Addition (DKA) using advanced electrode and flow cell technology in combination with the passive diffusion system.
  • Page 9 2111XP analyzer can begin sample measurement again. In addition to Double Known Addition (DKA), the 2111XP analyzer also allows the operator the ability to perform an offline calibration. Figure 2: Flow Cell Volume for DKA Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 10: Offline Calibration

    Calibration Port Flow Cell Reservoir Siphon Tube Figure 3: Fluidics Diagram Pressure Flow Cell Block Regulator Reagent Manifold Diverter Valve Bypass/Needle Valve Inlet Filter Reagent Bottle Diffusion Tubing Adapter Assembly Assembly Reagent Bottle Inlet Valve Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 11: Glossary

    Reference Electrode Filling Solution Bottle – Provides constant flow of electrolyte solution through reference electrode for maximum stability. ATC Probe – Measures sample temperature and inputs data to microprocessor for automatic temperature compensation (ATC). Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 12: Two Channel Analyzer Configurations

    Two Channel Analyzer Configurations A pH/ORP module or conductivity module can be added by the operator to the second channel of the Thermo Scientific Orion 2111XP sodium analyzer for the ultimate flexibility in measurement capabilities. The 2100 series pH/ORP and conductivity analyzers provide accurate and reliable measurements in ultra pure water as well as the harshest industrial environments.

  • Page 13: Section 2 Analyzer Preparation

    4. Carefully remove the entire mounting board with analyzer from the inner box. Note: Do not lift or pull the analyzer by the fluidics or the electronic components. Use the back panel to lift the analyzer system. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 14: Mounting And Plumbing Instructions

    Sample Conditions section. For proper flow cell operation, the analyzer must be installed straight and level upon its  mounting location. Failure to level the analyzer may cause poor siphoning in the flow cell. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 15: Sample Requirements

    The switch should be in close proximity to the analyzer and with easy reach of the user.  The switch should be marked as the disconnecting device for the analyzer.  Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 16: Warning Labels And Locations

    Figure 5: Faceplate Ch 2 Ch 2 status Ch 1 status Power supply – Refer to Figure 6.  Figure 6: Power Supply Note: Replace the fuse only with a fuse of same rating. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 17: Wiring The Analyzer

    2. Remove one or two of the two unused cable glands as required for wiring power cable or auxiliary connections. Power cable optional hole locations are shown in Figure 7. 3. Select and install the appropriate size cable gland or conduit fitting as required. Figure 8: Terminal Connector Location Terminal Connector Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 18: Terminal Assignments

    Do not connect Temperature ground Temperature drive Temperature sense Solution ground Conductivity drive + Conductivity sense + Conductivity sense - Conductivity drive - Reference electrode Jumper to pin 24 when using preamp Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 19: Electrode Wiring Assignments

    Connect red wire 2001SC pH Electrode Reference electrode Connect black wire Sensing electrode Connect clear wire 110250 ORP Electrode Solution ground Connect black wire Reference electrode Connect purple wire Sensing electrode Connect coax center wire Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 20: Installation Of Dipa Reagent And Diffusion Tubing

    The diffusion tubing ships fully assembled for quick and easy installation. Do not use Teflon tape during installation.  Twisting of the clear silicone tubing will compromise tubing integrity and may cause  ruptures. Be careful to avoid kinks and twisting during installation. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 21 If using the 8 inch diffusion tubing, Cat. No. 211198, ensure that the tubing is above the DIPA reagent level. The 8 inch diffusion tubing may need to be looped twice onto the hook to keep the tubing above the liquid level. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 22 5. Replace all three O-rings on the face of the reagent manifold. Refer to Figure 13. 6. Slide the reagent bottle adapter assembly over the threaded screw of the reagent manifold. Refer to Figure 13. 7. Tighten the thumb nut to secure the connection. Figure 13: Reagent Bottle Assembly Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 23: Installation Of Ammonia Reagent And Diffusion Tubing

    8. Re-attach the bottle adaptor/reagent bottle assembly to the flow cell by sliding it onto the screw and tightening the thumbnut. The bottle adaptor can be rotated to allow correct positioning on the analyzer. Figure 14: Reagent Bottle Assembly Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 24: Installation Of New Electrode Cables

    Gently blot the electrode bulb with a clean lab tissue paper. Rinse the electrode again with deionized water. 4. Insert the sodium electrode into its port in the flow cell cap. Refer to Figure 16 for the location. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 25: Installation Of The Atc Probe

    6. Hold the reservoir bottle above the electrode with the bottle cap end down. The electrode should be horizontal with the sidearm pointing up. Gently shake the electrode to allow any trapped air bubbles to rise into the bottle as the electrode fills with solution. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 26 Note: Do not twist the cable while tightening the connection. Twisting may cause damage requiring premature replacement of the cable. 11. Insert the reference electrode into its port in the flow cell cap. Refer Figure 16 for the location. Figure 18: Reference Mounting Clip Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 27: Section 3 Analyzer Operation

    Analyzer Operation S E C T I O N 3 Description of Basic Controls Figure 19: Faceplate Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 28: Description Of Keypad Icons

    Orange LED indicates a channel warning indicates that the electrode or probe Indicator Red LED indicates a channel failure needs to be installed and calibrated. Description of Keypad Icons Figure 20: Keypad Icons Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 29 Orange LED indicates a channel warning indicates that the electrode or probe Indicator Red LED indicates a channel failure needs to be installed and calibrated. Description of Keypad Icons Figure 20: Keypad Icons Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 30: Use Of The Setup Mode

    HOLD is displayed while in the setup mode.  The analyzer will enter the setup mode at the last menu that was used by the operator.  Press to loop through the menu options.  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 31  Main display bottom: 0000 (flashing)  Correct password – Allows operator to enter setup mode for custom programming options.  Incorrect password – Password incorrect or not entered correctly.  System password:  Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 32: Setup Mode Overview

    Default date – System will continue to keep date and time due to battery back up, operator  must set in accordance to local time zone If the battery is removed, the system will show 01/01/2000  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 33 The operator must select the channel number in the main setup mode (CH1 or CH2) and the menu options that are relative to the measurement capability of that channel will be displayed. If a one channel analyzer is being used, the CH1 and CH2 menus will not be shown. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 34  power to analyzer is lost), this alarm is influenced by calibration, errors and offline or hold status rLY3 options – OFF, CAL, HOLD, Err  Default setting for all alarms – OFF  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 35 Set the mA2 analog current output: Scroll between 4-20 mA or 0-20 mA current signals  The outputs share a common return, but are isolated from the main circuitry of the  analyzer Default output current: 4-20 mA  Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 36 Set RLY1, RLY2 and RLY3 status to OFF or On  Set calibration frequency in hours: High limit is 19999 hours  Low limit is 00000 hours  Default setting – 720 hours  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 37 The system will enter the setup mode at the last saved  DISP menu option MEAS HOLD TADJ ALRM mADJ TEST Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 38 SEL CH2 mADJ SEL CH2 TEST SEL CH2 SEL CH2 SEL CH2 Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 39 SET USA OR EUROPEAN US (flashing) SET USA OR EUROPEAN US or EUrO Press to scroll between US and (flashing) EUrO Press to accept the setting and advance to the next screen Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 40 Press to accept the time setting and return to the main setup mode TIME (flashing) SCrn Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 41 To Abort the Reset: PRESS TEST VIEW rSEt Press to return to the main setup mode ENTER TO RESET RSET (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 42 (refer to the menu option displays that are shown on the following pages for detailed instructions) (flashing) SCrn Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 43 SHOW MV ON SINGLE OFF or On Press to scroll between CHANNEL DISPLAY (flashing) OFF and On Press to accept the setting and advance to the next screen AUtO SELECT ISE UNIT UnIt AUtO (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 44 VALUE IN mA (change flashing digit) selected in previous screen Press to move to the next digit Press to set the values of the remaining digits and press move through the remaining digits Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 45 TEMPERATURE Press to set a positive or negative ADJUSTMENT - # . # c temperature value Press to accept the setting and return to the main setup mode Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 46 LOW OR OFF (flashing) SELECT ALARM 2 HIGH rLY2 Press to scroll through LOW OR OFF OFF, HI or LO OFF, HI and LO (flashing) Press to accept the setting and advance to the next screen Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 47 SELECT LOG OR LINEAR SOUt Press to scroll between LOg OUTPUT LOg or LIn and LIn (flashing) Press to accept the setting and advance to the next screen Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 48 Press to set the analog output 2 4-20 SELECT 0-20 OR 4-20 4-20 or 0-20 Press to scroll between 4-20 (flashing) and 0-20 Press to accept the setting and advance to the next screen Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 49 SCrn Action required for two Press to return to the channel channel analyzer specific menu options in the setup mode SEL CH1 or SEL CH2 on main display of two (flashing) SCrn channel analyzer Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 50 SEL CH1 or SEL CH2 on (flashing) SCrn main display of two channel analyzer Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 51 0 . 0 # (last flashing digit) mA2 OUTPUT Press to set the ADJUSTMENT 0 . 0 # temperature mA offset value (change flashing digit) Press to set a positive or negative temperature mA offset Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 52 HIGH VALUE # . # c output terminal 11 displayed Press to accept the test and return to the main setup mod CH1 or CH2 Display for two (flashing) SCrn channel analyzer only Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 53 Press to test the mA outputs (4-20) and relays (rLY) To Test rLY 4-20 SELECT mA OR RELAY tESt Press to scroll between 4-20 and rLY settings and select rLY (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 54 Press to accept the setting and return to the main setup mode CH1 or CH2 Display for two (flashing) SCrn channel analyzer only Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 55 Press to accept the setting and advance to the next screen 0.10 mL SET STD1 VOLUME IN mL Std1 # # . # # (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 56 SEL CH1 or SEL CH2 on (flashing) SCrn main display of two channel analyzer Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 57: Shutdown And Start-Up Procedure

    5. Carefully pull the sodium and reference electrodes out of the top of the flow cell and let them hang by their connectors. 6. Locate the protective cap from reference electrode kit and place it on the base of the reference electrode to prevent it from drying out. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 58 Be careful not to disconnect the reservoir tubing from the reference electrode sidearm. 5. Allow the analyzer to stabilize for approximately 1 hour and then recalibrate. Refer to Section 4, Performing a DKA Calibration. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 59: Section 4 Calibration

    S E C T I O N 4 Calibration Setup The Thermo Scientific Orion 2111XP sodium analyzer provides simple and fast calibration cycles using Double Known Addition (DKA) that quickly have your system back online with security and confidence. The 2111XP analyzer is offered with three application packages that are uniquely designed to accommodate the changing requirements for successful sodium monitoring.

  • Page 60: Flow Cell Operation

    Figure 21: Flow Cell Volumes Recommendations When the Thermo Scientific Orion 2111XP sodium analyzer is first commissioned, it is advisable to flush out fluidics system overnight prior to initial calibration and use. The electronics need not be turned on at this time. Refer to Section 4, Rinsing the Flow Cell.

  • Page 61: Rinsing The Flow Cell

    Position the valve with the pointed end facing up for open position.  2. Open the bypass/needle valve by turning it counterclockwise, see Check for the appropriate sample flow.  Adjust the pressure regulator if required. See step 3.  Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 62: Air Regulation

    6. Begin a DKA calibration. Refer to Section 4, Before Performing a DKA Calibration. Air Regulation The Thermo Scientific Orion 2111XP sodium analyzer utilizes pressure, gravity and fluid dynamics as the principal force of operation for the fluidic system. Air Pump...
  • Page 63 Be sure to hold the pipet completely vertical while dispensing. Do not inject the standard on  the side of the flow cell, as a film may be retained on the inside of the wall, resulting in errors in precision of calibration. Refer to Figure 24. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 64: Performing A Dka Calibration

    When the liquid level in the flow cell begins to drop, WHEN LIQUID LEVEL FLO OFF turn the inlet valve off. Open the calibration port on BEGINS TO DROP TURN the flow cell cap. INLET VALVE OFF OPEN CAL PORT Press PRESS ENTER Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 65 The new slope OR PRESS EXIT TO ABORT and E values will not be saved. The last saved WITHOUT SAVING calibration prior to the aborted calibration will be used in the measure mode. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 66: Calibration Abort Steps

    TURN INLET VALVE ON CLOSE CAL PORT Close the calibration port on the flow cell cap. PRESS ENTER Exit 6 PULL DIVERTER VALVE OUT FLO On Press TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 67: Calibration Error Codes

    PRESS ENTER the recommended range. despite the bad slope. Perform electrode cleaning and conditioning, refer to the Press to abort the calibration and troubleshooting section and repeat refer to Exit 3. the calibration. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 68: Calibration At Custom Concentrations Using Dka

    Calibration At Custom Concentrations Using The Thermo Scientific Orion 2111XP sodium analyzer software has default values to accommodate 0.1 mL additions of standard 1 and standard 2 and flow cell volume of approximately 95 mL.

  • Page 69: Span Check Procedure

    Calibration Section Span Check Procedure The Thermo Scientific Orion 2111XP sodium analyzer remains in the sample mode during the entire procedure. 1. The electrode must be etched within 2 to 3 hours of this procedure. 2. Fill the flow cell to the calibration level (V , approximately 95 mL).
  • Page 70 Actual E value The system will display the recalculated the E PRESS ENTER TO ACCEPT OR PRESS EXIT TO ABORT The system will return to the Press measure mode. Only MEASURE should appear as mode. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 71: Section 5 Analyzer Maintenance

    Analyzer Maintenance S E C T I O N 5 Maintenance Schedule The Thermo Scientific Orion 2111XP sodium analyzer is designed for simple maintenance. Follow the instructions in this section to ensure proper operation of your analyzer. Recommendations To ensure proper maintenance and good analyzer performance, a service logbook should be kept.

  • Page 72: Monthly Maintenance

    The 1/8'' tubing should extend into the bottle. 3. Invert the filling solution bottle and snap it into the clip. 4. Use the pushpin to puncture three air vents in the bottom of the bottle. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 73 3. Remove the diffusion tubing assembly by unhooking the tubing from the hook, pulling off the two diffusion tubing caps and pulling the tubing off of the connectors, as shown in the figures below. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 74 6. Properly dispose of the spent reagent and tubing. 7. Replace the reagent bottle cap adapter O-ring. 8. Follow the instructions in Section 2, Installation of DIPA Reagent and Diffusion Tubing. Figure 25: Exploded View Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 75 Properly dispose of spent reagent and tubing. 4. Fit the ends of the new diffusion tubing over the bottle adaptor nipples. 5. In a hood or outdoors, carefully remove the cap from a new reagent bottle. Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 76: Yearly Preventive Maintenance

    3. Replace all of the calibration and etching solutions (Cat. No. 181140 and/or Cat. No. 181141). Dispose of all old solutions according to the SDS instruction. The SDS files can be downloaded at www.thermofisher.com/water. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 77 4. Place the assembly back into the manifold block and tighten screws. Note: Do not use O-ring grease. Manifold Face O-rings 1. Remove the reagent bottle assembly. 2. Remove the three O-rings from the face of the flow cell manifold. 3. Insert the new O-rings. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 78 5. Unscrew the clip behind flow cell that holds the restrictor tube to panel. 6. Replace with new restrictor tubing assembly. 7. Be sure all fittings are secure, to prevent leaks. 8. Open the inlet valve to start sample flow through analyzer. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 79: Section 6 Troubleshooting

     access to menus used for system diagnostics. Each menu is sequential. Press to scroll through the diagnostics menu selections.  can be pressed at any time to return to the measure mode.  Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 80 # # # . # (mV offset) CALIBRATION CELL # . # # # (Cell Constant) CONSTANT CALIBRATION TIME/DATE HH:MM Press Press to display the calibration time MM/DD or DD/MM and date scroll through the last 12 calibrations Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 81 Actual temperature value for Concentration and mV Press to scroll between the logged measurement values for logged measurement log and the data and time measurement display Press to proceed to the next menu Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 82 Displays the model number of the system.  mV and Noise Measurements Displays the current mV measurement value and the noise associated with the  measurement. mA Output Values Displays current mA values for mA1 and mA2 outputs.  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 83 Press to start the test Verify that all of the display segments are All segments on All segments on System will cycle on and that the LED colors are functional through the LED colors Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 84: Slope Problems

    Check the electrode function, etch the electrode, recalibrate the analyzer, and if the  analyzer continues to read low, replace the electrode. Check electronics to read mV input correctly. Use electronic test kit (Cat. No. 180029)  procedure for checking electronics function. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 85 “Ref” for the reference electrode.  “Sensing” for the sodium electrode.  Sensing electrode coated – etch or replace the sensing electrode.  Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 86: Troubleshooting Matrix

    Repeat calibration using standards in the correct sequence. Temperature probe failure Disconnect ATC. Temperature should read 25 °C (E101). Replace if necessary. Background concentration too high for Repeat calibration using custom, higher concentration standards standards. Refer to Section 4, Calibration. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 87: Error/Event Codes

    Event Code System Status Codes A711 ALARM1 CH1 ON Alarm 1 channel 1 engaged (closed) A712 ALARM2 CH1 ON Alarm 2 channel 1 engaged (closed) A713 ALARM3 CH1 ON Alarm 3 channel 1 engaged (open) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 88 (5 °C to 45 °C) for ISE Replace if needed. E102 CH2 TEMP OUT OF RANGE Temperature sensor on channel 2 out of range Check ATC cable and probe connections. (5 °C to 45 °C) for ISE Replace if needed. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 89 E104 CH2 MEAS OVER RANGE Measurement is over range on channel 2, the display Check if electrode is not connected,electrode should also be flashing ‘9999’ cables are faulty or electrode junction is fouled Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 90: Resetting The Analyzer

    Replace electrode, if needed. Resetting the Analyzer The Thermo Scientific Orion 2111XP sodium analyzer allows the user to reset the analyzer through the setup mode or by a hard reset. Resetting the analyzer will restore all settings in the setup mode to factory default values.

  • Page 91: Serial Number And Software Revision

    Service and Repair Extended Warranty The Thermo Scientific Orion 2111XP sodium analyzer provides measurements through a combination of our premium electrode technology and user friendly scrolling marquee to set a new industry standard for reliability. Similarly, Thermo Fisher Scientific now offers multiple levels of service programs to meet your needs beyond the One-Year Product Warranty period.
  • Page 92 Not sure which plan is best for you? Ask your Thermo Scientific Orion products sales representative to put you in touch with the service plan manager. We have additional service options that are sure to address your concerns. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 93 Replacement of consumables (additional charge for consumables)  Diagnostic check to verify all operating parameters are within the factory specifications  Check analyzer electrodes, flows and pressures  Clean and replace any wearable items  Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 94: Section 7 Customer Service

    “This digital apparatus does not exceed the (Class A) limits for radio noise emissions from digital apparatus set out in the Radio Interference Regulations of the Canadian Department of Communications.” Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 95: Statement Of Conformity

    EN 61326-1:2013 EN 61010-1:2010 EN 50581:2012 This declaration is valid for the product(s) manufactured after the date listed below. Chelmsford, MA 15, December 2016 Shervin Ghorab Compliance Manager Thermo Fisher Scientific 271818-000 Rev. A Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 96: Weee Compliance

    U.S. and Canada, contact your international coordinator for rush order scheduling. All rush orders carry a $50 incremental charge per order. FOB: Beverly. Freight charges are prepaid and added or freight collect. All rush order processing is subject to stock availability. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 97 In the event of a delay in performance due to any such cause, the date of delivery or time for completion of performance will be extended by a period of time reasonably necessary to overcome the effect of such delay. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 98 Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 99: Appendix

    Appendix Appendix Mounting Dimensions Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 100: Ise Default Values

    • 90% of final reading within 5 minutes of injecting a standard solution • 5 minutes maximum for time from 5% to 90% of measured change following dynamic addition of a standard solution Units Displayed ppb, ppm (auto ranging) Temperature Compensation Automatic Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 101 54 x 76 mm (2 1/8 in x 3 in) Marquee Temperature, operator prompts Middle Line Concentration, error codes Lower Line mV (selectable) Text Display Scrolling marquee for English language instructions on setup, calibration and diagnostics menus Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 102 250 VAC/5A, 30 VDC/5A, resistive load only Minimum Value Alarm Maximum Value Alarm Error Alarm Calibration/offline Alarm Programmable Min. and Max. Values Analyzer Features Non-volatile Memory Battery Backup (replaceable) Data Logging Keypad 8 electromechanical keys with graphic overlay Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 103 Up to 95%, non-condensing Altitude Sea level to 2000 M Shock and Vibration Vibration, Shipping/handling 0 to 60 Hz @ 1 G Load Shock, Drop Test in Packaging 36'' on all sides and corners Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 104: Ordering Information

    (211194), reagent bottle adapter (2111RBA), sodium standard solutions kit (181140), sodium electrode (210045), reference electrode (210056), (5) x 2 oz. bottles of reference electrode filling solution (181073), O-ring kit, check valve, pipet tips (0.1 mL), restriction tubing assembly and inlet filters Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 105 Electrode Kit – includes sodium sensing electrode (210045), sodium reference electrode (210056) and reference electrode filling solution (181073) 210045 Sodium sensing electrode with screw cap 210056 Sodium reference electrode with screw cap 181073 Reference electrode filling solution, (5) x 2 oz bottles Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 106: Accessory Options

    Inlet valve assembly 2100BV Bypass/needle valve assembly 2100RG Regulator assembly 2100DA Drain and clamp assembly 2100FM Flow meter assembly 2100RT Restrictor tubing assembly 2100RF Reagent bottle adapter fittings 2100FC Flow cell assembly 2100PA Air pump assembly Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 107: Recommended Consumables For Annual Operation

    Diisopropylamine Application Consumables Package 211192XPF Reagent-less Diisopropylamine Application For International Consumables Package Use Only For Cation/High Acid Application Package: 211150XP Cation/High Acid Application Consumables Package 211150XPF Reagent-less Cation/High Acid Application Consumables Package For International Use Only Thermo Scientific Orion 2111XP Sodium Analyzer...

  • Page 108: Pipet Operation

    Clean the area where you plan to attach the shelf hanger. Apply two stickers to the underside of the shelf hanger. Press the shelf hanger firmly into place on a shelf, counter top or pipet stand. To use, hang the finger rest on the shelf hanger. Orion 2111XP Sodium Analyzer Thermo Scientific...

  • Page 109: Pipet Techniques

    This action will empty the tip. 4. Release the push button to the ready position. If necessary, change the tip and continue pipeting. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 110 UM-263639-005 0117 Rev...
  • Page 111 HOLD is displayed while in the setup mode.  The analyzer will enter the setup mode at the last menu that was used by the operator.  Press to loop through the menu options.  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 112  Main display bottom: 0000 (flashing)  Correct password – Allows operator to enter setup mode for custom programming options.  Incorrect password – Password incorrect or not entered correctly.  System password:  Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 113 Default date – System will continue to keep date and time due to battery back up, operator  must set in accordance to local time zone If the battery is removed, the system will show 01/01/2000  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 114 The system will enter the setup mode at the last saved  DISP menu option MEAS HOLD TADJ ALRM mADJ TEST Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 115 SEL CH2 mADJ SEL CH2 TEST SEL CH2 SEL CH2 SEL CH2 Press to loop through the menu options Press to select the desired menu option and enter the submenu to customize setup parameters Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 116 SET USA OR EUROPEAN US (flashing) SET USA OR EUROPEAN US or EUrO Press to scroll between US and (flashing) EUrO Press to accept the setting and advance to the next screen Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 117 Press to accept the time setting and return to the main setup mode TIME (flashing) SCrn Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 118 To Abort the Reset: PRESS TEST VIEW rSEt Press to return to the main setup mode ENTER TO RESET RSET (flashing) SCrn Press to scroll to the next menu Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 119 (refer to the menu option displays that are shown on the following pages for detailed instructions) (flashing) SCrn Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 120 SHOW MV ON SINGLE OFF or On Press to scroll between CHANNEL DISPLAY (flashing) OFF and On Press to accept the setting and advance to the next screen AUtO SELECT ISE UNIT UnIt AUtO (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 121 VALUE IN mA (change flashing digit) selected in previous screen Press to move to the next digit Press to set the values of the remaining digits and press move through the remaining digits Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 122 TEMPERATURE Press to set a positive or negative ADJUSTMENT - # . # c temperature value Press to accept the setting and return to the main setup mode Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 123 LOW OR OFF (flashing) SELECT ALARM 2 HIGH rLY2 Press to scroll through LOW OR OFF OFF, HI or LO OFF, HI and LO (flashing) Press to accept the setting and advance to the next screen Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 124 SELECT LOG OR LINEAR SOUt Press to scroll between LOg OUTPUT LOg or LIn and LIn (flashing) Press to accept the setting and advance to the next screen Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 125 Press to set the analog output 2 4-20 SELECT 0-20 OR 4-20 4-20 or 0-20 Press to scroll between 4-20 (flashing) and 0-20 Press to accept the setting and advance to the next screen Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 126 SCrn Action required for two Press to return to the channel channel analyzer specific menu options in the setup mode SEL CH1 or SEL CH2 on main display of two (flashing) SCrn channel analyzer Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 127 SEL CH1 or SEL CH2 on (flashing) SCrn main display of two channel analyzer Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 128 0 . 0 # (last flashing digit) mA2 OUTPUT Press to set the ADJUSTMENT 0 . 0 # temperature mA offset value (change flashing digit) Press to set a positive or negative temperature mA offset Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 129 HIGH VALUE # . # c output terminal 11 displayed Press to accept the test and return to the main setup mod CH1 or CH2 Display for two (flashing) SCrn channel analyzer only Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 130 Press to test the mA outputs (4-20) and relays (rLY) To Test rLY 4-20 SELECT mA OR RELAY tESt Press to scroll between 4-20 and rLY settings and select rLY (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 131 Press to accept the setting and return to the main setup mode CH1 or CH2 Display for two (flashing) SCrn channel analyzer only Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 132 Press to accept the setting and advance to the next screen 0.10 mL SET STD1 VOLUME IN mL Std1 # # . # # (flashing) Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 133 SEL CH1 or SEL CH2 on (flashing) SCrn main display of two channel analyzer Press to scroll to the next menu Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 134 5. Carefully pull the sodium and reference electrodes out of the top of the flow cell and let them hang by their connectors. 6. Locate the protective cap from reference electrode kit and place it on the base of the reference electrode to prevent it from drying out. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 135 When the liquid level in the flow cell begins to drop, WHEN LIQUID LEVEL FLO OFF turn the inlet valve off. Open the calibration port on BEGINS TO DROP TURN the flow cell cap. INLET VALVE OFF OPEN CAL PORT Press PRESS ENTER Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 136 The new slope OR PRESS EXIT TO ABORT and E values will not be saved. The last saved WITHOUT SAVING calibration prior to the aborted calibration will be used in the measure mode. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 137 TURN INLET VALVE ON CLOSE CAL PORT Close the calibration port on the flow cell cap. PRESS ENTER Exit 6 PULL DIVERTER VALVE OUT FLO On Press TURN INLET VALVE ON CLOSE CAL PORT PRESS ENTER. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 138 PRESS ENTER the recommended range. despite the bad slope. Perform electrode cleaning and conditioning, refer to the Press to abort the calibration and troubleshooting section and repeat refer to Exit 3. the calibration. Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 139 Calibration At Custom Concentrations Using The Thermo Scientific Orion 2111XP sodium analyzer software has default values to accommodate 0.1 mL additions of standard 1 and standard 2 and flow cell volume of approximately 95 mL.
  • Page 140 Calibration Section Span Check Procedure The Thermo Scientific Orion 2111XP sodium analyzer remains in the sample mode during the entire procedure. 1. The electrode must be etched within 2 to 3 hours of this procedure. 2. Fill the flow cell to the calibration level (V , approximately 95 mL).
  • Page 141 Actual E value The system will display the recalculated the E PRESS ENTER TO ACCEPT OR PRESS EXIT TO ABORT The system will return to the Press measure mode. Only MEASURE should appear as mode. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 142  access to menus used for system diagnostics. Each menu is sequential. Press to scroll through the diagnostics menu selections.  can be pressed at any time to return to the measure mode.  Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 143 # # # . # (mV offset) CALIBRATION CELL # . # # # (Cell Constant) CONSTANT CALIBRATION TIME/DATE HH:MM Press Press to display the calibration time MM/DD or DD/MM and date scroll through the last 12 calibrations Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 144 Actual temperature value for Concentration and mV Press to scroll between the logged measurement values for logged measurement log and the data and time measurement display Press to proceed to the next menu Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 145 Displays the model number of the system.  mV and Noise Measurements Displays the current mV measurement value and the noise associated with the  measurement. mA Output Values Displays current mA values for mA1 and mA2 outputs.  Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 146 Press to start the test Verify that all of the display segments are All segments on All segments on System will cycle on and that the LED colors are functional through the LED colors Thermo Scientific Orion 2111XP Sodium Analyzer...
  • Page 147 Check the electrode function, etch the electrode, recalibrate the analyzer, and if the  analyzer continues to read low, replace the electrode. Check electronics to read mV input correctly. Use electronic test kit (Cat. No. 180029)  procedure for checking electronics function. Orion 2111XP Sodium Analyzer Thermo Scientific...
  • Page 148 Replace electrode, if needed. Resetting the Analyzer The Thermo Scientific Orion 2111XP sodium analyzer allows the user to reset the analyzer through the setup mode or by a hard reset. Resetting the analyzer will restore all settings in the setup mode to factory default values.
  • Page 149 Service and Repair Extended Warranty The Thermo Scientific Orion 2111XP sodium analyzer provides measurements through a combination of our premium electrode technology and user friendly scrolling marquee to set a new industry standard for reliability. Similarly, Thermo Fisher Scientific now offers multiple levels of service programs to meet your needs beyond the One-Year Product Warranty period.

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