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Summary of Contents for HACH LANGE ORBISPHERE 6110
- Page 1 DOC024.52.93009 ORBISPHERE Model 6110 Package Analyzer User Manual 08/2013, Edition 5...
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Page 3: Table Of Contents
Table of Contents ......................5 Section 1 General Information 1.1 About this manual ........................5 1.2 Contact information........................5 1.3 Safety information ........................5 1.3.1 Use of hazard information ....................5 1.3.2 Disclaimer ........................... 6 1.3.3 Safety precautions ......................6 1.3.4 Service and repairs ...................... - Page 4 Table of Contents 5.3.1 Package management ......................35 5.3.2 Formula management .......................36 5.4 Instrument parameters .......................37 5.4.1 Measurement output ......................37 5.4.2 Time and date ........................37 5.4.3 System information......................38 5.5 Security and user management ....................38 5.5.1 Security management .......................38 5.5.2 User management......................38 5.5.3 Audit trail ...........................39 5.6 Communication ..........................39 5.6.1 Data download configuration.....................39...
- Page 5 Table of Contents ......................63 Section 10 Troubleshooting 10.1 Error and warning messages ....................63 10.1.1 Error messages....................... 63 10.1.2 Warning messages ......................64 10.1.3 Red LED’s on startup screen ..................65 10.1.4 Measurement problems ....................66 ..................67 Section 11 Spare Parts and Accessories ................
- Page 6 Table of Contents...
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Page 7: Section 1 General Information
Copyright © 2013 by Hach Lange. All rights reserved. No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of Hach Lange. -
Page 8: Disclaimer
General Information 1.3.2 Disclaimer CAUTION The manufacturer is not responsible for damages resulting from misapplication or misuse of this product and rejects the regulation of such damages, including direct, indirect and consequential damages, and in full accordance with applicable law. The user is solely responsible for the identification of critical applications and risks and taking appropriate measures to protect processes during a possible equipment malfunction. -
Page 9: Use Of Antifoam
General Information 1.3.6 Use of antifoam Antifoam is injected into the sample as part of the measurement process. Once a sample has completed the measurement process it will therefore contain a small amount of antifoam. After measurement, ensure the sample is disposed of in a sink (or similar) to avoid any risk of ingestion. -
Page 10: Product Recycling Information
General Information 1.4 Product recycling information ENGLISH Electrical equipment marked with this symbol may not be disposed of in European public disposal systems after 12 August 2005. In conformity with European local and national regulations (EU Directive 2002/96/EC), European electrical equipment users must now return old or end-of-life equipment to the manufacturer for disposal at no charge to the user. - Page 11 General Information SVENSKA Elektronikutrustning som är märkt med denna symbol kanske inte kan lämnas in på europeiska offentliga sopstationer efter 2005-08-12. Enligt europeiska lokala och nationella föreskrifter (EU-direktiv 2002/96/EC) måste användare av elektronikutrustning i Europa nu återlämna gammal eller utrangerad utrustning till tillverkaren för kassering utan kostnad för användaren. Obs! Om du ska återlämna utrustning för återvinning ska du kontakta tillverkaren av utrustningen eller återförsäljaren för att få...
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Page 12: Product Disposal
European public disposal systems after 12 August 2005. Hach Lange will offer to take back (free of charge to the customer) any old, unserviceable or redundant instruments and systems which carry the above symbol, and which were originally supplied by Hach Lange. -
Page 13: Restriction Of Hazardous Substances (Rohs)
Currently, monitoring and control instruments do not fall within the scope of the RoHS Directive, however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing. - Page 14 General Information...
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Page 15: Section 2 Specifications
Section 2 Specifications 2.1 Technical specifications Specifications are subject to change without notice. Analysis 1 ppb - 12 ppm Measurement range 0.75 - 5 V/V or 1.5 - 10 g/kg Total Package Oxygen ± 5 µg/L ± 10% whichever is the greater on equilibrated Repeatability r packages at T = 10 to 25°C... -
Page 16: Instrument Dimensions
Specifications 2.2 Instrument dimensions Figure 1 Instrument dimensions... -
Page 17: Main Instrument Components
Specifications 2.3 Main instrument components 2.3.1 Front view 1. Display panel 4. Knob to tilt package 2. Package piercing device 5. Measurement start button with LED 3. Package holder 6. Package backstop Figure 2 Instrument components - front view... -
Page 18: Left Side View
Specifications 2.3.2 Left side view 1. Power socket 4. Ethernet connection 2. Power ON/OFF rocker switch 5. USB-B client 4-pin connector 3. USB-A connector for mass storage device Figure 3 Instrument components - left side view... -
Page 19: Right Side View
Specifications 2.3.3 Right side view 1. Gas connection No. 1 (IN) - Forcing gas (Air or N 4. Gas connection No. 4 (OUT) - Pressure sensor calibration 2. Gas connection No. 2 (IN) - Purge gas (CO 99.9% purity) 5. Emergency STOP button 3. -
Page 20: Instrument Switches And Buttons
Specifications 2.4 Instrument switches and buttons The mains power switch is located at the rear left of the instrument (No. 2 in Figure 3 on To switch the instrument on and off, press the rocker switch to the page 16). required position: “O”... -
Page 21: Section 3 Installation
Section 3 Installation WARNING This section provides necessary information to install and connect the analyzer. The installation of the analyzer should be performed in accordance with relevant local regulations, and only by personnel trained and experienced in the installation of the 6110 analyzer. Disconnect the power supply of the analyzer before carrying out any work inside the analyzer. -
Page 22: Positioning
(or similar) attached to the lifting ring located on the top of the instrument when moving it. Hach Lange recommends installing the instrument on a sturdy laboratory table that can more than support the 55kg weight. Place it on a clean flat surface, and convenient to the power source. -
Page 23: Physical Installation
The instrument should now be ready for use. If a problem should arise with the instrument, please refer initially to Troubleshooting on page 63. If the problem cannot be overcome, please contact your Hach Lange representative who will be happy to assist you. -
Page 24: Additional Installation Information
Installation 3.5 Additional installation information 3.5.1 Microsoft ActiveSync® configuration This software must be installed on your PC when connecting to the instrument via the USB client connector (No. 5 in Figure 3 on page 16). The latest version of ActiveSync® is available as a free download from www.microsoft.com Once successfully installed, ActiveSync®... -
Page 25: Power Supply
Important Note: To optimize the performance and reliability of the instrument, it is strongly recommended to only use the silicon antifoam supplied by Hach Lange (part number 33156). To fill the cartridge, proceed as follows (numbers in the boxes correspond to the steps):... - Page 26 Installation 1. Connect the syringe to the tubing with the quick connector. 2. Unscrew the cap from the antifoam recharge bottle and put the tubing in, making sure it goes as near to the bottom of the liquid as possible. 3.
- Page 27 Installation 7. Attach the end of the second piece of tubing to the antifoam cartridge by pressing until the connector clicks into place on the inlet valve. Then, push on the end of the syringe to empty the contents into the cartridge. The syringe has a volume of 100mL and the cartridge a volume of 280mL, so repeat the process until the antifoam cartridge is full.
- Page 28 Installation...
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Page 29: Section 4 User Interface And Startup
Section 4 User Interface and Startup 4.1 User interface 4.1.1 Turning the instrument ON and OFF The instrument has a power switch located at the rear of the left side of the base (No. 2 in Figure 3 on page 16). -
Page 30: Rolling Lists
User Interface and Startup 4.1.4 Rolling lists For convenience, selection through a possible large list of items has been designed with a rolling list as in the example below. Use the up and down arrows at the side to navigate through the list, or select one item directly. -
Page 31: Information And Warning Windows
User Interface and Startup 4.1.6 Information and warning windows At various stages, an information or warning message may be displayed to request confirmation from the operator that his last action(s) must be applied, or that there is a problem that did not enable the requested action to be performed. -
Page 32: Instrument Startup
User Interface and Startup 4.2 Instrument startup Important Note: The following assumes that the instrument is already fully operational and has been used for taking measurements. For first time startup of the instrument refer to Installation on page 20 to ensure additional procedures have been completed successfully for the instrument to start up without errors occurring during the auto check procedures. -
Page 33: User Identification And Access Level
User Interface and Startup 4.2.2 User identification and access level If access rights have been enabled, it will be necessary to log on as an authorized user to get access to the instrument functionalities and settings (see Security and user management on page 38 to set these up). -
Page 34: Menu Structure Overview
User Interface and Startup 4.3 Menu structure overview... -
Page 35: Section 5 Configuration
Section 5 Configuration 5.1 Configuration menu overview... -
Page 36: Units And Resolutions
Configuration This section describes the sequence of actions required to configure the instrument. The following configuration options are available from the main screen: Units and resolutions • Package parameters • Instrument parameters • Security and user management • Communication • Scheduled operations •... -
Page 37: Package Parameters
Configuration 5.3 Package parameters 5.3.1 Package management Package management Add new package definitions (up to a maximum of 100), and edit or delete existing definitions. To edit or delete a package, first select the package from the list displayed by touching the package name on the screen, and then press either Edit or Delete as appropriate. -
Page 38: Formula Management
Configuration 5.3.2 Formula management Formula management This option allows you to add new formula definitions (up to a maximum of 40), and edit or delete existing definitions. You can use up to 16 variables pre-defined by the instrument and 2 user defined numerical variables that are set up manually at the end of each measurement. -
Page 39: Instrument Parameters
Configuration Table 1 Formula terms and definitions Term Definition O2 HS in headspace O2 liquid in liquid O2 total in headspace + O in liquid CO2 HS in headspace CO2 liquid dioxide in liquid CO2 total in headspace + CO in liquid CO2 PT Concentration of dissolved CO... -
Page 40: System Information
Configuration 5.4.3 System information System information Display the system information about the currently configured boards. Select Exit to exit the screen. 5.5 Security and user management 5.5.1 Security management Note: When the instrument is started for the first time, security is disabled by default. To avoid any unauthorized access, it is highly recommended that each user be entered into the system and given appropriate access rights as soon as possible. -
Page 41: Audit Trail
Note: It is recommended to set the files to text format for easy loading into standard software applications on the PC such as Microsoft Excel or similar. The data format is only required for Hach Lange service and support personnel. -
Page 42: Ethernet Configuration
Configuration The text files (with a .txt file extension) are in a readable format on a PC and most document editors (MS Word, Notepad, etc.) can be used to open these files as well as spreadsheet and other reporting tools (e.g. MS Excel). The following is an example of the instrument configuration report (Configuration.txt) as viewed using the Notepad utility. - Page 43 Configuration You will be required to enter a valid username and password combination (defined in Security and user management on page 38). The initial screen will then be displayed. You can then click on Expand All to see all the available options.
- Page 44 Configuration 5.6.2.2 OPC client OPC (Open Process Control) is a software interface standard that allows Windows PC programs to communicate with industrial hardware devices. The OPC client software is installed on a PC and communicates directly with the OPC server embedded in the 6110 instrument. To activate the link, check the OPC option on the ethernet configuration screen.
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Page 45: Scheduled Operations
Configuration 5.7 Scheduled operations This option defines the sensor service and calibration schedule for all the sensors installed on the instrument. 5.7.1 Manual calibration Manual calibration Select a sensor and check the activation flag as required. When set, the system will set a yellow status indicator message to inform you when a Calibration sensor calibration is required (see also Instrument status indicator on page... - Page 46 Configuration...
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Page 47: Section 6 Calibration
Section 6 Calibration 6.1 Calibration menu overview This section describes the sequence of actions required to calibrate the sensors and flow meter on the instrument: 1. Barometric pressure sensor 2. Pressure sensor 3. Temperature sensor 4. CO2 sensor 5. Flow sensor 6. -
Page 48: Barometric Pressure Sensor
Calibration 6.4 Barometric pressure sensor After selecting this option, the details of the last barometric pressure sensor calibration are displayed. This shows the values recorded, and information about who performed the last calibration and when. The due date of the next calibration is also shown (determined by the parameters entered in Scheduled operations on page 43). -
Page 49: Temperature Sensor
Calibration 6.6 Temperature sensor After selecting this option, the details of the last temperature sensor calibration are displayed. This shows the values recorded, and information about who performed the last calibration and when. The due date of the next calibration is also shown (determined by the parameters entered Scheduled operations on page 43). -
Page 50: Flow Sensor
Calibration 6.8 Flow sensor After selecting this option, the details of the last flow sensor calibration are displayed. This shows the values recorded, and information about who performed the last calibration and when. The due date of the next calibration is also shown (determined by the parameters entered in Scheduled operations on page 43). -
Page 51: Section 7 Measurement
Section 7 Measurement The following flow chart shows an overview of the measurement process. The actions listed on the left are performed by the user, and those on the right by the instrument. -
Page 52: Main Screen
Measurement 7.1 Main screen The initial screen displays standard information about the package to measure: You have the option to change the details displayed or to start the measurement process: User • Package ID • Start analysis • 7.1.1 User User Enter a valid User ID and Password. - Page 53 Measurement Select the Start Analysis option to start the measurement process. The instrument will display information regarding the measurement step being taken, instructions on any user involvement required, and the measurement progress throughout the duration of the measurement process. The first screen gives details of the package being analyzed and gives the user information on what action to take.
- Page 54 Measurement The head space is analyzed • The liquid is analyzed • Note: This step will not be executed if the Headspace measurement has been defined for this package (see Package parameters on page 35). The measurement completes and the piercing arm is raised to its home position •...
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Page 55: Diagnostic Measurement And Results Views
Measurement 7.2 Diagnostic measurement and results views These views are essentially used for troubleshooting purposes by Hach Lange service technicians, therefore no detailed explanation of the data displayed is given in this manual. 7.2.1 Measurement view As the measurement process executes, the measurement details are displayed down the left side of the screen. - Page 56 Measurement...
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Page 57: Section 8 Analysis
Section 8 Analysis 8.1 Analysis menu overview 8.1.1 Open data Open data This option allows you to view the measurement data from the last 1000 measurements. The data elements displayed are those defined in Table settings below. Use the Previous and Next buttons to scroll through the data. Select one of the lines of data and the Info button will be made available. - Page 58 Analysis...
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Page 59: Section 9 Maintenance
Every 6 months Replace flow chamber O-ring Every 6 months Replace the blue sample tubing Every 6 months The following are performed by a Hach Lange service technician Sensor calibrations Twice a year Replace needle valve Yearly Replace antifoam cartridge internal membrane... -
Page 60: Maintenance Menu Overview
To ensure the performance and reliability of the instrument, it is strongly recommended to only use the silicon antifoam supplied by Hach Lange (part number 33156). Chemical reactions within the gas sensor requires that the oxygen sensor be serviced EC sensor regularly to restore its original sensitivity. -
Page 61: Digital Input Verification
If this button is activated it means that the system is in an abnormal state of operation and you should call your local Hach Lange representative. Activated when the piercing device is in its lowest position. End of travel lower bound activated Activated when the front door is closed. -
Page 62: Actuator Verification
Maintenance 9.3.3 Actuator verification Manual displacement Press on the icons displayed left to perform the required operation on Move to the home the piercing assembly. position (top) The current position is displayed on the left side of the screen as the assembly moves either up or down. -
Page 63: Analog Value Monitoring
Maintenance Antifoam system Use this option to check the level of antifoam remaining, and to test that the antifoam injector system is working. This option is useful to purge the system before an extended stand-by (several weeks) or when performing start up procedures. Injection number Enter the number of injections. -
Page 64: Global System View
Maintenance 9.3.5 Global system view This option allows you check various components of the instrument: O2 calibration valve • Gas calibration valve • Reference volume valve • Main purge valve • Needle purge valve • On-off valves function • Regulating valves function •... -
Page 65: Section 10 Troubleshooting
Section 10 Troubleshooting 10.1 Error and warning messages Note: If any error or warning persists, please contact your Hach Lange representative for assistance. 10.1.1 Error messages Error Displayed message Probable cause Solution code Release emergency STOP button by turning it clockwise. -
Page 66: Warning Messages
8 and 2 from the above table are relevant, it will be displayed as an A in the warning flag column of the measurement file. If you have any difficulties relating the measurement file warning flags to the codes in the above table, please contact your Hach Lange representative for assistance. -
Page 67: Red Led's On Startup Screen
Switch instrument off, wait 10 seconds and switch back Boards may happen when switching the instrument on. If the LED is still red call Hach Lange service support. No communication between sensor and Check connection of the oxygen sensor. If problem sensor board. -
Page 68: Measurement Problems
Troubleshooting 10.1.4 Measurement problems Observation Explanation Negative TPO results purge gas is not of the required purity of > 99.9% The instrument never reaches the threshold value purge gas is not of the required purity of > 99.9% Stop the analysis by pressing the emergency STOP button. Disconnect instrument from the power supply and remove the bottle. -
Page 69: Section 11 Spare Parts And Accessories
Section 11 Spare Parts and Accessories Part N° Description 2956A-A A1100 cartridge 32912 O2 flow chamber O-ring kit 33001 Power Cord - EU Plug 33002 Power Cord - US Plug 33003 Power Cord - Swiss Plug 33004 Power Cord - UK Plug 33117 Package seal 33122... - Page 70 Spare Parts and Accessories...
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Page 71: Section 12 Material Safety Data Sheets (Msds)
Section 12 Material Safety Data Sheets (MSDS) 12.1 Silicon antifoam (part number 33156) PRODUCT AND COMPANY IDENTIFICATION PRODUCT NAME Silicon antifoam, emulsion, 30% in water COMPANY Hach Lange SA 6 Route de Compois Case Postale 212 CH-1222 Vésenaz, Switzerland PHONE NO. 0041 22 594 64 00... - Page 72 Material Safety Data Sheets (MSDS) PHYSICAL AND CHEMICAL PROPERTIES APPEARANCE Color: White. Form: Turbid viscous liquid Property Value At temperature or pressure 6.5 - 7.5 BP/BP range 100 °C 760 mmHg MP/MP range - 1.0 °C Flash point Flammability Autoignition temp Oxidizing properties Explosive properties Explosion limits...
- Page 73 Material Safety Data Sheets (MSDS) ECOLOGICAL INFORMATION Test Type: LC0 Fish Species: Brachydanio rerio Time: 96 h Value: 180 mg/l Test Type: LC50 Fish Species: Brachydanio rerio Time: 96 h Value: 250 mg/l Test Type: LC100 Fish Species: Brachydanio rerio Time: 96 h Value: 350 mg/l DISPOSAL CONSIDERATIONS...
- Page 74 Material Safety Data Sheets (MSDS)
- Page 76 Tel. +49 (0) 2 11 52 88-320 SWITZERLAND Fax (970) 669-2932 Fax +49 (0) 2 11 52 88-210 Tel. +41 22 594 6400 orders@hach.com info@hach-lange.de Fax +41 22 594 6499 www.hach.com www.hach-lange.de © Hach Lange, 2013. All rights reserved. Printed in Europe.
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