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Varian 1200 GC/MS Pre-Installation Instructions

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NOTICE: Varian, Inc. was acquired by Agilent
Technologies in May 2010. This document is provided
as a courtesy but is no longer kept current and thus
will contain historical references to Varian. For more
information, go to www.agilent.com/chem.
Use this checklist as a guide while preparing your site for the installation of the Varian 1200 or
1200L MS system. Make sure that your site meets all of the requirements detailed in these
instructions before you request installation.
Complete the Checklist
Refer to the appropriate topics in these instructions for more information about each item.
General Requirements
The installation area is in compliance with all
relevant safety regulations
The principle operator will be available during
the installation and certification period
Entrance to the lab is > 100 cm (36 in.)
The workbench can support the load of the
system
Sufficient bench space is available for all
equipment, including optional items
Environmental Requirements
The lab temperature can be maintained
between 15 and 30 ºC
The relative humidity can be maintained
between 40 – 80%
The lab is free of particulate matter
The system workbench is free from vibrations
The system area is free from electromagnetic
disruption and electrostatic discharge
There is a suitable exhaust system
Request Installation
When you have prepared your site in accordance with this checklist, contact the Customer Service
office in your region to schedule installation. Keep this checklist handy and review it with the Field
Representative when arranging the installation.
Please Note: If the laboratory is not ready for installation when the Field Service Representative
arrives, Varian, Inc. reserves the right to invoice for the Representative's time.
Pre-installation Checklist
Varian 1200/1200L Mass Spectrometer
Power Requirements
The specified electrical supply and power
outlets are available
Gas and Solvent Requirements
There is proper gas equipment
HPLC solvents available
Carrier gases are available
Appropriate lab glassware is available
Nitrogen at 99.999% purity
Argon at 99.999% purity
Air at 99.999% purity
Methane at 99.999% purity
n/a
n/a
n/a
n/a
n/a
n/a

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Summary of Contents for Varian 1200 GC/MS

  • Page 1 Varian 1200/1200L Mass Spectrometer Use this checklist as a guide while preparing your site for the installation of the Varian 1200 or 1200L MS system. Make sure that your site meets all of the requirements detailed in these instructions before you request installation.

  • Page 2: Table Of Contents

    Varian 1200 GC/MS, 1200L GC/MS, 1200L LC/MS, or 1200L GC/LC/MS system. Use the general requirements and the appropriate section of these pre-installation instructions as a guide while preparing the installation site.

  • Page 3: General Requirements

    Operating the system at high humidity may produce condensation and result in short circuits. Varian recommends that your laboratory be equipped with a temperature/humidity monitor. This will ensure that your laboratory is always in conformance with temperature and humidity specifications.

  • Page 4: 1200 Gc/Ms

    1200 GC/MS Entrance Before arranging for delivery of the 1200 GC/MS to your facility, please make sure that all passages to the site of installation are at least 36 in. (110 cm) wide. Allow additional room for maneuvering the shipping containers around corners and/or through doors.

  • Page 5: Power Requirements 1200 Gc/Ms

    The 1200 GC/MS system should be installed on a clean, flat surface. The minimum bench space required for the system is 57 cm x 195 cm, for the CP-3800 GC, 1200 MS, and PC: 275 cm if the printer is on the bench as illustrated above. Ensure that the bench is capable of supporting the weight of the system: at least 150 kg plus allowances for any options.

  • Page 6: Gas Requirements 1200 Gc/Ms

    Gas Requirements 1200 GC/MS CI Reagent Gases The CI mode for the 1200 MS typically uses methane, isobutane, or ammonia. The amount of gas consumed during CI operation is approximately 1 to 2 mL/min. The CI reagent gas should contain less than 1 ppm water. The methane, isobutane, or ammonia gas supply line connects directly to the CI gas inlet using 1/8-inch Swagelok®...

  • Page 7: 1200L Gc/Ms

    The presence of greater than 1 ppm oxygen or water in the carrier gas supply may significantly affect the performance of the 1200 GC/MS. It may also damage such components as the capillary column, filaments, and multiplier. Varian recommends that you verify that your gas suppliers use controlled tanks to ensure that purity standards are maintained.

  • Page 8: Power Requirements 1200L Gc/Ms

    Figure 2 Recommended 1200L GC/MS System Layout The 1200L GC/MS system should be installed on a clean, flat surface. The minimum bench space required for the system is 57 cm x 195 cm, for the CP-3800 GC, 1200MS, and PC; 275 cm with the printer.

  • Page 9: Gas Requirements 1200L Gc/Ms

    Table 2 1200L GC/MS Power Requirements Max Current Draw Max Current Draw Instrument 100-115V (Amps) 200-240V (Amps) CP-3800 Gas Chromatograph 1200 Mass Spectrometer Computer Monitor Printer NOTE: See Appendix 2 for complete current supply requirements for the standard modules. The power cable from the GC is approximately 80 in. (2 meters) long and fitted with National Electronics Manufacturers Association (NEMA) 5-20P power plugs.
  • Page 10 The presence of greater than 1 ppm oxygen or water in the carrier gas supply may significantly affect the performance of the 1200 GC/MS. It may also damage such components as the capillary column, filaments, and multiplier. Varian recommends that you verify that your gas suppliers use controlled tanks to ensure that purity standards are maintained.

  • Page 11: 1200L Lc/Ms

    Filter Use of a carrier gas filter is required for optimum performance and to protect your system from potential contamination. Your GC Accessory Kit includes a GC/MS Gas Clean Oxygen/Moisture filter (CP-17973) and filter base. This easy-to-remove gas filter cartridge combines three highly adsorptive materials in one filter to remove water, oxygen, and organic compounds to purify the GC/MS gas.

  • Page 12: Power Requirements 1200L Lc/Ms

    Figure 3 Recommended 1200L LC/MS System Layout The 1200L LC/MS system should be installed on a clean, flat surface. The minimum bench space required for the system is 57 cm x 210 cm for the LC, 1200, and PC, 275 cm with the printer.

  • Page 13: Gas Requirements 1200L Lc/Ms

    0.1 ppm hydrocarbons, and less than 1% oxygen. The nitrogen should be dry, with a −40 degree dew point. Varian recommends the use of a nitrogen generator, or liquid nitrogen blow- off to supply the gas. All nitrogen generators require regular maintenance to continue to perform to specification.

  • Page 14: Solvent Requirements 1200L Lc/Ms

    99% and be regulated to 1−3 psi (0.1−0.2 bar). Solvent Requirements 1200L LC/MS Installation by a Varian Field Service Representative will normally include a basic test of the system’s functionality. Mobile phase solvents required for installation are methanol and de-ionized water. All solvents should be pure HPLC-grade, and degassing apparatus should be available, if required.

  • Page 15: Power Requirements 1200L Gc/Lc/Ms

    NOTE: This figure illustrates North American power requirements (115 Vac). See Table 4 for 230 Vac amperage requirements. Figure 4 Recommended 1200L GC/LC/MS System Layout The 1200L GC/LC/MS system should be installed on a clean, flat surface. The minimum bench space required for the system is 57 cm x 250 cm for the HPLC, 1200, and PC, 325 cm with the printer.

  • Page 16: Gas Requirements 1200L Gc/Lc/Ms

    0.1 ppm hydrocarbons, and less than 1% oxygen. The nitrogen should be dry, with a −40 degree dew point. Varian recommends the use of a nitrogen generator, or liquid nitrogen blow- off to supply the gas. All nitrogen generators require regular maintenance to continue to perform to specification.
  • Page 17 A compressed air gas supply that is capable of providing up to 2L/min regulated to 80 psi is required for negative ESI as a nebulizing gas. It is the customer's responsibility to conform to all regulations regarding the installation and operation of the gas system. The air should be clean and dry, with less than 0.1 ppm total hydrocarbons, including methane, and a –40 degree dew point.
  • Page 18 The presence of greater than 1 ppm oxygen or water in the carrier gas supply may significantly affect the performance of the 1200 GC/MS. It may also damage such components as the capillary column, filaments, and multiplier. Varian recommends that you verify that your gas suppliers use controlled tanks to ensure that purity standards are maintained.

  • Page 19: Solvent Requirements 1200L Lc/Ms

    Solvent Requirements 1200L LC/MS Installation by a Varian Field Service Representative will normally include a basic test of the systems functionality. Mobile phase solvents required for installation are methanol and de-ionized water. All solvents should be pure HPLC-grade, and degassing apparatus should be available, if required.

  • Page 20: Instrument Arrival

    Most systems are shipped FOB Varian, and any damages incurred in shipment are the responsibility of the purchaser and the carrier. Contact the Varian office for assistance with claims filing and billing for repairs if necessary.

  • Page 21: Unpacking And Installation

    Unpacking and Installation Before coming on site for installation, a Varian Field Service Representative will contact you to go through the “Pre-installation Checklist” at the front of this document to ensure that all of the site requirements have been met. The Varian Field Service Representative will unpack and install the 1200L LC/MS or 1200/1200L GC/MS and will demonstrate the fundamental operation and maintenance of the MS.

  • Page 22: Appendix 1. Module Specifications

    The following table identifies the space and weight requirements for Varian MS, LC, and GC components. Varian MS systems are intended to sit on a workbench that is wide enough and deep enough to accommodate these components, and sturdy enough to support their combined weight.

  • Page 23: Appendix 2. Power Consumption

    Table 6 Spatial Setup Recommendations for 1200L LC/MS and GC/MS Recommendations Purpose Recommended Distance Allow adequate space to the side of Solvent bottle placement for ≥ 24 in. (61 cm) the LC. HPLC pumps. See Figure 3. Allow adequate space to the side of Permit access to the transfer ~ 24 in.
  • Page 24 Table 8 Maximum Power Draws for Varian Modules Component 100-115 Vac 200-240 Vac (Amperes) (Amperes) Mass Spectrometer LC/MS Foreline pumps (2 ea. @ 220V) ProStar 210/215 SDM 2.25 1.125 ProStar 220, 230, 240 SDM 2.25 1.125 PrepStar SD-1 SDM PrepStar SD-2 (220V only) SDM 1.65...

  • Page 25: Appendix 3. Nema Plugs And Power Outlets

    Constant high line voltage or surges in voltage may produce overheating and component failures. Constant low line voltage or sags in voltage may cause the system to function erratically, or even to cease functioning. Transients, even of a few microseconds duration, may cause electronic devices to fail catastrophically or degrade sufficiently to significantly shorten device lifetime.

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