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Trace Nitrogen in Argon Analyzer
regulator on the sample inlet. Do not exceed a maximum of
20 psig (138 kPa).
4.5.2.2 R
ECOMMENDED
Teledyne recommends the following gases be used for calibration:
Zero Gas:
Span Gas:
For 0-1 ppm range:
For 0-10 ppm range: 7-10 ppm N
For 0-100 ppm range: 70 – 100 ppm N
The first calibration point is fixed by a zero gas. The most
convenient source of nitrogen-free argon is through an activated
molecular sieve scrubber cooled to liquid oxygen temperatures or a
heated transition metal scrubber. A commercially available scrubber the
Teledyne Part number S1748-120 (or S1748 -240 depending on AC
voltage) is ideal for this. Alternatively, a zero gas cylinder with a low
ppb nitrogen level can be used for zeroing in the low ppm range
specified, as long as the N
The second point is fixed by a certified span gas normally supplied
in a high-pressure cylinder.
4.5.2.3 Z
C
ERO
AL
The ZERO button on the front panel is used to enter the zero
calibration function. Zero calibration can be performed in either the
automatic or manual mode. In the automatic mode, an internal
algorithm compares consecutive readings from the sensor to determine
when the output is within the acceptable range for zero. In the manual
mode, the operator determines when the reading is within the acceptable
range for zero. Make sure the zero gas is connected to the instrument.
See Section 3.6 for gas connections.
After pressing the ZERO button, the mode selection screen appears:
Teledyne Analytical Instruments
C
G
ALIBRATION
ASES
N
-free Ar
2
0.7-1.0 ppm N
in Ar
2
in Ar
2
in Ar (best for overall
2
accuracy on all ranges)
concentration is known.
2
Operation
55
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