Thermo Scientific DSQ II Manuals

Thermo Scientific DSQ II Manuals

Manuals and User Guides for Thermo Scientific DSQ II. We have 2 Thermo Scientific DSQ II manuals available for free PDF download: Hardware Manual, User Manual

Thermo Scientific DSQ II Hardware Manual

Thermo Scientific DSQ II Hardware Manual (242 pages)

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 4 MB

Table of Contents

Table of Contents
9
Basic Operations
17
Chapter 1 Basic Operations

17
Chapter 2 Maintaining the DSQ II

37
Chapter 3 Troubleshooting

137
- Running Tune Diagnostics
  138
- Communication Symptoms
  139
- Contamination Symptoms
  143
- Filament and Lens Control Symptoms
  146
- Heated Zone Symptoms
  148
- High Vacuum Symptoms
  151
- Linearity Symptoms
  154
- Power Supply Symptoms
  155
- RF and DC Control Symptoms
  157
- Sensitivity Symptoms
  160
- Stability Symptoms
  164
- Tuning Symptoms
  165
Chapter 4 Vacuum System and Gas Inlets

169
- Vacuum System
  169
  - Fore Pressure Gauge and Foreline Adapter
    171
  - High Vacuum Pump (Single Turbomolecular Pump)
    172
  - High Vacuum Pump (Split-Flow Turbomolecular Pump)
    173
  - Ion Gauge (Upgrade)
    174
  - Rotary-Vane Pump
    175
  - Vacuum Manifold
    176
- Gas Inlet Components
  178
  - Calibration Gas Flow Module
    179
  - CI Reagent Gas Flow Module (Upgrade)
    180
  - Vent Valve Solenoid
    181
Chapter 5 Ion Source and Inlet Valve

183
- Ion Source
  183
  - Filament
    185
  - Ion Source
    186
  - Ion Volume
    188
  - Lenses
    189
  - Magnets and Magnet Yoke
    190
- Inlet Valve (Upgrade)
  191
  - Ball Valve
    193
  - Inlet Valve Lever
    194
  - Guide Bar Housing
    195
  - I/R Tool and Guide Bar
    196
  - Inlet Valve Plug
    197
  - Inlet Valve Seal
    197
Chapter 6 Prefilter and Quadrupole

199
Chapter 7 Ion Detector

203
- Conversion Dynode
  204
- Electron Multiplier
  205
Chapter a Reordering DSQ II Components

207
- Vacuum Manifold Parts List
  208
- Ion Source Parts List
  210
- Ion Source Parts List
  211
- Lens Assembly Parts List
  213
- Quadrupole Parts List
  214
- Gas Inlets and Gauges Parts List
  215
- Boards and Cables Parts List
  217
- Turbomolecular Pump Parts List
  224
- Split-Flow Turbomolecular Pump (Upgrade) Parts List
  226
- Inlet Valve (Upgrade) Parts List
  228
- Power Module Parts List
  230
- Installation Kit Parts List
  230
- Documentation Parts List
  231
- Miscellaneous Items Parts List
  232
- Electronic Assemblies
  234
- Power Distribution
  235
- Remote Start Cable Connections
  236

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Thermo Scientific DSQ II User Manual

Thermo Scientific DSQ II User Manual (116 pages)

Direct Probe System

Brand: Thermo Scientific | Category: Laboratory Equipment | Size: 3 MB

Table of Contents

Customer Registration Card
3
Reader's Survey
3
Table of Contents
9
Preface
13
Safety Alerts and Special Notices
13
Safety Symbols and Signal Words
14
Contacting Us
15
To Contact Customer Service for Ordering Information
15
To Contact Technical Support
15
Related Documentation
16
To Suggest Changes to Documentation or to Instrument Help
16
Using a Direct Insertion Probe (DIP)
19
How the Direct Probe System Works
20
Analyzing Cholesterol with the Ion Trap Series
22
Step 1: Connect the Direct Probe System
23
Step 2: Change the Ion Volume
25
Step 3: Deselect as and GC Devices
27
Step 4: Tune and Calibrate the Mass Spectrometer
28
Step 5: Program the DPC
28
To Retrieve Methods
29
Step 6: Prepare the Sample
30
Step 7: Create a Method File
30
Step 8: Create a Sequence File
31
Step 9: Insert the Probe Using Xcalibur
33
Step 10: Remove the Probe Using Xcalibur
35
Step 11: Analyze the Data File
36
Analyzing Cholesterol with the DSQ Series
38
Step 1: Connect the Direct Probe System
39
Step 2: Change the Ion Volume
41
Step 3: Deselect as and GC Devices
43
Step 4: Tune and Calibrate the Mass Spectrometer
44
Step 5: Program the DPC
44
Step 6: Prepare the Sample
46
Step 7: Create a Method File
46
To Retrieve Methods
46
Step 8: Create a Sequence File
47
Step 9: Insert the Probe Using Xcalibur
49
Step 10: Remove the Probe Using Xcalibur
51
Step 11: Analyze the Data File
52
Loading DIP Samples
53
Loading Liquid Samples
54
Cleaning the DIP
55
Loading Solid Samples
55
DIP Modes
56
Top Terms to Know
56
Probe Shaft
57
Probe Tip
57
Sample Cups
57
Hints
58
Top Safeguards to Know
58
Using a Direct Exposure Probe (DEP)
61
How the Direct Probe System Works
62
Analyzing Cholesterol with the Ion Trap Series
64
Step 1: Connect the Direct Probe System
65
Step 2: Change the Ion Volume
66
Step 3: Deselect as and GC Devices
68
Step 4: Tune and Calibrate the Mass Spectrometer
69
Step 5: Program the DPC
69
To Retrieve Methods
70
Step 6: Prepare the Sample
71
Step 7: Create a Method File
72
Step 8: Create a Sequence File
73
Step 9: Insert the Probe Using Xcalibur
75
Step 10: Remove the Probe Using Xcalibur
77
Step 11: Analyze the Data File
78
Analyzing Cholesterol with the DSQ Series
80
Step 1: Connect the Direct Probe System
81
Step 2: Change the Ion Volume
82
Step 3: Deselect as and GC Devices
84
Step 4: Tune and Calibrate the Mass Spectrometer
85
Step 5: Program the DPC
85
To Retrieve Methods
86
Step 6: Prepare the Sample
87
Step 7: Create a Method File
88
Step 8: Create a Sequence File
89
Step 9: Insert the Probe Using Xcalibur
90
Step 10: Remove the Probe Using Xcalibur
92
Step 11: Analyze the Data File
93
Loading DEP Samples
94
Loading Liquid Samples
95
Cleaning the DEP
96
Loading Solid Samples
96
DEP Modes
99
Top Terms to Know
99
Probe Shaft
100
Probe Tip
100
Top Safeguards to Know
100
Hints
101
Chapter 3 Getting Help

103
- Who to Call
  104
- Technical Support
  104
- Customer Service
  104
- Spare Parts
  104
- Technical Publications Editor
  104
- Detuning the Instrument
  105
- Getting Spare Parts
  107
- Abbreviations
  111
- Index
  115

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