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Gamry Instruments Reference 3000 Manuals
Manuals and User Guides for Gamry Instruments Reference 3000. We have
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Gamry Instruments Reference 3000 manual available for free PDF download: Operator's Manual
Gamry Instruments Reference 3000 Operator's Manual (106 pages)
Potentiostat/Galvanostat/ZRA
Brand:
Gamry Instruments
| Category:
Laboratory Equipment
| Size: 7.2 MB
Table of Contents
If You Have Problems
3
Limited Warranty
3
Copyrights
4
Disclaimers
4
Table of Contents
5
Chapter 1: Safety Considerations
9
Inspection
9
Product Safety
9
AC Mains Connection to the Power Brick
9
Grounding in the Reference 3000
10
Operation with Earth-Grounded Cells and Auxiliary Apparatus
11
Temperature and Ventilation
12
Defects and Abnormal Stresses
12
Environmental Limits
12
Cleaning
13
Service
13
RFI Warning
13
Electrical Transient Sensitivity
13
CE Compliance
14
Rohs Compliance
14
Chapter 2: Introduction
15
About this Manual
15
About the Reference 3000
15
About the Auxiliary Electrometer Option
16
Notational Conventions
16
Chapter 3: Instrument Circuitry
17
Reference 3000 Schematic/Block Diagrams
17
Chapter 4: Installation
27
Initial Visual Inspection
27
Physical Location
28
Computer Requirements
28
Quick-Start Guide for System Installation
29
Software Installation
29
Reboot Your Computer after Software Installation
29
Power Cord and Power Connection
30
Power-Up Test
31
USB Cables
31
Front Panel USB LED
31
First-Time Device Installation in Windows
32
Running the Framework
32
Framework Device Status Bar
32
Gamry Instrument Manager
33
Changing the Label
34
Firmware Update
35
Chapter 5: Calibration
37
Introduction
37
DC and AC Calibration
37
Low I Range DC Calibration
38
Cable Calibration
39
Procedure to Calibrate the Cable
40
Chapter 6: Cell Connections
43
Cell Cable Overview
43
Ancillary Apparatus
43
AE Connections
43
Fuses in the Cell Cable
43
Normal Cell Connections
43
ZRA Mode Cell Connections
45
Stack Mode Cell Connections
46
Membrane Cell Connections
46
Fuses in the Cell Cable
47
In-Line Fuse-Holders and Fuses
47
Fuses Located in the Cable Hood
48
Testing for Open Fuses
50
Chapter 7: Panel Indicators and Connectors
53
Front Panel
53
Counter/Working Connector
53
Sense Inputs Connector
54
Power LED
54
Usb Led
56
Cell on LED
56
Overload LED
56
Rear Panel
58
Power in Jack
58
Power Switch
59
Chassis Ground
60
USB Port
60
Thermocouple Input
61
Misc. I/O Connector
61
I Monitor BNC
62
E Monitor BNC
63
Ext. Sig. in BNC
63
Sig Gen. out BNC
64
Aux. in BNC
64
Expansion Interface
64
Chapter 8: Auxiliary Electrometer Option
65
Overview
65
AC Performance and CMRR
65
Experiments
66
Connections Using Standard Cables
66
Connections Using Custom Cables
67
AE Specifications
67
Chapter 9: Stability in Potentiostat Mode
69
Capacitive Cells and Stability
69
Improving Potentiostat Stability
69
Chapter 10: Measurement of Small-Current Signals
73
Overview
73
Description of the Problem
73
Measurement System Model and Physical Limitations
73
Johnson Noise in Z Cell
74
Finite Input Capacitance
75
Leakage Currents and Input Impedance
75
Voltage Noise and DC Measurements
76
Shunt Resistance and Capacitance
76
Hints for System and Cell Design
77
Faraday Shield
77
Avoid External Noise Sources
77
Cell Cable Length and Construction
77
Lead Placement
78
Cell Construction
78
Reference Electrode
78
Instrument Settings
78
EIS Speed
79
Ancillary Apparatus
79
Floating Operation
79
Chapter 11: EIS Measurement of Small Impedances
81
Overview
81
Why Galvanostatic Mode
81
DC Errors and Four-Terminal Measurements
81
What Is Mutual Inductance
82
Avoid High Frequencies
83
Minimize the Net Magnetic Field
83
Separate the Pairs
83
Twist the Sense Wires
84
How Should You Hook up Your Cell
84
Appendix A: Reference 3000 Specifications
85
Control Amplifier
85
Differential Electrometer
85
Voltage Measurement
86
Current-To-Voltage Converter
86
Current Measurement
86
Potentiostatic Mode
87
Galvanostatic Mode
87
Auxiliary A/D Input (See
87
Auxiliary A/D Input (See Appendix D)
87
Auxiliary D/A Output
87
Environmental
87
General
88
Appendix B: Reference 3000 Cell Connectors
91
Appendix C: Misc. I/O Connector
93
Appendix D: Auxiliary A/D Input Characteristics
95
Overview
95
Jumper Identification
95
Input Impedance Selection
96
Bandwidth Selection
96
Aux A/D Specifications
96
Function Call to Set the Aux A/D BNC Characteristics
96
Appendix E: Auxiliary Electrometer Specifications
97
DC Voltage Measurement
97
Input Impedance
97
Common Mode Rejection
97
Crosstalk
97
Other AC Specifications
97
Appendix F: Power LED Blink Codes
99
Normal Start-Up
99
Failure in an Electronics Module
99
Severe Problem
99
Appendix G: Certifications
101
Declaration of Conformity: No. DOC-2009-CE-REF3000
101
Certificate of Conformance
102
Declaration of Conformity: No. DOC-2021-UKCA-REF3000
103
Appendix H: Comprehensive Index
105
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