Related Manuals for Hanna Instruments HI 83200
Summary of Contents for Hanna Instruments HI 83200
- Page 1 Instruction Manual HI 83200 Multiparameter Bench Photometer for Laboratories This Instrument is in w w w . h a n n a i n s t . c o m Compliance with the CE Directives...
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Page 2: Table Of Contents
Dear Customer, PRELIMINARY EXAMINATION Thank you for choosing a Hanna product. Please read this instruction manual carefully before using the instrument. This manual will provide you with the necessary information for the correct use of the Please examine this product carefully. Make sure that the instrument is not damaged. If any damage occurred during shipment, please notify your Dealer. -
Page 3: Specifications
Where: SPECIFICATIONS -log I/I =Absorbance (A) =intensity of incident light beam Light Life Life of the instrument I =intensity of light beam after absorption Light Detector Silicon Photocell ε =molar extinction coefficient at wavelength λ λ Environment 0 to 50°C (32 to 122°F); =molar concentration of the substance max 90% RH non-condensing =optical path through the substance... -
Page 4: Functional Description
KEYPAD DESCRIPTION FUNCTIONAL DESCRIPTION The keypad contains 8 direct keys and 3 functional keys with the following functions: INSTRUMENT DESCRIPTION Press to perform the function displayed above it. The functions are screen related. Press to exit the current screen. Press to access the select method menu. Press to move up in a menu or a help screen, to increment a set value, to access second level functions. -
Page 5: Tips For An Accurate Measurement
USING LIQUID AND POWDER REAGENTS TIPS FOR AN ACCURATE MEASUREMENT • Proper use of the dropper: The instructions listed below should be carefully followed during testing to ensure most accurate results. (a) for reproducible results, tap the dropper on the table for several times and wipe the outside of the dropper tip with a cloth. -
Page 6: Health & Safety
Pay attention to push the cuvette completely down in the holder. HEALTH & SAFETY The chemicals contained in the reagent kits may be hazardous if improperly handled. Read the Material Safety Data Sheet (MSDS) before performing tests. Safety equipment: Wear suitable eye protection and clothing when required, and follow instructions carefully. Reagent spills: If a reagent spill occurs, wipe up immediately and rinse with plenty of water. -
Page 7: Operational Guide
• After the desired method was selected, follow the measurement described in the related section. OPERATIONAL GUIDE • Before performing a test you should read all the instructions carefully. POWER CONNECTION AND BATTERY MANAGEMENT DATA MANAGEMENT The meter can be powered from an AC/DC adapter (included) or from the built-in rechargeable battery. The instrument features a data log function to help you keep track of all your analysis. -
Page 8: Setup
Date / Time S E T U P S E T U P S E T U P S E T U P S E T U P This option is used to set the instrument’s date and time. In the Setup mode the instrument’s parameters can be changed. Some parameters affect the measuring sequence and Press Modify functional key to change the date/time. -
Page 9: Help Mode
Instrument ID SAMPLE PREPARATION Option: 0 to 9999. This option is used to set the instrument’s ID (identification number). LIST OF MATERIAL The instrument ID is used while exchanging data with a PC. HI 83200 is supplied with the following accessories for sample preparation: Press Modify functional key to access the instrument ID screen. - Page 10 • Mix well using the spoon and then wait for 5 minutes. • Remove the cap and fill the Demineralizer Bottle with tap water. • Replace the cap and shake gently for at least 2 minutes. filter • Unscrew the filter assembly, put a filter disc inside and close disc •...
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Page 11: Aluminum
Note: To measure exactly 5 mL of sample with the syringe, push the plunger completely into the syringe ALUMINUM and insert the tip into the sample. Pull the plunger out until the lower edge of the seal is on the 5 mL mark of the syringe. -
Page 12: Alkalinity
• Add the content of one packet of HI 93712C-0 Bleaching ALKALINITY powder to one of the two cuvettes. Replace the cap and shake vigorously until completely dissolved. This is the blank. SPECIFICATIONS Range 0 to 500 mg/L (as CaCO Resolution 5 mg/L •... -
Page 13: Ammonia Mr
• Remove the cuvette. AMMONIA MEDIUM RANGE • Add carefully the content of one packet of HI 93755-0 Alkalinity SPECIFICATIONS Indicator Reagent. Replace the cap and shake vigorously for 30 Range 0.00 to 10.00 mg/L seconds. Note: Pay attention not to spill reagent otherwise full color Resolution 0.01 mg/L Accuracy... -
Page 14: Ammonia Lr
• Remove the cuvette. AMMONIA LOW RANGE SPECIFICATIONS • Add 4 drops of HI 93715A-0 First Reagent (6 drops for seawater Range 0.00 to 3.00 mg/L analysis). Replace the cap and mix the solution. Resolution 0.01 mg/L Accuracy ±0.04 mg/L ±4% of reading Typical EMC ±0.01 mg/L Deviation... -
Page 15: Bromine
• Remove the cuvette. BROMINE SPECIFICATIONS • Add 4 drops of HI 93700A-0 First Reagent (6 drops for seawater Range 0.00 to 8.00 mg/L analysis). Replace the cap and mix the solution. Resolution 0.01 mg/L Accuracy ±0.08 mg/L ±3% of reading Typical EMC ±0.01 mg/L Deviation... -
Page 16: Calcium
• Remove the cuvette and add the content of one packet of HI 93716-0 CALCIUM DPD reagent. Replace the cap and shake gently for about 20 seconds to dissolve most of the reagent. SPECIFICATIONS Range 0 to 400 mg/L Resolution 10 mg/L Accuracy ±10 mg/L ±5% of reading... -
Page 17: Free Chlorine
• Replace the cap and invert several times to mix. FREE CHLORINE FREE CHLORINE FREE CHLORINE FREE CHLORINE FREE CHLORINE FREE CHLORINE • Place the cuvette into the holder and close the lid. SPECIFICATIONS • Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. - Page 18 • Press ZERO key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement. • Reinsert the cuvette into the instrument. • Press READ to start the reading. The instrument displays the results • Remove the cuvette. in mg/L of free chlorine.
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Page 19: Total Chlorine
• Press ZERO key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement. TOTAL CHLORINE SPECIFICATIONS Range 0.00 to 3.50 mg/L Resolution 0.01 mg/L Accuracy ±0.03 mg/L ±3% of reading • Remove the cuvette. Typical EMC ±0.01 mg/L Powder reagents procedure Deviation... -
Page 20: Chlorine Dioxide
• Press TIMER and the display will show the countdown prior to the measurement or, alternatively, wait CHLORINE DIOXIDE for 2 minutes and 30 seconds and press READ. When the timer ends the meter will perform the reading. SPECIFICATIONS Range 0.00 to 2.00 mg/L Resolution 0.01 mg/L... - Page 21 • Add the content of one packet of HI 93738B-0 Dechlorinating Reagent to one of the two cylinders • Press ZERO key. The meter will show “-0.0-” when the meter is zeroed and ready for measurement. (#1), close and invert it several times until it is totally dissolved. This is the blank. •...
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Page 22: Chromium Vi Hr
CHROMIUM VI HIGH RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0 to 1000 µg/L • Press TIMER and the display will show the countdown prior to the Resolution 1 µg/L measurement or, alternatively, wait for 6 minutes and press READ. Accuracy ±5 µg/L ±4% of reading When the timer ends the meter will perform the reading. -
Page 23: Chromium Vi Lr
CHROMIUM VI LOW RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS • Press TIMER and the display will show the countdown prior to the Range 0 to 300 µg/L measurement or, alternatively, wait for 6 minutes and press Resolution 1 µg/L READ. -
Page 24: Color Of Water
• Fill the second cuvette up to the mark with unfiltered sample and COLOR OF WATER 10 mL replace the cap. This is the apparent color. SPECIFICATIONS Range 0 to 500 PCU (Platinum Cobalt Units) • Filter 10 mL of sample through a filter with a 0.45 µm membrane into the Resolution 1 PCU third cuvette, up to the 10 mL mark and replace the cap. -
Page 25: Copper Hr
• Remove the cuvette. COPPER HIGH RANGE • Add the content of one packet of HI 93702-0 Bicinchoninate. Replace SPECIFICATIONS the cap and shake gently for about 15 seconds. Range 0.00 to 5.00 mg/L Resolution 0.01 mg/L Accuracy ±0.02 mg/L ±4% of reading Typical EMC ±0.01 mg/L Deviation... -
Page 26: Copper Lr
• Remove the cuvette. COPPER LOW RANGE • Add the content of one packet of HI 93747-0 Bicinchoninate. SPECIFICATIONS Replace the cap and shake gently for about 15 seconds. Range 0 to 1000 μg/L Resolution 1 μg/L Accuracy ±10 μg/L ±5% of reading Typical EMC ±1 μg/L Deviation... -
Page 27: Cyanide
Note: Pay attention to the way the spoon is filled: CYANIDE - do not press the powder; SPECIFICATIONS - do not overfill it. Range 0.000 to 0.200 mg/L Resolution 0.001 mg/L Accuracy ±0.005 mg/L ±3% of reading • Place the HDPE plastic stopper and cap immediately, to prevent the Typical EMC Dev. -
Page 28: Cyanuric Acid
• Press the to access the second level of functions. CYANURIC ACID • Press the Chem Frm functional key to convert the result in mg/L of Potassium Cyanide (KCN). SPECIFICATIONS Range 0 to 80 mg/L Resolution 1 mg/L ±1 mg/L ±15% of reading Accuracy Typical EMC ±1 mg/L... -
Page 29: Fluoride
• Fill a second cuvette with 10 mL of the reacted sample up to the FLUORIDE 10 mL mark. Replace the cap. SPECIFICATIONS Range 0.00 to 2.00 mg/L Resolution 0.01 mg/L ±5% of reading Accuracy • Reinsert the cuvette into the instrument. Typical EMC ±0.01 mg/L Deviation... -
Page 30: Calcium Hardness
• Press TIMER and the display will show the countdown prior to zeroing the blank or, alternatively, wait CALCIUM HARDNESS for two minutes and press ZERO. The display will show “-0.0-” when the meter is zeroed and ready for measurement. SPECIFICATIONS Range 0.00 to 2.70 mg/L... - Page 31 • Press the Unit functional key to change the current measurement unit. The results can be converted to French degrees (°f), German degrees (°dH) and English degrees (°E). • Add 1 drop of HI 93720C-0 EGTA solution to one cuvette (# 1), replace the cap and invert the cuvette several times to mix.
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Page 32: Magnesium Hardness
MAGNESIUM HARDNESS 10 mL 10 mL • Fill both cuvettes up to the 10 mL mark. SPECIFICATIONS Range 0.00 to 2.00 mg/L Resolution 0.01 mg/L • Add 1 drop of HI 93719C-0 EDTA solution to one cuvette (# 1), Accuracy ±0.11 mg/L ±5% of reading replace the cap and invert the cuvette several times to mix. -
Page 33: Hydrazine
• Press the to access the second level of functions. HYDRAZINE • Press the Chem Frm functional key to convert the result in mg/L of Magnesium (Mg). SPECIFICATIONS Range 0 to 400 µg/L Resolution 1 µg/L Accuracy ±4% of full scale Typical EMC ±2 µg/L •... -
Page 34: Iodine
IODINE SPECIFICATIONS Range 0.0 to 12.5 mg/L • Add 12 drops of the HI 93704-0 reagent to each Resolution 0.1 mg/L x 12 x 12 cuvette. Replace the caps and shake gently to mix. Accuracy ±0.1 mg/L ±5% of reading Typical EMC ±0.1 mg/L Deviation... -
Page 35: Iron Hr
IRON HIGH RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0.00 to 5.00 mg/L Resolution 0.01 mg/L Accuracy ±0.04 mg/L ±2% of reading • Press TIMER and the display will show the countdown prior to the measurement or, alternatively, wait Typical EMC ±0.01 mg/L for 2 minutes and 30 seconds and press READ. -
Page 36: Iron Lr
IRON LOW RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0 to 400 µg/L • Press TIMER and the display will show the countdown Resolution 1 µg/L prior to the measurement or, alternatively, wait for 3 Accuracy ±10 µg/L ±8% of reading minutes and press READ. - Page 37 INTERFERENCES • Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. Interference may be caused by: Cadmium above 4.0 mg/L Chromium above 0.25 mg/L Chromium above 1.2 mg/L Cobalt above 0.05 mg/L Copper above 0.6 mg/L Cyanide above 2.8 mg/L Manganese above 50.0 mg/L...
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Page 38: Magnesium
MAGNESIUM • Remove the cuvette. 0.5 mL SPECIFICATIONS of sample Range 0 to 150 mg/L • Using the other 1 mL syringe, add to the cuvette exactly 0.5 mL of sample. Resolution 5 mg/L Note: Do not mix up the two syringes! Accuracy ±5 mg/L ±3% of reading Light Source... -
Page 39: Manganese Hr
MANGANESE HIGH RANGE • Add the content of one packet of HI 93709B-0 Sodium Periodate reagent. Replace the cap and shake gently until completely dissolved. SPECIFICATIONS Range 0.0 to 20.0 mg/L Resolution 0.1 mg/L Accuracy ±0.2 mg/L ±3% of reading •... -
Page 40: Manganese Lr
MANGANESE LOW RANGE • Add 0.2 mL of the HI 93748B-0 Alkaline-cyanide reagent SPECIFICATIONS solution to each cuvette, replace the caps and shake gently. Range 0 to 300 µg/L Resolution 1 µg/L Accuracy ±2 µg/L ±3% of reading Typical EMC ±1 µg/L Deviation Light Source... -
Page 41: Molybdenum
• Press READ to start the reading. The instrument displays the results in µg/L of manganese. MOLYBDENUM SPECIFICATIONS Range 0.0 to 40.0 mg/L Resolution 0.1 mg/L Accuracy ±0.3 mg/L ±5% of reading • Press the to access the second level of functions. Typical EMC ±0.1 mg/L •... - Page 42 • Press TIMER and the display will show the countdown prior to the measurement or, alternatively, wait for five minutes and press READ. When the timer ends the meter will perform the reading. The • Fill one graduated mixing cylinder up to the 25 mL instrument displays concentration in mg/L of molybdenum.
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Page 43: Nickel Hr
• Reinsert the cuvette into the instrument. NICKEL HIGH RANGE • Press TIMER and the display will show the countdown prior SPECIFICATIONS to the measurement or, alternatively, wait for 1 minute and Range 0.00 to 7.00 g/L press READ. When the timer ends the meter will perform the Resolution 0.01 g/L reading. -
Page 44: Nickel Lr
• Press TIMER and the display will show a countdown prior to adding reagent C or, alternatively, wait NICKEL LOW RANGE for 15 minutes. Add one packet of HI 93740C-0 EDTA reagent to each beaker, cap and swirl to mix until completely dissolved. -
Page 45: Nitrate
INTERFERENCES NITRATE Interference may be caused by: must not be present SPECIFICATIONS must not be present Range 0.0 to 30.0 mg/L above 32 mg/L Resolution 0.1 mg/L above 1000 mg/L (as CaCO Accuracy ±0.5 mg/L ±10% of reading above 20 mg/L Typical EMC ±0.1 mg/L Deviation... -
Page 46: Nitrite Hr
NITRITE HIGH RANGE • Replace the cap and immediately shake vigorously up and down for exactly 10 seconds. Continue to mix by SPECIFICATIONS inverting the cuvette gently for 50 seconds, while taking Range 0 to 150 mg/L care not to induce air bubbles. Powder will not com- Resolution 1 mg/L pletely dissolve. -
Page 47: Nitrite Lr
NITRITE LOW RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0.00 to 0.35 mg/L • Press TIMER and the display will show the countdown prior Resolution 0.01 mg/L to the measurement or, alternatively, wait for 10 minutes Accuracy ±0.02 mg/L ±4% of reading and press READ. -
Page 48: Dissolved Oxygen
DISSOLVED OXYGEN • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0.0 to 10.0 mg/L • Press TIMER and the display will show the countdown prior Resolution 0.1 mg/L to the measurement or, alternatively, wait for 6 minutes ±0.4 mg/L ±3% of reading Accuracy and press READ. -
Page 49: Ozone
OZONE • Let the sample stand and the flocculent agent will start to settle. SPECIFICATIONS x 10 • After approximately 2 minutes, when the upper half of the bottle becomes Range 0.00 to 2.00 mg/L limpid, add 10 drops of HI 93732C-0. Resolution 0.01 mg/L Precision... - Page 50 • Press ZERO key. The display will show “-0.0-” the meter is zeroed and ready for measurement. • Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. • Remove the cuvette. • Remove the cuvette. •...
- Page 51 • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 6.5 to 8.5 pH Resolution 0.1 pH • Press the READ key to start the reading. The instrument displays ±0.1 pH Accuracy the pH value. Typical EMC ±0.1 pH Deviation Light Source Tungsten lamp with narrow band interference filter @ 525 nm Method Adaptation of the Phenol Red method.
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Page 52: Phosphate Hr
• Add the content of one packet of HI 93717B-0 Phosphate PHOSPHATE HIGH RANGE HR Reagent B to the cuvette. Replace the cap and shake gently until completely dissolved. SPECIFICATIONS Range 0.0 to 30.0 mg/L Resolution 0.1 mg/L • Reinsert the cuvette into the instrument. Accuracy ±1 mg/L ±4% of reading Typical EMC Dev. -
Page 53: Phosphate Lr
PHOSPHATE LOW RANGE • Reinsert the cuvette into the instrument. SPECIFICATIONS Range 0.00 to 2.50 mg/L Resolution 0.01 mg/L • Press TIMER and the display will show the countdown prior to the Accuracy ±0.04 mg/L ±4% of reading measurement or, alternatively, wait for 3 minutes and press READ. Typical EMC Dev. -
Page 54: Phosphorus
• Add the content of one packet of HI 93706B-0 Phosphorus PHOSPHORUS Reagent B (Amino Acid) to the cuvette. Replace the cap and shake gently until completely dissolved. SPECIFICATIONS Range 0.0 to 15.0 mg/L Resolution 0.1 mg/L • Reinsert the cuvette into the instrument. Accuracy ±0.3 mg/L ±4% of reading Typical EMC Dev. -
Page 55: Potassium Hr
• Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. POTASSIUM HIGH RANGE SPECIFICATIONS Range 20 to 200 mg/L Resolution 5 mg/L Accuracy ±30 mg/L ±7% of reading Typical EMC ±5 mg/L •... -
Page 56: Potassium Mr
INTERFERENCES POTASSIUM MEDIUM RANGE Interferences may be caused by: Ammonium above 10 ppm SPECIFICATIONS Calcium above 10000 ppm as CaCO Range 10 to 100 mg/L Chloride above 12000 ppm Resolution 2.5 mg/L Magnesium above 8000 ppm as CaCO Accuracy ±15 mg/L ±7% of reading Sodium above 8000 ppm Typical EMC ±2.5 mg/L... -
Page 57: Potassium Lr
• Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. POTASSIUM LOW RANGE SPECIFICATIONS Range 0.0 to 20.0 mg/L Resolution 0.5 mg/L Accuracy ±3.0 mg/L ±7% of reading • Remove the cuvette and add the content of one packet of HI 93750B-0 reagent. -
Page 58: Silica
• Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. SILICA SPECIFICATIONS Range 0.00 to 2.00 mg/L Resolution 0.01 mg/L Accuracy ±0.03 mg/L ±3% of reading • Remove the cuvette and add the content of one packet of Typical EMC ±0.01 mg/L HI 93750B-0 reagent. - Page 59 INTERFERENCES • Place the cuvette into the holder and close the lid. Interference may be caused by: Phosphate above 60 mg/L • Press ZERO key. The display will show “-0.0-” when the Phosphate above 75 mg/L meter is zeroed and ready for measurement. Sulfide and high concentration of iron Eliminate color and turbidity interferences by zeroing the meter with the original water sample.
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Page 60: Silver
SILVER SPECIFICATIONS • Add exactly 1.0 mL of HI 93737B-0 Buffer reagent to the second beaker Range 0.000 to 1.000 mg/L (the sample) and swirl gently to mix. Resolution 0.001 mg/L Accuracy ±0.005 mg/L ±10% of reading Typical EMC ± 0.001 mg/L Deviation Light Source Tungsten lamp with narrow band interference filter @ 575 nm. -
Page 61: Sulfate
• Press ZERO key. The display will show “-0.0-” when the meter is zeroed and ready for measurement. SULFATE SPECIFICATIONS Range 0 to 150 mg/L Resolution 5 mg/L Accuracy ±5 mg/L ±3% of reading Light Source Tungsten lamp with narrow band interference filter @ 466 nm Method Sulfate is precipitated with barium chloride crystals. -
Page 62: Zinc
ZINC • Add the content of one packet of HI 93751-0 SPECIFICATIONS Indicator reagent. 1’ Range 0.00 to 3.00 mg/L Resolution 0.01 mg/L • Replace the cap and shake gently for 1 minute. Accuracy ±0.03 mg/L ±3% of reading Typical EMC ±0.01 mg/L Deviation •... -
Page 63: Errors And Warnings
ERRORS AND WARNINGS • Place the cap and insert the cuvette into the instrument and close the lid. • Press ZERO key. The display will show “-0.0-” when the The instrument shows clear warning messages when erroneous conditions appear and when measured values are meter is zeroed and ready for measurement. -
Page 64: Data Management
DATA MANAGEMENT STANDARD METHODS Description Range Method The analyzed data can be managed using Hanna’s product HI92000, Windows Compatible Software. ® Aluminum 0.00 to 1.00 mg/L Aluminon Alkalinity 0 to 500 mg/L Colorimetric Ammonia MR 0.00 to 10.00 mg / L Nessler Ammonia LR 0.00 to 3.00 mg / L... -
Page 65: Accessories
HI 93721-01 100 iron HR tests ACCESSORIES HI 93721-03 300 iron HR tests HI 93722-01 100 cyanuric acid tests REAGENT SETS HI 93722-03 300 cyanuric acid tests HI 93700-01 100 ammonia LR tests HI 93723-01 100 chromium VI HR tests HI 93700-03 300 ammonia LR tests HI 93723-03 300 chromium VI HR tests HI 93701-01 100 free chlorine tests (powder) -
Page 66: Warranty
(20 pcs) HI 740157 If the instrument is to be returned to Hanna Instruments, first obtain a Returned Goods Authorization Number HI 740220 25 mL glass cylinders with caps (2 pcs) HI 740223 170 mL plastic beaker from the Customer Service Department and then send it with shipment costs prepaid. - Page 67 SALES AND TECHNICAL SERVICE CONTACTS Australia: Tel. (03) 9769.0666 • Fax (03) 9769.0699 e-mail: hannains@hannainst.com.au China: Tel. (10) 88570068 • Fax (10) 88570060 e-mail: hannachina@vip.sina.com Egypt: Tel. & Fax (02) 2758.683 e-mail: hannaegypt@go.com.eg Germany: Tel. (07851) 9129-0 • Fax (07851) 9129-99 e-mail: hannager@aol.com Greece: Tel.
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