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Summary of Contents for Thermo Scientific 1371 Series
- Page 1 Thermo Scientific Barnstead Nanopure ™ TOC - Analytical Ultrapure Water System Series 1371 and 1379 Operating Manual and Parts List LT1371X1 Rev. 1 _________________________________________________________________________________ Part of Thermo Fisher Scientific...
- Page 2 Voltage D11941 (7147) 90-240V D12411 (7151) 100-240V MANUAL NUMBER LT1371X1 (7007147) 26925 3/10/11 Decreased water pressure rating in Specifications from 100 to 80 psi 7/22/10 Transfer to Marietta (was LT1371X1 3/8/10) ECR/ECN DATE DESCRIPTION Thermo Scientific Nanopure TOC - Analytical...
- Page 3 Thermo Fisher Scientific makes no representations or warranties with respect to this manual. In no event shall Thermo be held liable for any damages, direct or incidental, arising out of or related to the use of this manual. ©2010 Thermo Fisher Scientific. All rights reserved. Nanopure TOC - Analytical Thermo Scientific...
- Page 4 Always use the proper protective equipment (clothing, gloves, goggles, etc.) 4 Always dissipate extreme cold or heat and wear protective clothing. 4 Always follow good hygiene practices. 4 Each individual is responsible for his or her own safety. Thermo Scientific Nanopure TOC - Analytical...
- Page 5 We can also provide you with a quotation on our Extended Warranty for your Thermo Scientific products. Whatever Thermo Scientific products you need or use, we will be happy to discuss your applications. If you are experiencing technical problems, working together, we will help you locate the problem and, chances are, correct it yourself...over the telephone without a service...
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Page 6: Table Of Contents
Dispensing Water ........8-2 Thermo Scientific... - Page 7 Wiring Diagram ........14-5 Nanopure TOC - Analytical Thermo Scientific...
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Page 8: Safety Information
Safety Information Section 1 Your Thermo Scientific Barnstead Nanopure TOC - Analytical ultrapure water system has been designed with function, reliability, and safety in mind. It is your responsibility to install it in conformance with local electrical codes. This manual contains important operating and safety information. - Page 9 6. Carefully follow manufacturer’s safety instructions on labels of chemical containers and material safety data sheets. 7. Depressurize system prior to removing the cartridge pack. 8. Refer servicing to qualified personnel. 9. A full cartridge pack may weigh about 20 lbs. Nanopure TOC - Analytical Thermo Scientific...
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Page 10: Introduction
Introduction Section 2 Congratulations on your purchase of a Thermo Scientific Barnstead Nanopure TOC - Analytical ultrapure water system. This water purification system is designed to provide low TOC, high resistivity, reagent grade water that exceeds ASTM Type I, ISO 3696 and CLSI- CLRW Type I standards. -
Page 12: General Specifications
Cycle Time ....< 3.5 minutes Water Consumption ..< 15 ml per cycle Min. Water Resistivity ..> 10 MΩ for specified accuracy Thermo Scientific Nanopure TOC - Analytical... - Page 13 Measurement, Control and Laboratory Use; Part I: General Requirements per the provisions of the Electromagnetic Compatibility Directive 2004/108/EC, and per the provisions of the Low Voltage Directive 2006/95/EC. Copies of the Declaration of Conformity are available upon request. Nanopure TOC - Analytical Thermo Scientific...
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Page 14: Unpacking
Plug Adapter ......CEX42 Power Cords Also required for installation: * Customer Supplied Fasteners to mount unit and remote display. Thermo Scientific Nanopure TOC - Analytical... -
Page 16: Installation
This device contains components which may ignite such materials. Note The outlet of a gravity feed storage reservoir must be above or at the same level as the inlet of the Nanopure TOC - Analytical. Thermo Scientific Nanopure TOC - Analytical... -
Page 17: Wall Mounting
Note The outlet of a gravity feed storage reservoir must be above or at the same level as the inlet of the Nanopure TOC - Analytical. Nanopure TOC - Analytical Thermo Scientific... -
Page 18: Install Control Panel In A Remote Location
2. Slide the control panel upward about 1/4” (.64 cm) to 3/8” (.95 cm) - (just enough to clear connector on top cover), pull forward, and remove. (The control panel fits tightly in the unit so it may be difficult to remove.) Thermo Scientific Nanopure TOC - Analytical... - Page 19 7. Tighten the cable screws on each end to secure the cable to the unit and control panel. 8. The control panel may now be mounted on the wall. Nanopure TOC - Analytical Thermo Scientific...
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Page 20: Atmospheric Drain Connection
Ensure there are no kinks in the tubing and that it proceeds in a downward plane. Proceed to “Initial Operation.” Note To prevent leaking, push the tubing into the atmospheric drain connection until it bottoms out. Thermo Scientific Nanopure TOC - Analytical... -
Page 21: Tubing Installation
4. To remove tubing, push collet toward fitting body and pull on tubing. To reuse fitting, begin assembly at Step 1. COLLET TYPICAL TUBING FITTING Figure 5-5. Tubing Adapter Installation Figure 5-6. Tubing Removal Nanopure TOC - Analytical Thermo Scientific... -
Page 22: Electrical Connections
Before connecting the power cord to the power module, install the proper fuses in the fuse holder. Refer to Power switch Figure 5-7. Power cord Figure 5-7. Electrical Connections Thermo Scientific Nanopure TOC - Analytical... -
Page 24: Controls
LED is not illuminated: System is OFF or in (Idle) mode. • Solid Green LED: System is recirculating and operating normally. • Blinking Green LED: System is in Standby mode. • Red LED: System is alerting user to an operational error or maintenance issue. Thermo Scientific Nanopure TOC - Analytical... -
Page 25: Switches
Push to the left to deliver water manually until button is released. Note The unit MUST be in the normal recirculating mode (when the display is showing purity) in order to dispense water. Nanopure TOC - Analytical Thermo Scientific... -
Page 26: Initial Operation
Low Organics, Type 1 Water, Reverse Osmosis or Distilled Water Feed DIamond Kit Type 1 Deionized Feed D50283 Low Organics, Type 1 Water, DI Water Feed Each cartridge pack includes one 0.2 micron absolute final filter. Manifold Figure 7-1. Cartridge Pack Installation Thermo Scientific Nanopure TOC - Analytical... -
Page 27: Initial Rinse
Warning Use a properly grounded electrical outlet of correct voltage and current handling capacity. 5. Connect/attach to proper electrical outlet and the unit. 6. Turn the unit on by turning the main power switch to the “I” (ON) position. Nanopure TOC - Analytical Thermo Scientific... -
Page 28: System Cleaning Procedure
The entire cleaning procedure will take approximately 3.5 hours to complete. Note After cleaning is complete, the cleaning timer will need to be reset (refer to Resetting the Cleaning Timer) for another six month timing sequence. Thermo Scientific Nanopure TOC - Analytical... - Page 29 Carefully follow manufacturer’s safety instructions and material safety data sheets. This device to be used with water feeds only. Cleaning agents must be used in compliance with instructions in this manual. Failure to comply could result in explosion and personal injury. Nanopure TOC - Analytical Thermo Scientific...
- Page 30 15-20 liters through the cartridges and 0.2 micron filter may be necessary. Caution Never dispense water without first installing hose barb provided in parts bag or final filter supplied with cartridge pack. Thermo Scientific Nanopure TOC - Analytical...
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Page 32: Normal Operation
The unit pump will begin to run. 5. The display will then begin reading resistivity of the product water. Initially it will read “..MΩ-cm” until the air is bled from the system. Thermo Scientific Nanopure TOC - Analytical... -
Page 33: Automatic Dispensing
Note Press any switch except ENTER to stop dispensing. Display will read, “Auto Dispense Interrupted by User.” Note If the Nanopure “Auto Dispense” feature is set to (TIME), a connected Accudispense accessory (if one exists) will not automatically dispense. Nanopure TOC - Analytical Thermo Scientific... -
Page 34: User Settings
BACK switch until the display reads Language “LANGUAGE.” 2. The currently selected language is displayed on line 2 of the display. 3. Press the UP or DOWN arrow to select the language desired. 4. Press ENTER. Thermo Scientific Nanopure TOC - Analytical... -
Page 35: Setting The Date And Time
10. Press the UP or DOWN arrow until you reach the desired hour value. Press ENTER. 11. Press the UP or DOWN arrow until you reach the desired minute value. Press ENTER. 12. Press BACK twice to return to the (Idle) mode. Nanopure TOC - Analytical Thermo Scientific... -
Page 36: Setting The Cell Constant
14. If the cell constants displayed on line 1 of the display are correct, press the UP or DOWN arrow to select “Yes.” 15. Press ENTER. 16. Press BACK twice to return to the (IDLE) mode. Thermo Scientific Nanopure TOC - Analytical... -
Page 37: Selecting The Setpoint
UP or DOWN arrow until display reads, “Advanced Menu?” 2. Press ENTER. 3. Proceed through the options by pressing ENTER until “Adjust Set Point” is displayed. 4. Press the UP or DOWN arrow to choose “Yes.” 5. Press ENTER. Nanopure TOC - Analytical Thermo Scientific... -
Page 38: Resetting The Toc Lamp Timer
4. Press ENTER and the timer will be reset for approximately 1820 hours of operational time. The display will now display “Reset TOC Timer.” Press BACK two times to return to the (Idle) mode. Thermo Scientific Nanopure TOC - Analytical... -
Page 39: Using The Toc Analyzer
Note Once Volumetric or Timed Dispensing values are set, they will remain in memory until changed by the user. To turn the dispense method OFF, select “OFF” in the “Dispense Method” menu. Nanopure TOC - Analytical Thermo Scientific... -
Page 40: Change Purity Units: Factory Set - "Mω-Cm
3. Press BACK to return to the normal recirculating mode. Note Purity displayed will have an asterisk (*) left of the reading (* xx.x MΩ-cm or * x.xx uS/cm) to indicate that uncompensated purity is being displayed. Thermo Scientific Nanopure TOC - Analytical... -
Page 41: Temperature Compensation
5. Press ENTER. 6. Press the UP or DOWN arrow until the desired time is displayed for the unit to automatically enter Standby. 7. Press ENTER. 8. Press BACK until you return to the (Idle) display. Nanopure TOC - Analytical Thermo Scientific... -
Page 42: Unit Under Counter
4. Press the UP or DOWN arrow to choose “YES.” Note When “UNIT UNDER COUNTER” is set to “YES,” Auto Dispense will not be available from the main unit dispenser. 5. Press ENTER. 6. Press BACK until you return to the (Idle) display. Thermo Scientific Nanopure TOC - Analytical... -
Page 44: Accessories
5. Remove the jumper plug from the back, upper left portion of the unit and save for future use. 6. Plug the cable into the jumper plug outlet. 7. Reconnect the electrical power. Tank D8964 Float Switch D2706 Pressure Switch Figure 10-1. Feed Water Float/Pressure Switch Thermo Scientific Nanopure TOC - Analytical 10-1... -
Page 45: Dispense Overflow Cutoff Float
Note If an auto dispense is stopped by the overflow float switch, the Nanopure will change modes to normal recirculation. Figure 10-2. AY1367X1 Dispense Overflow Cutoff Float 10-2 Nanopure TOC - Analytical Thermo Scientific... -
Page 46: Electronic Calibration W/ N.i.s.t. Cal Module
12. Turn the main power switch to the OFF “O” position. Unplug the unit. 13. Remove the calibration module and reconnect the cell. 14. Reattach the cover plate and close and latch the door. 15. Reconnect the power cord. The calibration procedure is complete. Thermo Scientific Nanopure TOC - Analytical 10-3... -
Page 47: Manual/Accudispense Remote Dispensers
Section 10 Accessories Manual/Accudispense Refer to the Operating Instructions for your manual or Accudispense volumetric remote dispenser (LT1366X11). Remote Dispensers 10-4 Nanopure TOC - Analytical Thermo Scientific... -
Page 48: Computer/Printer Setup
Computer/Printer Setup called capture.txt and the file will be an ASCII text file. 11. You should see the data on the computer screen. Thermo Scientific Nanopure TOC - Analytical 11-1... -
Page 49: Procomm
12. Type in 21 <Enter>, sets to COM2: or (Type in 20 <Enter>, sets to COM1:), depending on your computer. 13. Type in 24 <Enter>, saves settings. 14. Type ESC to exit setup menu. 15. Procomm is now ready to accept input from the Nanopure. 11-2 Nanopure TOC - Analytical Thermo Scientific... -
Page 50: Connecting And Starting The Printer
Located on the front of the printer (AY1137X1), this switch turns power to the printer ON and OFF. The POWER light will illuminate when the printer is ON. For additional setup and operation, refer to the instruction manual included with the printer. Thermo Scientific Nanopure TOC - Analytical 11-3... -
Page 52: Maintenance And Servicing
6. Thoroughly rinse the cell in deionized or distilled water following the detergent or acid cleaning. 7. After cleaning, check the o-ring; replace if necessary. 8. Reinstall the cell into the cell well and hand-tighten. Thermo Scientific Nanopure TOC - Analytical 12-1... -
Page 53: System Cleaning
From the (Idle) mode, press the UP or DOWN arrow until the display reads, “Clean Unit?” 2. Press ENTER. 3. Display will prompt, “Disconnected Inlet Water (NO).” 4. Disconnect feed water supply at the quick-disconnect inlet valve. 12-2 Nanopure TOC - Analytical Thermo Scientific... -
Page 54: System Depressurization
2. From “Air Purge?” press the UP arrow. 3. From “Depressurize”, press the UP arrow to select (YES). 4. Press ENTER. Display will show “System Flushing” and the time remaining as the system depressurizes. Thermo Scientific Nanopure TOC - Analytical 12-3... -
Page 55: Cartridge Pack Replacement
7. Install new cartridge pack, rinse and clean according to the instructions in the “Initial Operation” section. Warning A full cartridge pack may weigh about 20 lbs. (9 kg). Manifold Figure 11-1. Cartridge Pack Replacement 12-4 Nanopure TOC - Analytical Thermo Scientific... -
Page 56: Micron Filter Replacement
Note If a newly installed 0.2 micron filter clogs rapidly after installation, the Nanopure TOC - Analytical may need to be cleaned to remove bacterial contaminants. See “System Cleaning.” 0.2 Micron Fiilter Figure 11-2. Replacing the 0.2 Micron Final Filter Thermo Scientific Nanopure TOC - Analytical 12-5... -
Page 57: Toc Lamp Replacement
7. Reconnect power cord and reset the TOC lamp timer. (See “Resetting the TOC Lamp Timer.”) Clips Sockets Chamber used for Pin Pins Insertion Figure 12-3. Lamp Chamber Replacement 12-6 Nanopure TOC - Analytical Thermo Scientific... -
Page 58: Shutdown
If the system has remained inactive and full of water for more than 96 hours, the unit should be drained, cleaned and new cartridge pack installed prior to use. Thermo Scientific Nanopure TOC - Analytical 12-7... -
Page 60: Troubleshooting
Check the expiration date. Cartridge packs begin to lose capacity after being stored for 2 years from Short cartridge pack life. Cartridge pack is beyond expiration date. the date of manufacture. Replace the cartridge pack with an unexpired one. Thermo Scientific Nanopure TOC - Analytical 13-1... - Page 61 Replace final filter as indicated in 0.2 micron filter clogged. Error.” “0.2 Micron Filter Replacement.” Solenoid failure. Replace BK1367X1. Check tubing for kinks – including Kinked tubing. tubing for manual or Accudispense accessory. 13-2 Nanopure TOC - Analytical Thermo Scientific...
- Page 62 Shorted TOC resistivity sensor. (under Diagnostics); if still shorted, replace TOC Analyzer. Verify TOC lamp is connected. Replace TOC lamp (See “TOC TOC UV lamp error. Lamp Replacement”) All other error codes. Contact Technical Services. Thermo Scientific Nanopure TOC - Analytical 13-3...
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Page 64: Replacement Parts
Main Fuse, 230 Volt - Type T Time Lag, 0.63 Amp, 250V FZX54 PTFE Tape, Roll 06078 Transformer Fuse, Type F Fast-Acting, 3.15 Amp, 250V AZ9027 Cleaning Solution CMX25 TOC Analyzer Lamp LMX26 Thermo Scientific Nanopure TOC - Analytical 14-1... - Page 65 Calibration PC Board PC1190X2 Resistivity Meter PC Board PC896X2 Check Valve PMX214 Flow Sensor ME1190X1 Flush Solenoid RY1190X3 Cartridge Pack Manifold BK1190X3 Dispenser Manifold w/Solenoid BK1367X1 Dispense Switch SW1190X1 Cell O-ring GSX29 TOC Analyzer PCX54 14-2 Nanopure TOC - Analytical Thermo Scientific...
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Page 66: Ordering Procedures
All parts listed herein may be ordered from the Thermo Scientific dealer from whom you purchased this unit or can be obtained promptly from the factory. -
Page 67: Flow Chart
Remote Gun System flush? Date Format Auto Dispense Set Date Menu? Set Time Arrow Legend: Set Cell Constant Keypress Options Set Display Automatic Entry Brightness Menu Wrap-around Adjust Set Point Diagnostics Operational Overview menu? 14-4 Nanopure TOC - Analytical Thermo Scientific... -
Page 68: Wiring Diagram
Section 14 Wiring Diagram Wiring Diagram Thermo Scientific Nanopure TOC - Analytical 14-5... - Page 70 Thermo Fisher Scientific 401 Millcreek Road Marietta, Ohio 45750 United States www.thermofisher.com...
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