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ThermoFisher Scientific iCAP 7000 Plus Series Operating Manual

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iCAP 7000 Plus Series ICP-OES
Operating Manual
BRE0004150 Revision C
January 2018

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mansour
May 7, 2025

why detector temperature showed blue color in the Interlocks dash

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Mr. Anderson
May 18, 2025

The detector temperature shows a blue color in the Interlocks dash of the ThermoFisher Scientific iCAP 7000 Plus Series when the camera is too cold.

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Summary of Contents for ThermoFisher Scientific iCAP 7000 Plus Series

  • Page 1 7000 Plus Series ICP-OES Operating Manual BRE0004150 Revision C January 2018...
  • Page 3 7000 Plus Series ICP-OES Operating Manual BRE0004150 Revision C January 2018...
  • Page 4 Legal Notices © 2018 Thermo Fisher Scientific Inc. All rights reserved. Original Operating Instructions Published by: Thermo Fisher Scientific (Bremen) GmbH, Hanna-Kunath-Str. 11, 28199 Bremen, Germany Tel: +49(0)421 5493 0, Fax: +49(0)421 5493 396 Microsoft and Windows are registered trademarks of Microsoft Corporation in the United States and other countries.

  • Page 5: Table Of Contents

    Volatile Organic Samples .......... 3-15 High Dissolved Solid Samples........3-16 Argon Humidifier Accessory ........3-16 Aerosalt Nebulizer............. 3-17 Parallel Path Nebulizer..........3-17 Sheath Gas Adaptor ..........3-17 HF Samples ..............3-18 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 6 Radial View Interfaces on a Duo Instrument..... 6-17 Example Standard Operating Procedures ..... 6-19 Preparing the System..........6-19 Lighting the Plasma ..........6-20 Setting Up Analyses ..........6-23 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 7 Returning Parts ............8-11 Services to be Performed by Thermo Fisher Scientific Service Only ..........8-11 Appendix A Advanced Hardware ............A-1 Sprint Valve ..............A-2 Supported Autosamplers ..........A-2 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 8 Hydride Generation ............B-4 On-line Hydride Generation Kit......... B-4 Integrated Hydride Generation Kit ......B-6 Gas Liquid Separator (GLS)........B-7 Appendix C Legal Documents..............C-1 Glossary ................. G-1 Index..................I-1 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 9 Technical Data for iCAP 7000 Plus Series ICP-OES Systems The table below summarizes the most important technical specifications of the iCAP 7000 Plus Series ICP-OES systems, in relation to the installation. See the respective chapters of the manual for details and additional information.
  • Page 10 Technical Data for iCAP 7000 Plus Series ICP-OES Systems iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 11 Scientific™ iCAP™ 7000 Series ICP-OES. In addition, this manual provides step-by-step instructions for cleaning and maintaining your instrument. This iCAP 7000 Plus Series ICP-OES Operating Manual is intended for all personnel that need a thorough understanding of the instrument (to perform maintenance or troubleshooting, for example). Read this manual carefully before using the instrument and keep it for future reference.

  • Page 12: Using This Manual

    “press <Shift> + <F1>” means press and hold the <Shift> key and then press the <F1> key. • Any button that you click on the screen is represented in bold face letters. For example, “click Close”. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 13: Topic Headings

    The following headings are used to show the organization of topics within a chapter: Chapter Name Chapter 1 Second Level Topics Third Level Topics Fourth Level Topics Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 14: Reference Documentation

    • iCAP 7000 Series ICP-OES Accessories Guide • Qtegra for iCAP 7000 Series ICP-OES Software Manual The Qtegra iCAP 7000 Plus Series ICP-OES Online Help page provides help with running your instrument, including software guides. See Figure 1-1. Figure 1-1. Qtegra ISDS Software Help topics...

  • Page 15: Contacting Us

    Germany • Send an e-mail message to the Technical Editor at documentation.bremen@thermofisher.com You are encouraged to report errors or omissions in the text or index. Thank you. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 16 Using this Manual Contacting Us iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 17: System Accessories

    System Accessories Chapter 2 In addition to the iCAP 7000 Plus Series ICP-OES, some of the system accessories are required whereas others are optional. Contents • Required Accessories page 2-1 • Optional Accessories page 2-1 Required Accessories The following accessories are mandatory. They can be ordered from Thermo Fisher Scientific or an equivalent can be supplied by the user: •...
  • Page 18 The above list is subject to change. Contact Thermo Fisher Scientific or a local representative for a list of currently supported accessories. Request site requirement guides for any purchased accessories. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 19 Sample Introduction System page 3-11 • Internal Standards Kit page 3-13 • Organic Solvent Analysis page 3-14 • High Dissolved Solid Samples page 3-16 • HF Samples page 3-18 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 20: Functional Description

    Functional Description Introduction Introduction The Thermo Scientific iCAP 7000 Plus Series ICP-OES is a range of inductively coupled plasma-optical emission spectrometers (ICP-OES), which use an echelle optical design and a Charge Injection Device (CID) solid-state detector to measure trace elemental concentrations in a wide range of samples.

  • Page 21: Introduction

    7600 ICP-OES Duo Full mass flow controlled gas box, axial and radial plasma view optics, advanced sample introduction, and enhanced software The following sections describe the specification details. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 22: Instrument Specification

    Fullframe imaging Sprint mode Fullframe imaging Productivity features Intelligent Uptake and Rinse Sprint Valve Speed acquisition mode Intelligent Uptake and Rinse — Speed acquisition mode Sprint acquisition mode iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 23: Optical System

    Unique, all spherical mirror design for very high image quality, improved optical resolution and very low stray light performance. Focal Length Effective focal length 383 mm Imaging Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 24: Detector Specifications

    9.5° prism. Ultra pure ultraviolet fused silica. Spectral Bandpass 7 pm at 200 nm, 3.5 pm per pixel. Wavelength Coverage iCAP 7000 Plus Series ICP-OES have a wavelength range from 166 nm to 847 nm. Detector Specifications Type RACID86 Charge Injection Device (CID). High performance solid state CID camera system.

  • Page 25: Detector Mode

    Plasma Source Specification Type Inductively Coupled Argon Plasma using the internationally approved Industrial Scientific and Medical (ISM) radio frequency bands. Solid state RF generator with power efficiency above 78%. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 26: Sample Introduction Specifications

    Glass cyclonic type with separate radial or axial connection adapter fitted as standard Optional: IsoMist™ XR temperature controlled spray chamber, baffled cyclonic spray chamber, HF resistant cyclonic spray chamber iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 27 Semi-demountable quartz torch fitted with either a 1.5 mm center tube (Radial instruments) or 2 mm center tube (Duo instruments). On Radial instruments the fully demountable ceramic D-Torch is delivered as standard. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 28 0–2 L/min in 0.1 L/min increments. • The coolant flow is computer controlled through a MFC from 0– 20 L/min in 1 L/min increments. • Air as additional gas is standard. 3-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 29: Operating Noise Level

    Standard on Duo configurations dissolved solids solutions (single blue ring) 2.0 mm ceramic for Used for specific sample types (for HF solutions example, hydrofluoric acid digests) Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 3-11...

  • Page 30: Nebulizer Options

    Typically, the peristaltic pump is operated at a speed of approximately 50 rpm when using an iCAP 7000 Plus Series ICP-OES. If you intend to analyze samples containing high concentrations of dissolved solids or volatile organic constituents, it may be necessary to reduce the pump speed to between 35–45 rpm.

  • Page 31: Internal Standards Kit

    To minimize sample dilution, the tubing for the internal standard solution has a smaller bore than that of the sample solution. To ensure thorough mixing of the internal standard with the sample, a mixing loop Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 3-13...

  • Page 32: Organic Solvent Analysis

    The V-groove nebulizer should be configured in the cyclonic spray chamber with the gas connection pointing vertically downwards. Figure 3-6. The orientation of the nebulizer is essential to enable successful sample aspiration. 3-14 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 33: Volatile Organic Samples

    Glass Expansion, which can be used effectively with iCAP 7000 Plus Series ICP-OES for applications with volatile organic solvents. Figure 3-7. IsoMist™ XR - temperature controlled spray chamber Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 3-15...

  • Page 34: High Dissolved Solid Samples

    Figure 3-8. pergo argon nebulizer gas humidifier and pergo system diagram (source: ESI) 3-16 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 35: Aerosalt Nebulizer

    The additional gas mass flow controller can be used for the addition of the sheath gas (standard on the iCAP 7600 ICP-OES and optional on the iCAP 7400 ICP-OES). Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 3-17...

  • Page 36: Hf Samples

    (see Figure 3-10): • Ceramic center tube • HF resistant nebulizer • HF resistant spray chamber with spray chamber adapter Figure 3-10. HF sample introduction configuration 3-18 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 37 Safety Symbols on the Instrument page 4-2 • Intended Use page 4-4 • Electric Safety Precautions page 4-6 • In Case of Emergency page 4-7 • Residual Hazards page 4-8 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 38: Safety

    Ensure permanent access to this document for quick reference. System configurations and specifications in this manual supersede all previous information received by the purchaser. Before you operate your iCAP 7000 Plus Series ICP-OES, read and understand all the safety information in this manual. Safety Symbols on the Instrument...

  • Page 39: Rating Plate

    DK>  W z Z K& D Eh& dhZ ^hWW>z sK>d ' &ZYhEz WKtZ D y ^Zs/ z Yh >/&/ WZ^KEE> KE>z Figure 4-1. Rating plate (example) Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 40: Intended Use

    If the iCAP 7000 Plus Series ICP-OES is used in a manner not specified by Thermo Fisher Scientific, the protection provided by the instrument could be impaired. Thermo Fisher Scientific assumes no responsibility and will not be liable for instrument damage and/or operator injury.

  • Page 41: Permitted Materials

    The users must be advised to read the relevant Material Safety Data Sheets (MSDSs). Permitted Materials The iCAP 7000 Plus Series ICP-OES system is designed to be operated with the materials listed in Table 4-2.

  • Page 42: Electric Safety Precautions

    If the equipment is used in a manner that is not specified by the manufacturer, the safety protection provided by the equipment might be impaired. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 43: In Case Of Emergency

    (for example, an autosampler) with their respective On/Off switches. WARNING Electric Current. Electric shock hazard. Capacitors inside the instrument might still be charged for some time even if the instrument is turned off. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 44: Residual Hazards

    Safety Residual Hazards Residual Hazards Users of the iCAP 7000 Plus Series ICP-OES must pay attention to the following residual hazards. WARNING Toxic Gases. Risk of intoxication. Toxic gases are released that might lead to severe bodily harm when the plasma exhaust is not connected to an exhaust system or the spray chamber is disassembled.

  • Page 45: Personal Protective Equipment

    Scientific recommends white nitrile clean room gloves from Fisher Scientific Unity Lab Services. For handling hot objects, gloves made of heat-resistant materials (for example, leather) should be available. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 46 Safety Residual Hazards 4-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 47 ICP-OES system. To be sure that your laboratory is ready for installation of the iCAP 7000 Plus Series ICP-OES, you have to meet all requirements specified in the iCAP 7000 Plus Series ICP-OES Pre-Installation Requirements Guide. This guide also provides comprehensive information to assist in planning and preparing your lab site.

  • Page 48: Installation

    CAUTION Hot Surface. Risk of burns. Let any hot components cool for at least 10 minutes before you remove them from the torch compartment. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 49: Spectrometer Dimensions

    (29½ inch) (23¼ inch) (187 lb) Figure 5-1 shows a schematic of the iCAP 7000 Plus Series ICP-OES in front view, whereas Figure 5-2 shows it in top view. 840 mm Figure 5-1. iCAP 7000 Plus Series ICP-OES in front view Figure 5-2.

  • Page 50: Installation Requirements

    Installation Requirements This section describes the environment and the resources required at the installation site of the iCAP 7000 Plus Series ICP-OES and associated equipment. Safety requirements for the installation are detailed as well. The installation of all services must comply with the appropriate rules and regulations required by the local authorities responsible for those services in the workplace.

  • Page 51: Environmental Requirements

    Appropriate placement of the The iCAP 7000 Plus Series ICP-OES, as with all ICP-OES, draws air instrument with availability of a through the unit as a source of cooling. If the laboratory air contains a...

  • Page 52: Electrical Requirements

    Appropriate placement of sample Liquid autosamplers should be installed to ensure a sufficient air introduction accessories when clearance around the base of the iCAP 7000 Plus Series ICP-OES. working with corrosive or volatile Thermo Fisher Scientific also recommends using a cover and/or...

  • Page 53: Gas Requirements

    Power Quality The power supplied to iCAP 7000 Plus Series ICP-OES must be stable. The input (line) voltage must be 230 V AC. The input frequency must be between 47 and 63 Hz. Avoid brownouts (drop in voltage) and spikes (increase in voltage) over short timescales.
  • Page 54 Gas Consumption The gas consumption of an iCAP 7000 Plus Series ICP-OES varies with plasma conditions and purge operating parameters. Table 5-3 shows the approximate gas consumption for plasma gas and purge gas at different conditions.

  • Page 55: Recirculating Chiller

    An appropriate container is required that is solvent-proof, shatter-proof and vented away from the instrument. Compatible container materials ensure that waste does not react with them or corrode them. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 56: Spectrometer Fume Extraction

    The extraction tube has an inlet diameter of 125 mm (5 inch). A 2 m (6.5 ft) flexible tube is supplied with the instrument. 5-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 57 Consult a qualified extraction specialist to ensure that the correct flow is achieved at the instrument. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 5-11...

  • Page 58: Sample Fume Extraction

    Thermo Fisher Scientific field service engineer. The instrument IP address is 90.0.0.50. Tip The instrument Ethernet port must be configured to allow it to communicate with the instrument. 5-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 59: Data Station Requirements

    (left side of the spectrometer) Electrical supply Plug 200–240 V AC, 20–32 A, single phase required 4000 W, 50/60 Hz Standard mains plug 200–240 V AC for each required accessory Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 5-13...
  • Page 60 Minimum 1 L container for the rinse supply 2 needed station and waste Chiller Maximum distance from the spectrometer Pipe supply outer diameter dimension 12 mm 5-14 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 61 Cooling capability 750 W minimum Flow rate (all chillers) > 5 L/min Pressure at 5 L/min (ThermoFlex 900 chiller 5.5 bar (80 psi) only) Corrosion inhibitor required Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 5-15...
  • Page 62 Installation Installation Checklist 5-16 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 63: System Operation

    Example Standard Operating Procedures page 6-19 • Reporting Results page 6-27 • Exporting LabBooks page 6-28 • Auto Peak Adjust page 6-30 • Shutting Down the System page 6-32 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 64: Safety Guidelines For Operation

    CAUTION Hot Surface. Risk of burns. Let any hot components cool for at least 10 minutes before you remove them from the torch compartment. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 65: Preparing The System For Use

    Preparing the System for Use Preparing the System for Use The iCAP 7000 Plus Series ICP-OES is designed to be constantly powered up and the optical system continuously purged. The instrument is powered with an on/off switch at the rear of the left side.

  • Page 66: Instrument Optimization

    You may want to select higher power for organics and High TDS samples. Pump speed 45 to 50 rpm for most samples As low as 30 rpm for organics to reduce the plasma loading iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 67: Setting The Pump Tension

    NOTICE Always wear gloves when you handle glass or ceramic torches. Handprints reduce the life of the torch and might cause the torch not to light. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 68: Duo Torch Assembly

    3. Check that the four O-rings in the center tube holder are not damaged. Fully insert the center tube into the plastic center tube holder. See Figure 6-6. Figure 6-6. Torch assembly - center tube iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 69 See Figure 6-9. Figure 6-9. Insertion of the torch assembly into the box Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 70 10. Attach the spray chamber adapter to the spray chamber with the fitting clamp provided. The adapter provided with the instrument is specially designed to prevent UV radiation from escaping from the torch box. See Figure 6-12. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 71 Problems in any of these areas might cause air leaks or disruption of the gas flows making the plasma difficult to ignite and might cause damage to the torch. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 72: Radial Torch Assembly

    The associated line marking on the torch should be aligned with the edge of the torch holder assembly. Figure 6-16. Radial torch assembly 6-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 73 6. Push the torch assembly up into the torch box and twist clockwise until the red orientation lock locates in the torch box casting. See Figure 6-20. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-11...
  • Page 74 10. With a twisting motion, insert the nebulizer into the spray chamber so that the collar is tight fit. The collar will set the insertion depth and aid reproducibility of results. 6-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 75 This could result in exposure to dangerous radio and UV frequency radiation. To feed the sample capillary tubing, proceed with “Connection of Pump Tubing” page 6-14. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-13...

  • Page 76: Connection Of Pump Tubing

    Figure 6-23 shows the peristaltic pump and 2-stop tubing that is typical of the iCAP 7000 Plus Series ICP-OES, except for the iCAP 7600 ICP-OES. Here, the sample pump tubing has white and orange stops, and the drain tubing has white and white stops.
  • Page 77 Gripping the PTFE tube with fine sandpaper is recommended. Figure 6-25. Sample capillary tubing NOTICE Connect the drain tubing correctly to the peristaltic pump to account for the counterclockwise flow. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-15...
  • Page 78 7600 ICP-OES. Tubings of both diameters are part of the sample introduction kits supplied with a spectrometer. The wider tube is available as P/N 8423 120 52671. 6-16 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 79: Radial View Interfaces On A Duo Instrument

    If the radial glass window is removed from the periscope, ensure that sufficient time is left to stabilize the purge after replacing the window. Figure 6-28. Radial glass window Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-17...
  • Page 80 Thermo Fisher Scientific field service engineer because it may be necessary to perform a fore-optics alignment. Later maintenance of the radial POP interface can be done by the user. 6-18 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 81: Example Standard Operating Procedures

    2. Turn on the air supply for the Additional gas supply (iCAP 7400 ICP-OES and iCAP 7600 ICP-OES) if used. 3. Switch on power to the iCAP 7000 Plus Series ICP-OES. NOTICE For normal use, leave the power constantly on. If the instrument power has been switched off, wait at least for two hours after restoring power to let the instrument thermally stabilize.

  • Page 82: Lighting The Plasma

    If red, the plasma will not light. If the LED flickers even slightly, the plasma will go out. This indicates a problem with the chiller. 6-20 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 83 Is usually selected to perform an automatic Optimization minor correction of the location of the emission spectrum on the detector. Nebulizer Is usually selected to improve performance Optimization tests. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-21...
  • Page 84 Dashboard page. Tip To let the plasma stabilize, leave the plasma on with a blank solution running for about 10 minutes before carrying out an analysis. 6-22 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 85: Setting Up Analyses

    The availability of each parameter is controlled by the type of Evaluation defined for the Template or LabBook. Refer to the Qtegra for iCAP 7000 Series ICP-OES Software Manual for more information. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-23...
  • Page 86 Use Manual Sample Control to disable the autosampler and define the Uptake time and the Wash time. See Figure 6-34. Figure 6-34. Manual Sample Control page 6-24 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 87 QC checks. Use the label identifier and sample type drop down list as required. If using an autosampler, identify the rack and vial for each sample. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-25...

  • Page 88: Running The Analysis

    If the Automatic check box has been selected for Start Queue in the Options settings of the Scheduler, the measurement is started immediately. Figure 6-37. Running a LabBook 6-26 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 89: Reporting Results

    Save Report applies settings to the current report style. The reported LabBook can also be printed or saved in a different file. Figure 6-38. Specifying report settings Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-27...

  • Page 90: Exporting Labbooks

    Export from the menu. See Figure 6-40. Figure 6-40. Exporting a LabBook 2. Select the location to save the data. Click OK. See Figure 6-41. 6-28 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 91 Other data (such as instrument logs) can also be exported as a .csv file. This is particularly useful when requesting Service Engineer help. See Figure 6-42. Figure 6-42. Exporting a log Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-29...

  • Page 92: Auto Peak Adjust

    Auto Peak adjustment takes place. If not all elements to be auto peaked are in the same solution, multiple standards may be used. 6-30 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 93 See Figure 6-44. Figure 6-44. AutoPeak procedure result Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-31...

  • Page 94: Shutting Down The System

    6-45. Figure 6-45. System shutdown The optical components move to a parked position after about 30 seconds. The iCAP 7000 Plus Series ICP-OES shuts down and the plasma is switched off. The state of the Configuration changes to NotReady. 6. When using the Sprint Valve on the iCAP 7600 ICP-OES, it has to be emptied at the end of a run.
  • Page 95 9. After the plasma has been switched off, wait five minutes before switching off the power to the instrument. 10. Release the tension on the sample pump platens to preserve the life of the pump tubing. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 6-33...
  • Page 96 System Operation Shutting Down the System 6-34 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 97 Resolving Problems with Analytical Results page 7-5 • Resolving Specific Analytical Problems page 7-7 • Suggested Maintenance in Case of Poor Precision and Detection Limits page 7-12 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 98: Troubleshooting

    Pinch Point Hazard. Risk of injuries. The peristaltic pump rollers can pull in hair, clothing, ties and other loose objects. Stay clear from the peristaltic pump during operation. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 99: Problems With Plasma Ignition

    1. Make sure that your argon plasma gas supply pressure is set to 5.5 bar with a regulator close to the instrument. Make sure that the pressure is stable and does not fall during ignition. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 100: Ignition Spark

    5% of the recommended inhibitor solution must be added to the water. 3. Check the water filters on input to the instrument, if fitted. 4. Look for deposits on the torch. Replace the torch, if necessary. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 101: Problems With Plasma Going Out Unexpectedly

    2. Feel for flats where the rollers have been. If flats exist, change the tubing. It is advisable to change the pump tubing just before starting the soak tests. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 102 13. If the draining is poor, check the pressure of the pump clamp for the drain tube. Otherwise, flush the system for a couple of minutes with a 10% Decon™ 90 solution. Aspirate the Decon with the plasma running. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 103: Resolving Specific Analytical Problems

    Troubleshooting Resolving Specific Analytical Problems 14. Make sure that your torch is fitted properly. This is especially important with a iCAP 7000 Plus Series ICP-OES Duo to ensure that Radial view is good. ❖ To make sure that your sample introduction system is clean 1.
  • Page 104 This is usually caused by an oily film and can be easily cured by aspirating a 1–5% Decon™ 90 solution for about clean spray chamber 30 seconds. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 105 Any such damaged pumps should be replaced. The peristaltic pump may also be used for the pumped drain spray chamber systems and the internal standards mixing kits. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 106 1/2 inch of the tubing and reinserting it. Replace the tubing with 1/4 inch Teflon™ if the tubing becomes too short. 7-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 107: Poor Accuracy/Feedback

    Purged Optical Path. UV burn or a dirty mirror is characterized by a long term decline (six months or longer) of intensities. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 7-11...

  • Page 108: Suggested Maintenance In Case Of Poor Precision And Detection Limits

    Hardened and discolored tubing is caused by chemical reactions with the sample. While these phenomena cannot be avoided, they can be minimized by frequently flushing it with deionized water. 7-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 109: Preventing Blockage Of The Nebulizer

    A low-pH (acidic) sample should be followed by a low-pH rinse, a high-pH sample by a high-pH rinse, and an organic sample by an appropriate solvent. The final rinse should use deionized water and/or isopropyl alcohol. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 7-13...

  • Page 110: Removing Solids From The Nebulizer

    2. Gently tap or flick the shell soundly with your fingernail a few times. If this fails to dislodge the particle, close off the liquid and gas input tubes with your fingertips. 7-14 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 111 Use acid resistant laboratory gloves and glasses. • Make yourself aware of all safety procedures in case of spillage or exposure to skin or eyes before commencing the cleaning. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 7-15...
  • Page 112 NOTICE Avoid overheating residues that might produce insoluble pyrolysis products. 2. Stop treatment when you have opened a passage through the blockage. 7-16 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 113 Safety Guidelines for Maintenance page 8-2 • Cleaning the Instrument page 8-3 • Preventive Maintenance page 8-8 • Torch Alignment page 8-9 • Thermo Fisher Scientific Service page 8-10 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 114: Maintenance

    Stay clear from the peristaltic pump during operation. Do not open the instrument or remove covers. No user serviceable parts are inside. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 115: Cleaning The Instrument

    Remove stains and marks on the covers with a soft cloth moistened with a mild detergent solution. Do not use any solvent-based cleaners. NOTICE The iCAP 7000 Plus Series ICP-OES covers are made of ABS plastic which can be damaged by solvents and concentrated acids. Cleaning and Decontaminating the Sample Introduction System Failure to maintain the sample introduction system can result in erroneous results, poor precision, poor detection limits and blockages.

  • Page 116: Cleaning The Spray Chamber

    A mixture of nitric acid and hydrochloric acid is normally suitable. After cleaning, rinse the spray chamber in deionized water. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 117: Cleaning The Nebulizer

    “To shut down the system” page 6-32. 2. Open the small access door next to the sample compartment door. Figure 8-2. Figure 8-2. Access to POP window Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 118: Cleaning The Radial View Interfaces

    If you are using a Duo instrument, the interfaces for the radial view can get dirty and have an impact on the measured signal. When using the radial glass window for radial view, the cleaning procedure is as follows: iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 119 See Figure 8-4. Figure 8-4. Removing green O-ring 5. Clean the circular glass window using a lint-free cloth and clean water. 6. Repeat step 4 with methanol. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 120: Preventive Maintenance

    Water Chiller It is critical to the performance of your instrument that the cooling fluid used for your iCAP 7000 Plus Series ICP-OES is made up correctly as specified in the iCAP 7000 ICP-OES Pre-Installation Requirements Guide. An effective maintenance plan includes replacing the cooling...

  • Page 121: Water Filter

    2. On the Dashboard, click Torch Alignment to start the procedure. 3. Aspirate the so-called “Loaded Blank” solution as supplied with the iCAP 7000 Plus Series ICP-OES or any other aqueous 2 ppm Zn solution. Optionally, use an organic solvent 2 ppm Zn solution, which applies slightly different plasma settings (higher auxiliary gas flow, slightly decreased nebulizer gas flow, slightly decreased pump speed).

  • Page 122: Thermo Fisher Scientific Service

    Safety documentation and the decontamination certificate must be made available to the Thermo Fisher Scientific field service engineer. 8-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 123: Returning Parts

    Services to be Performed by Thermo Fisher Scientific Service Only The annual preventive maintenance must be performed by a Thermo Fisher Scientific field service engineer only. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) 8-11...
  • Page 124 Maintenance Thermo Fisher Scientific Service 8-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 125 7600 ICP-OES and optional accessories for the other spectrometers of the iCAP 7000 Plus Series ICP-OES. Contents • Sprint Valve page A-2 • Additional Gas Accessory page A-24 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 126: Appendix A Advanced Hardware

    • Solutions of concentrated acids (greater than 40%) • Partially halogenated hydrocarbons or extremely aggressive organic solvents (chloroform, methylene dichloride, 1,1,2-trichloroethane). iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 127 Sprint Valve system and must be followed. See Figures to A-4. Figure A-1. Standard configuration for loading sample into sample loop Figure A-2. Standard configuration for injection of sample from sample loop Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 128 Figure A-3. Standard configuration for loading sample into sample loop with additional internal standard Figure A-4. Standard configuration for injection of sample from sample loop with additional internal standard iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 129 Advanced Hardware Sprint Valve Connecting the Tubing Figure A-5. Sprint Valve tubing connections with 6-port valve Figure A-6. Sprint Valve tubing connections with 7-port valve Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 130 4. Screw the green valve fitting into port 5 on the valve head. 5. Take the white valve fitting tube and attach one end to port 3 on the valve head. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 131 Service Test Kit). 10. Screw the fitted nebulizer tube into port 6. 11. Attach the other end on the nebulizer line and the nebulizer gas fitting onto the nebulizer. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 132: Operational Settings

    Operational Settings The operational settings of the iCAP 7000 Plus Series ICP-OES Sprint Valve are either controlled • by a separate software package (Sprint Valve Configurator), which is installed along with your installation of Qtegra ISDS Software or •...
  • Page 133 To define the Sprint Valve settings with the external Sprint Valve Configurator 1. Click Connect to Sprint Valve. The parameters of the Sprint Valve Configurator window become available. See Figure A-9. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 134 To operate the Sprint Valve with the plugin in Qtegra ISDS Software, the cables between Sprint Valve, autosampler and PC need to be connected as shown in Figure A-10. A-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 135 To define the Sprint Valve settings with the Sprint Valve plugin 1. Enable Sprint Valve in the autosampler plugin in the configuration. Figure A-11. Figure A-11. Enabling Sprint Valve in autosampler plugin Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-11...
  • Page 136 3. Select and modify the required settings. See Figure A-12 Table A-1. When the instrument configuration is saved, the settings are uploaded to the Sprint Valve. A-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 137: Description Of Timings

    Rinse Evacuation Delay/Loop Rinse Delay • Loop Load • Equalization Delay • Time to get the sample from loop to plasma • Stabilization time (~5 seconds) Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-13...

  • Page 138: Manual Control Features

    Configurator, click this button. The window expands to show the manual control features. See Figure A-14. Figure A-14. Manual control features in external Sprint Valve Configurator A-14 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 139 “Homing the valve” needs to be performed each time the valve is removed and re-attached. Vacuum Pump Control Switches the iCAP 7600 ICP-OES vacuum pump on and off Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-15...

  • Page 140: Manual Sampling Using The Sprint Valve

    Routine maintenance also includes checking the Sprint Valve components for leaks or other damage. • Additional periodic maintenance tasks may be required, including replacement of peristaltic pump tubing, rinse tubing, and sample probe. A-16 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 141 For more information on how to install the rinse tubing, see “Plumbing Connections” page A-3. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-17...
  • Page 142 In the manual control of the Sprint Valve, set the valve to Load. c. Turn on the vacuum pump until the loop is dry. d. Turn off the vacuum pump. A-18 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 143 30 minutes. ii. Inspect rotor and stator for scratches or blockage. • Option B – Cotton swab + solvent Inspect rotor and stator for scratches or blockage. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-19...
  • Page 144 The 6-port/7-port valve assembly has a finite lifespan that depends upon the conditions and sample media to which it is exposed. Exposure to higher sample solids levels reduces the lifespan of the valve. A-20 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 145 See Figure A-21. Figure A-21. Loosening the hex screw 3. Firmly but carefully remove the valve head. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-21...
  • Page 146 A-23. Figure A-23. Checking the valve seat 7. Use the hex key to tighten the locking collar. See Figure A-24. Figure A-24. Tightening the locking collar A-22 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 147 A-26. Figure A-26. Reconnecting the tubing 10. When using the external Sprint Valve Configurator, check for any leaks using the Manual Cycle function. See Figure A-27. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) A-23...

  • Page 148: Additional Gas Accessory

    For best performance, it is recommended that the addition is made to the auxiliary gas in preference to the nebulizer gas (this is the standard configuration). See Figure A-28. Figure A-28. Additional gas accessory aux gas connections A-24 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 149: Installing The Additional Gas Accessory

    For safety reasons, 100% (pure) oxygen is not approved to be used as additional gas in the iCAP 7000 Plus Series ICP-OES. For the additional gas MFC, clean dry oil-free air is required. Thermo Scientific...
  • Page 150 Advanced Hardware Additional Gas Accessory A-26 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 151: Appendix B Optional Accessories

    Request site requirement guides for any purchased accessories. Contents • Autosampler page B-2 • Ultrasonic Nebulizer page B-3 • Hydride Generation page B-4 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 152: Autosampler

    Series ICP-OES, accessories and associated equipment must be installed by a certified Thermo Fisher Scientific service representative. For details, refer to the installation and operation documentation of your particular model of autosampler that is supplied with your iCAP 7000 Plus Series ICP-OES. Autosampler Setup...

  • Page 153: Ultrasonic Nebulizer

    4. Use the 4 mm argon tubing supplied with the accessory to connect the nebulizer gas outlet of the iCAP 7000 Plus Series ICP-OES with the inlet on the rear panel of the ultrasonic nebulizer. Thermo Scientific...

  • Page 154: Hydride Generation

    Tip Because two different peristaltic pumps (standard and mini) are used with the iCAP 7000 Plus Series ICP-OES, tubing sizes are adjusted to fit the purpose. Tubing sizes for the standard pump (mini pump in brackets) are indicated.
  • Page 155 Nebulizer gas typical operating range 0.19–0.29 MPa (~0.5 L/min) Pump speed 45 rpm 3. Aspirate a solution of 50 g/L arsenic solution and check the signal in the subarray window. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 156: Integrated Hydride Generation Kit

    The unit is supplied with all pump tubing connected. • The user must attach the pump tubing to the peristaltic pump on the ICP-OES and set up the Gas Liquid Separator. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 157: Gas Liquid Separator (Gls

    Teflon coated face Reaction zone Drain channel black connector Sample channel green connector Reductant channel red connector Acid channel blue connector Figure B-5. Schematic of Gas Liquid Separator Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 158 The drain is the only tubing that needs to be connected in the opposite direction. That is, the tubing is passed under the pump so that the drain outlet is on the left hand side. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 159 ❖ To fit the pump tubing 1. Release the plungers to free the pump platens. 2. Feed the pump tubing around the pump rollers. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 160 This gives a good compromise set of operating conditions. If better sensitivity is required for a particular element, this element should be used for optimization. B-10 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 161 The default pump speed is 30 rpm. Good results can be obtained with pump speeds up to 45 rpm. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) B-11...
  • Page 162 Optional Accessories Hydride Generation B-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 163 Legal Documents Appendix C Contents • WEEE Compliance page C-2 • Declaration of Conformity page C-3 • Health and Safety Form page C-5 Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)

  • Page 164: Appendix C Legal Documents

    RoHS For additional information about the Restriction on Hazardous Substances (RoHS) Directive for the European Union, search for RoHS on the Thermo Fisher Scientific European language websites. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 165 Legal Documents Declaration of Conformity Declaration of Conformity Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 166 Legal Documents Declaration of Conformity iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 167 No ticks go to section 5 environment gas under other harmful explosive substances pressure Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Health and Safety Form (P/N 1342350, Revision F) Page 1 of 2...
  • Page 168 Describe the decontamination process Return Number Name of authorized person (block letters) Date Signature Company stamp iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific Health and Safety Form (P/N 1342350, Revision F) Page 2 of 2...

  • Page 169: Glossary

    – electron which accelerates through a potential difference of one volt. BLK abbr. for a blank (analyte). f femto (10 °C degrees Celsius. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 170 PCB printed circuit board. I/O input/output. PCL abbr. for Process Control Language. IP internet protocol. PEEK Polyether ether ketone. iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 171 Electronic Equipment Directive. Provides guidelines EU directive on the restriction of the use of certain for disposal of electronic waste. hazardous substances in electrical and electronic equipment. s second. Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 172 Glossary: WEEE–WEEE iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

  • Page 173: Index

    LabBooks 7-13 6-28 bubbler extraction system A-16 5-10–5-11 camera Field Service Test Kit 6-21 capillary tubing fire hazard 3-14 carbon deposits flammable liquids Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 174 6-19 on-line hydride generation optical system specification standard aqueous optical tank 6-21 optimization options examples nebulizer 3-12 lab coat organic sample spray chamber 3-14 LabBook window 6-23 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...
  • Page 175 Qtegra Help page cleaning quartz center tube 3-11 cyclonic 3-14 quartz window drain 6-8, 6-12 Sprint Valve A-16, A-18 rapid sample introduction system reinsertion A-20 Sprint Valve Configurator Thermo Scientific iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C)
  • Page 176 Get Ready 6-22 coil LabBook 6-23 glassware ignition spark plasma going out unexpectedly problems with plasma ignition tubing yttrium bullet test lifespan A-17 material 7-12 iCAP 7000 Plus Series ICP-OES Operating Manual (P/N BRE0004150, Revision C) Thermo Scientific...

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