ThermoFisher Scientific iCAP 7400 ICP-OES Manuals

Manuals and User Guides for ThermoFisher Scientific iCAP 7400 ICP-OES. We have 1 ThermoFisher Scientific iCAP 7400 ICP-OES manual available for free PDF download: Operating Manual

ThermoFisher Scientific iCAP 7400 Operating Manual (178 pages)

ICP-OES systems

Brand: ThermoFisher Scientific | Category: Laboratory Equipment | Size: 5 MB

Table of Contents
5
Data Input
12
Signal Words
12
Typographical Conventions
12
Using this Manual
12
Viewpoint Orientation
12
Topic Headings
13
Reference Documentation
14
Assistance
15
Contacting Us
15
Suggestions to the Manual
15
Optional Accessories
17
Required Accessories
17
System Accessories
17
Functional Description
20
Introduction
21
Instrument Specification
22
Optical System
23
Detector Specifications
24
Detector Mode
25
Plasma Source Specification
25
Plasma Viewing Specifications
25
Sample Introduction Specifications
26
Center Tube Options
29
Operating Noise Level
29
Sample Introduction System
29
Nebulizer Options
30
Pump Tubing Options
30
Internal Standards Kit
31
Heavy Organic Samples
32
Light Organic Samples
32
Organic Solvent Analysis
32
Volatile Organic Samples
33
Argon Humidifier Accessory
34
High Dissolved Solid Samples
34
Aerosalt Nebulizer
35
Parallel Path Nebulizer
35
Sheath Gas Adaptor
35
HF Samples
36
Observing this Manual
38
Safety
38
Safety Symbols and Signal Words in this Manual
38
Safety Symbols on the Instrument
38
Rating Plate
39
Intended Use
40
Intended User
40
Permitted Materials
41
Electric Safety Precautions
42
Impaired Safety Protection
42
In Case of Emergency
43
Residual Hazards
44
Personal Protective Equipment
45
Installation
48
Safety Guidelines for Installation
48
Spectrometer Dimensions
49
Before Installation
50
Installation Requirements
50
Location Requirements
50
Environmental Requirements
51
Electrical Requirements
52
Gas Requirements
53
Recirculating Chiller
55
Waste Storage
55
Spectrometer Fume Extraction
56
Communications Interface
58
Sample Fume Extraction
58
Spectrometer Communication Requirements
58
Data Station Requirements
59
Installation Checklist
59
System Operation
63
Safety Guidelines for Operation
64
LED Indicators
65
Preparing the System for Use
65
Instrument Optimization
66
Method Optimization
66
Setting the Pump Tension
67
Standard Sample Introduction Glassware Assembly
67
Duo Torch Assembly
68
Radial Torch Assembly
72
Connection of Pump Tubing
76
Radial View Interfaces on a Duo Instrument
79
Example Standard Operating Procedures
81
Preparing the System
81
Lighting the Plasma
82
Setting up Analyses
85
Running the Analysis
88
Reporting Results
89
Exporting Labbooks
90
Auto Peak Adjust
92
Shutting down the System
94
Safety Guidelines for Troubleshooting
98
Troubleshooting
98
Argon Gas
99
Problems with Plasma Ignition
99
Ignition Spark
100
RF Power to the Coil from the RF Generator
100
Problems with Plasma Going out Unexpectedly
101
Resolving Problems with Analytical Results
101
Poor Precision
103
Resolving Specific Analytical Problems
103
Poor Accuracy/Feedback
107
Poor Detection Limits
107
Replacing the Pump Tubing
108
Suggested Maintenance in Case of Poor Precision and Detection Limits
108
Preventing Blockage of the Nebulizer
109
Removing Solids from the Nebulizer
110
Maintenance
114
Safety Guidelines for Maintenance
114
Cleaning and Decontaminating the Sample Introduction System
115
Cleaning the Instrument
115
Cleaning the Torch
115
Cleaning the Spray Chamber
116
Cleaning the Nebulizer
117
Cleaning the Purged Optical Path Window
117
Cleaning the Radial View Interfaces
118
Preventive Maintenance
120
Water Chiller
120
Gas Filters
121
Torch Alignment
121
Water Filter
121
Thermo Fisher Scientific Service
122
Returning Parts
123
Services to be Performed by Thermo Fisher Scientific Service Only
123
Appendix A Advanced Hardware

126
- Sprint Valve
  126
- Supported Autosamplers
  126
- Functional Description
  126
- Operational Settings
  132
- Description of Timings
  137
- Manual Control Features
  138
- Manual Sampling Using the Sprint Valve
  140
- Routine Maintenance
  140
- Additional Gas Accessory
  148
- Installing the Additional Gas Accessory
  149
Appendix B Optional Accessories

151
- Autosampler
  152
- Autosampler Setup
  152
- Ultrasonic Nebulizer
  153
- Hydride Generation
  154
- On-Line Hydride Generation Kit
  154
- Integrated Hydride Generation Kit
  156
- Gas Liquid Separator (GLS
  157
Appendix C Legal Documents

164
- Glossary
  169
- Index
  173

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ThermoFisher Scientific iCAP 7400 ICP-OES Manuals

ThermoFisher Scientific iCAP 7400 Operating Manual (178 pages)

Table of Contents

Appendix A Advanced Hardware

Appendix B Optional Accessories

Appendix C Legal Documents

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