Waltron 9096 User Manual
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Waltron 9096 User Manual

Degassed cation conductivity analyzer
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EXPERTS IN WATER CHEMISTRY SINCE 1903
9096 Degassed Cation Conductivity Analyzer
User Manual
101-046-B.3

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Summary of Contents for Waltron 9096

  • Page 1 EXPERTS IN WATER CHEMISTRY SINCE 1903 9096 Degassed Cation Conductivity Analyzer User Manual 101-046-B.3...

  • Page 2: Waltron Customer Commitment

    It is Waltron’s commitment to provide the customer with timely and accurate technical service and support. Waltron fully expects the customer to be satisfied with the quality, performance, and cost of this product. If there are any questions or concerns regarding this product, please feel free to contact Waltron at (908)-534-5100.

  • Page 3: Safety

     Follow all regulations and warning labels when disposing of chemicals. Do not mix chemicals. To obtain analyzer safety information or Safety Data Sheets (SDS), please contact Waltron or logon to www.waltron.net. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 4: Warranty Agreement

    If, within one year from the date of shipment, the customer experiences any equipment defects or is not satisfied with the analyzer manufacturing, Waltron will repair, or at its option, replace any defective part(s) free of charge. This warranty requires that the defective part(s) be returned to Waltron with shipping charges prepaid.

  • Page 5: Checklist Of Materials

    Checklist of Materials CHECKLIST OF MATERIALS  In order to ensure customer satisfaction, Waltron does its best to provide adequate and timely packaging and shipping services. Please perform the following after receiving a shipment:  Inspect all shipping containers upon receipt and record any visible damage. If there are any outward signs of damage, please retain all containers and packages for inspection by carrier.

  • Page 6: Table Of Contents

    Analyzer Initial Start-Up ................23 Preparing the Analyzer for Start-Up ................... 23 4.1.1 Installing Cation Resin Bottle ....................23 4.1.2 Installing Decarbonization Column ..................25 Putting the Analyzer Online ......................25 Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 7 Scheduled Maintenance ......................47 Replacing Cation Resin ........................ 48 Replacing Decarbonization Catridge ................... 50 Spare Parts ....................51 Appendix A: USB Data Logger Extraction (Optional) ........52 Memory Manager Menu Items: ....................52 Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 8: Overview

    Four 0/4 – 20 mA for measured signals Analog Outputs: Serial I/O for Signals: RS422/RS485 (optional) General Alarm, Low Degassing Efficiency Alarm, Resin Alarms: Exhausted Alarm Optional: Additional inputs and outputs available Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 9: Safety Precautions, Instructions, And Hazards

     Waltron shall not be liable for errors contained herein and/or for an incorrect use of the analyzer. The department head and analyzer’s users must be sure to read and observe the following instructions and to apply all the national and local regulations and laws regarding workers health and safety.

  • Page 10: List Of Warnings And Potential Dangers

    Only qualified personnel fully trained on analyzer use and maintenance is allowed to proceed with service operations on the unit. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 11: Sample

    The analyzer’s transmitter enclosure is IP67 (NEMA 6).  Protection against indirect contacts is guaranteed by efficient grounding of all isolated metal masses. Grounding screw is located inside the electrical enclosure, in the lower right position. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 12: Introduction

    “high” cation conductivity indication, so removing the carbon dioxide becomes the final step in providing an accurate cation conductivity value. The new 9096 Degassed Cation Conductivity Analyzer from Waltron removes carbon dioxide using a desorption column. Using this method, 93.5% of the CO is removed in the 45 seconds the sample is in the desorption column.
  • Page 13 (DCC). Oxygen (as tracer) degasing; real reactor 100% Measuring values, real reactor Fitting curve, ideal reactor Eff. = 93,5 % t = 45 sec Time [sec] Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 14: Flow & Component Diagram

    Introduction FLOW & COMPONENT DIAGRAM Figure 2.1: Flow & Component Diagram. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 15: Wet-Section

    Introduction WET-SECTION Figure 2.2: Waltron 9096 Analyzer front view. ELECTRONICS The microprocessor and its PCB assembly are located in the electronic section. It provides control for the entire analyzing system. It handles the analyzer operations, it collects all the information and data coming from the different analyzer devices and it controls all the I/O for communication with the user touchscreen interface and transfer data equipment.

  • Page 16: Installation

    Installation 3 INSTALLATION RECEIVING The Waltron 9096 Desgassed Cation Conductivity Analyzer is assembled and fully tested for proper performance. Before proceeding with analyzer installation, it is recommended to:  Check that the box and analyzer have not been damaged during transportation.

  • Page 17: Mounting Schematics

    Installation MOUNTING SCHEMATICS Figure 3.1: The dimensions for mounting the analyzer. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 18: Sample Connections

    Installation SAMPLE CONNECTIONS Sample Inlet 6mm Swagelok Sample Outlet To Atmospheric Pressure Figure 3.2: Sample Connections. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 19: Electrical Connections

    In case of loss of power, the analyzer stops and automatically restarts into standby mode as soon as power is restored. No maintenance should be carried out inside the transmitter without first switching off the power. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 20: Transmitter Enclosure

    Figure 3.3: Transmitter enclosure. Figure 3.4: Electrical connections inside the transmitter housing. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 21: Terminal Block Connections

    1. Prior to installing the wires to the push-in spring terminal blocks of the power supply unit and the base unit, the wire coating should be stripped back approximately ¼” to expose Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 22: Ac Power Connection

    AC POWER CONNECTION 3.6.3 The Waltron 9096 Degassed Cation Conductivity Analyzer is designed for operation with 110- 220Vac, 48-63 Hz power. All the connections must be made in accordance with national or local regulations. It is always recommended that the analyzer is connected to the mains via a circuit breaker or an isolating switch installed near the unit.

  • Page 23: User Signal Connections

    4-20 mA; CC conductivity Option board OUT 6 Analog 4-20 mA; DC conductivity Option board OUT 8 Analog 4-20 mA; pH calculation 0-20 mA; calculated resin Option board OUT 10 Analog consumption Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 24: Analyzer Initial Start-Up

    Note the date and time you are exchanging the resin bottle. Remove cap from new bottle of resin. Resin has been pre-rinsed. Inside the cap is a gasket; remove it from the cap. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 25 Tighten about ¼ turn after the top of the bottle contacts the gasket. Note: If it leaks slightly, it can be tightened further until it stops leaking. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 26: Installing Decarbonization Column

    It is important to note that if Waltron’s pre-rinsed resin is not used, it may take anywhere from several hours to several days for the cation and degassed cation conductivities to read correctly.

  • Page 27: User Interface

    Figure 5.1: User interface main display screen. MAIN SCREEN NAVIGATION The main screen displays:  Specific Conductivity  Cation Conductivity  Degassed Cation Conductivity  Calculated pH  Flowrate  Temperature Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 28 Selecting the second option from the Operating Menu, Ion Exchange Capacity, will show the calculated life of the resin remaining before it will need to be replaced. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 29 Alternatively, pressing the button in the lower right hand corner of the main measurement screen will toggle through the above mentioned views. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 30: User Log On Navigation

    To logon, press the logon button. An ID input box will appear and pressing the input box where master is shown will provide options for the logon ID that will be used. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 31 ID. Type in the correct password and press the Enter button. Appropriate access (based on logon id used) will now be granted and the user will have permissions available to them. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 32: Alarm Log

    Details button can be pressed to show more information about the alarm. Pressing the confirm button while an alarm is highlighted will acknowledge the alarm and remove it from the list. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 33: Analog Outputs

    Open the main device menu by pressing the bottom left hand corner of the main display screen. Select the configuration menu, and then scroll down to Analog Outputs. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 34 (20mA). Pressing OK will return to the previous menu and save any changes made to the configuration. Pressing Cancel will return the previous menu without saving any changes that were made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 35 (20mA). Pressing OK will return to the previous menu and save any changes made to the configuration. Pressing Cancel will return the previous menu without saving any changes that were made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 36 (20mA). Pressing OK will return to the previous menu and save any changes made to the configuration. Pressing Cancel will return the previous menu without saving any changes that were made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 37 (20mA). Pressing OK will return to the previous menu and save any changes made to the configuration. Pressing Cancel will return the previous menu without saving any changes that were made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 38 (20mA). Pressing OK will return to the previous menu and save any changes made to the configuration. Pressing Cancel will return the previous menu without saving any changes that were made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 39: Calibration Menu

    (SC), Cation Conductivity (CC), and Degassed Cation Conductivity (DC) sensors. Select the desired sensor and select Calibration Logbook. The calibration logbook will show the date and result for the sensor’s calibration history. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 40 User Interface Selecting one of the calibrations and pressing the Details button will provide additional information about the date, time, and type of calibration that was performed. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 41 User Interface Select Calibration Values to view the cell constant for the conductivity sensor. The current cell constants for that conductivity sensor are shown. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 42: Configuration

    Configuration. From the Configuration menu select Analog Inputs > Universal Input 1 > Configuration. Press the yellow box for Operation mode and select Conductivity Measurement from the list of options. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 43 HCL 0 to 18 %, HCL 22 to 44 % Pressing the OK button will save configuration changes. Pressing Cancel will return to the previous screen without saving any of the changes made. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 44: Operation

    Obtain the known conductivity of the measured sample (in uS/cm). Use of a secondary conductivity measurement device is required. This will be the value for κ in the equation. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 45 The Calibration folder contains folders for the Specific Conductivity (SC), Cation Conductivity (CC), and Degassed Cation Conductivity (DC) sensors. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 46 Rel. Cell const. 2 field. Once both fields have been updated with the new value, press the OK button to save. Pressing cancel will exit the menu without Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 47 The entire procedure above can be repeated for the Cation Conductivity sensor. Note: the DC sensor relies on the CC sensor calibration and does not need to be calibrated individually. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 48: Maintenance

    7 MAINTENANCE SCHEDULED MAINTENANCE Basic maintenance of the Waltron 9096 Analyzer requires that the cation resin bottle and soda lime cartridge be replaced periodically. In addition, the user should perform a regular 'visual overall-check' of the wet section for immediate corrective measures, e.g. in case of leaks etc.

  • Page 49: Replacing Cation Resin

    Turn off sample flow to the analyzer and remove the old resin bottle from the analyzer. Remove cap from new bottle of resin. Resin has been pre-rinsed. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 50 Turn on sample flow to the analyzer and wait for approximately one hour for the Cation Conductivity and Degassed Cation Conductivity readings to drop to the expected value. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 51: Replacing Decarbonization Catridge

    Unscrew the exisiting cartridge from the housing block. Remove plugs covering the inlet (bottom or cartrdige) and outlet (top of cartridge) holes of the new cartridge. Screw the new cartridge into place. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 52: Spare Parts

    Pre-Rinsed Resin Bottle (with resin) W1234-609 Table 8.2: Spare Parts Listing. Description Part Number Air Pump Exchange Set P1000-210 Flowmeter L1000-015 Water Pump Exchange Set P1000-220 USB Data Logging Interface Adapter P1000-230 Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

  • Page 53: Appendix A: Usb Data Logger Extraction (Optional)

    NOTE: The "Recorder Update" and "Recorder Backup" functions are available only if the extra code "Recording" is enabled. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...
  • Page 54 Pressing the "OK" button saves the current configuration to the flash drive and overwrites the previous file. Waltron User Manual 101-046-B.3 9096 Degassed Cation Conductivity Analyzer...

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