Techne FSC496D Operator's Manual

Techne FSC496D Operator's Manual

Sample concentrator

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Sample
Concentrator
OPERATOR'S MANUAL
Issue 10
8/08

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Summary of Contents for Techne FSC496D

  • Page 1 Sample Concentrator OPERATOR'S MANUAL Issue 10 8/08...
  • Page 3: Table Of Contents

    CONTENTS PAGE INTRODUCTION Warning Operator safety Specification Installation Diagram of Sample Concentrator Guarantee OPERATION Preparation Operation ADDITIONAL INFORMATION User maintenance Solvent evaporation temperatures Diagram of gas chamber Replacement parts...
  • Page 4: Introduction

    Please read all the information in this user manual before using the Sample Concentrator. The Techne Sample Concentrator has been designed to provide a quick and convenient method of accelerating the concentration by evaporation of solvents from samples prior to analysis. It is designed to work in conjunction with Techne DB-3, DB-3A or DB-3D Dri-Block heaters*.
  • Page 5: Operator Safety

    SAFETY ADVICE BEFORE USE OPERATOR SAFETY All users of Techne equipment must have available the relevant literature needed to ensure their safety. It is important that only suitably instructed personnel operate this equipment, in accordance with the instructions contained in this manual and with proper safety standards and procedures.
  • Page 6: Diagram Of Sample Concentrator

    The gas pressure should be adjusted as required at the reducing valve but should not exceed 2 psi. Pressure in excess of 2 psi will cause gas to be vented and wasted. Place the Techne Dri-Block heater onto the base of the Sample Concentrator. It is positioned by ®...
  • Page 7: Guarantee

    This user’s manual has been prepared solely for the convenience of Techne customers and nothing in this manual shall be taken as a warranty, condition or representation concerning the description,...
  • Page 8: Operation

    (block number F3506) you would place a needle in all the holes labelled C and all holes labelled D. Only Sample Concentrators with the part number FSC496D or a replacement head part number 6104202 will have the 96 well array.
  • Page 9 96 well hole array (12 x 8 matrix as above) Press each needle firmly, pointed end first, through the guide holes and through the sealing pad behind so that it is held firmly in position. Build up the desired pattern of needles to suit the arrangement of test tubes to be used.
  • Page 10: Operation

    PROCESSING OF SAMPLES Warning - remember high temperatures are dangerous. The heater, insert blocks, sample vessels, needles and samples may be very hot. Always take the precautions listed earlier in this manual. By turning the carriage handle, on the right hand side, counter clockwise raise the gas chamber to take the needles well away from the heater.
  • Page 11: Additional Information

    To replace the sealing pad After many repeated needle insertions the self sealing property of the sealing pad may start to degrade. Spare pads can be obtained from your supplier or from Techne. Replacing the pad is simply accomplished as follows: •...
  • Page 12: Solvent Evaporation Temperatures

    SOLVENT EVAPORATION TEMPERATURES IUPAC Name Common Name Boiling point (°C) at Pressure (mbar) at 1013 mbar pressure which b.p is 40°C 2-propanone Acetone 1-pentanol Pentyl alcohol Benzene Benzene 1-butanol Butyl alcohol 2-methyl-2-propanol Tert-butyl alcohol Chlorobenzene Chlorobenzene Chloroform Trichloromethane Cyclohexane Cyclohexane Ethoxyethane Diethyl ether Atmospheric...
  • Page 13 SOLVENT EVAPORATION TEMPERATURES continued IUPAC Name Common Name Boiling point (°C) at Pressure (mbar) at 1013 mbar pressure which b.p is 40°C Methanol Methyl alcohol Dichloromethane Methylene chloride Atmospheric Pentane Pentane Atmospheric Propan-1-ol Propyl alcohol 1,1,1,2,2-pentachloroethane Pentachloroethane 1,1,2,2-tetrachloroethane Tetrachloroethane 1,1,1 -trichloroethane Trichloroethane Tetrachloromethane Carbon tetrachloride...
  • Page 14: Diagram Of Gas Chamber

    DIAGRAM OF GAS CHAMBER Matrix plate Sealing plate Support strip Spacer...
  • Page 15: Replacement Parts

    REPLACEMENT PARTS AND ACCESSORIES The following replacement parts and accessories may be obtained from your supplier or from Techne. Part Number Description F7209 Pack of 100 x 76mm long needles F7210 Pack of 100 x 127mm long needles FSC4NCS Pack of PTFE coated needles, 100 x 76mm long...
  • Page 16 United Kingdom Tel: +33 1 64 45 13 13 Tel: +44 (0)8449 360234 Fax: +33 1 64 45 13 00 Fax: +44 (0)8449 360235 e-mail: bsf@bibby-scientific.fr email: techne@bibby-scientific.com www.bibby-scientific.com www.bibby-scientific.com Bibby Scientific Italia Srl Techne Inc. Via Alcide de Gasperi 56...

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