Operation Manual Shodex GPC KD-800 series Version 211018E Operation Manual Shodex™ GPC KD-800 series (Please read this manual carefully to achieve the best and consistent column performance for a long time) Important Handling Instructions Caution! • Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column and understand their proper handling methods to prevent potential health hazards or death from occurring.
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Operation Manual Shodex GPC KD-800 series Version 211018E F6028225 GPC KD-802.5 8.0 x 300 ≥ 17,000 400 - 10,000 20,000 F6028230 GPC KD-803 8.0 x 300 ≥ 17,000 1,000 - 50,000 70,000 F6028240 GPC KD-804 8.0 x 300 1,500 ≥ 17,000...
Operation Manual Shodex GPC KD-800 series Version 211018E 30% m-Cresol/Chloroform 30% o-Chlorophenol/Chloroform 30% HFIP/Chloroform Tetrahydrofuran (THF) Chloroform Dimethylsulfoxide (DMSO) Carbon tetrachloride Ethyl acetate Hexane Acetonitrile Methanol Water O: Can be used X: Cannot be used (1) The standard solvent is N,N-Dimethylformamide (DMF).
Operation Manual Shodex GPC KD-800 series Version 211018E Sample Preparation (1) If possible, use the eluent for analysis to dissolve or dilute samples. If this is difficult, use a solvent which has a composition that is as close as possible to the eluent's composition, but which fully dissolves or dilutes the sample.
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Operation Manual Shodex GPC KD-800 series Version 211018E (3) Set the initial flow rate at less than 0.3 mL/min and start the system. If using the column at an elevated temperature, keep a low flow rate until the temperature of the column reaches to the set temperature, and then gradually increase the flow rate to the desired.
Operation Manual Shodex GPC KD-800 series Version 211018E 7.4. Column Cleaning Problems in peak shapes and elution timing changes or elevated column pressure etc. are often caused by insoluble or adsorbing components present in the eluent and reagents being deposited inside the column.
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3-3 If the Shodex product is disposed of 3-4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K.K. 3-5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below: a.
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