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1 OUTLINE OF SOLID-STATE NMR MEASUREMENT
1.1
SOLID-STATE NMR SYSTEM
High-Resolution solid-state NMR measurement by techniques such as cross-polarization
magic-angle spinning (CPMAS) method becomes possible when you add optional at-
tachments (such as a probe for the solid-state measurement) to the standard composition
of JNM-ECA/ECX series. Moreover, multinuclear observation and the measurement un-
der variable temperatures (VT) are also possible with this system.
If the Status cable is connected to the Status connector of the solid probe, the program
and the spectrometer will enter the solid mode automatically. The instrument is in the
solid mode if the LIQUID lamp of the INT CONT unit located behind the door on the
right of the front of the spectrometer is turned off.
LIQUID lamp
Fig. 1.1 INT CONT unit
The procedure for the measurement and processing in the solid mode are the same as
those for the solution mode. In this manual, measuring methods peculiar to the solid-state
NMR will be explained.
NMECAXS_V50-SLD-2
1-1
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