Christ RVC 2-33 CDplus Operating Manual
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Christ RVC 2-33 CDplus Operating Manual

Rotational vacuum concentrator with infrared heating
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Translation of the original operating manual
sb-bs
Rev. 3.6 of 22/11/2021
RVC 2-33 CDplus; ;with infrared heating
Version 08/2009
RVC 2-33 CDplus
with infrared heating
Operating Manual
part no. 100244
Rotational Vacuum
Concentrator
Please retain for later use!

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  • Page 1 Translation of the original operating manual sb-bs Rev. 3.6 of 22/11/2021 RVC 2-33 CDplus; ;with infrared heating Version 08/2009 RVC 2-33 CDplus with infrared heating part no. 100244 Rotational Vacuum Concentrator Operating Manual Please retain for later use!
  • Page 2 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 2 / 105 Translation of the original operating manual...
  • Page 3 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating In case of inquiries, please state the following numbers: Order number: Serial number: © Copyright by Martin Christ Gefriertrocknungsanlagen GmbH An der Unteren Söse 50 37520 Osterode am Harz Germany Tel.:...
  • Page 4 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 4 / 105 Translation of the original operating manual...

  • Page 5: Table Of Contents

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Table of contents General information ......................9 Importance of the operating manual .................. 9 Intended use ........................9 Warranty and liability....................... 11 Copyright ........................12 Explanation of symbols ....................12 Standards and regulations ....................12 Scope of supply ......................
  • Page 6 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Table of contents Procedures in the event of hazards and accidents ............29 3.10 Maintenance and cleaning of the rotational vacuum concentrator ........30 3.11 Measures to ensure the safe operation of the rotational vacuum concentrator ....31 3.12...
  • Page 7 11.1 Mathematical relations ....................88 11.2 Rotor program......................... 89 11.3 Overview of evaporation times (RVC 2-33 CDplus with infrared heating) ......90 11.4 Brief operating instructions ..................... 92 11.5 EC declaration of conformity ................... 95 Declaration of conformity – China RoHS 2 ..............97 11.6...
  • Page 8 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Table of contents Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 8 / 105 Translation of the original operating manual...

  • Page 9: General Information

    • General evaporation tasks in laboratories Any other use beyond this area of application is regarded as improper use. Martin Christ Gefriertrocknungsanlagen GmbH cannot be held liable for any damage resulting from such improper use. Evaporation of solvent-containing products (non-aqueous media) In terms of the corrosion resistance, the use of organic solvents in aqueous solutions is acceptable.
  • Page 10 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 1 General information With the exception of hydrochloric acid, nearly all standard solvents can be used. For further details, see the table below. Solvent Stainless Aluminium EPDM Borosilicate Experience steel glass...

  • Page 11: Warranty And Liability

    Use of the rotational vacuum concentrator within hazardous locations with an explosive atmosphere. • Use of the rotational vacuum concentrator with unauthorised additions or conversions without the written approval by Martin Christ Gefriertrocknungsanlagen GmbH. • Use of the rotational vacuum concentrator with accessories that have...

  • Page 12: Copyright

    Pos : 8 /200 C hrist/370 RVC- BA (ST ANDARDM ODULE)/010 Allgemei ne Informati onen/010-0040 Ur heberr echt @ 25\m od_1404984955490_68.docx @ 186547 @ 2 @ 1 → Copyright The copyright concerning the operating manual remains with Martin Christ Gefriertrocknungsanlagen GmbH. The operating manual is solely intended for the operator and their personnel.

  • Page 13: Layout And Mode Of Operation

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 2 Layout and mode of operation Pos : 17 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /020 Aufbau und Wirkungsweis e/020 Aufbau und Wirkungsweis e=========================== @ 25\m od_1404984977875_68.docx @ 186589 @ 1 @ 1 →...

  • Page 14: Name Plate

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 2 Layout and mode of operation Pos : 22 /200 C hrist/371 R VC-BA ( PROJ EKT E)/R VC 2-33 CD plus IR/020 Aufbau und Wirk ungsw eise/020-0010-0020 T ypenschil d R VC 2-33 IR @ 31\m od_1407484033115_68.docx @ 208942 @ 3 @ 1 →...

  • Page 15: Mode Of Operation

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 2 Layout and mode of operation Pos : 24 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /020 Aufbau und Wirkungsweis e/020-0020 Wirk ungsw eise--------------------------------------------------------- @ 25\m od_1404984979651_68.docx @ 186617 @ 2 @ 1 →...

  • Page 16: Advantages Of The Rotational Vacuum Concentration

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 2 Layout and mode of operation Fig. 5: Vapour pressure curves of commonly used organic solvents Pos : 26 /010 U nivers almodule/ Leerz eile @ 0\m od_1202116244500_0.doc x @ 114 @ @ 1 Pos : 27 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /020 Aufbau und Wirkungsweis e/020-0020- 0010-0010 Vorteile der Rotations-Vak uum- Konz entrati on @ 25\m od_1404984981567_68.docx @ 186645 @ 4 @ 1...

  • Page 17: Safety

    Pos : 33 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0010 Besc hilder ung des Ger äts RVC @ 25\mod_1404985001192_68.docx @ 186687 @ 2 @ 1 → Marking of the unit The following symbols are used for Christ RVC: Dangerous voltage On (Power)

  • Page 18: Explanation Of The Symbols And Notes

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 35 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0020 Sym bol- und Hi nw eiserkl ärungen @ 25\m od_1404985002176_68.docx @ 186701 @ 2 @ 1 →...

  • Page 19: Responsibility Of The Operator

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 37 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0030 Verantw ortung des Betr eibers @ 25\m od_1404985003110_68.docx @ 186715 @ 2 @ 1 →...

  • Page 20: Requirements Concerning The Personnel

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Additional points concerning the evaporation of solvent-containing products With regards of corrosion resistance, the use of some organic solvents in aqueous solutions is acceptable. Under certain circumstances, the evaporation of products containing solvents may lead to the formation of explosive mixtures.

  • Page 21: Informal Safety Instructions

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Specialised personnel Due to their special training, knowledge, experience and familiarity with the relevant regulations, specialised personnel are in the position to perform any tasks assigned to them and to autonomously identify and prevent possible hazards.

  • Page 22: Safety Notes Concerning The Transport, Set-Up And Connection And Initial Start-Up Of The Freeze-Dryer

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 43 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0060 Sic her heitshi nweis e Tr ansport, Aufs tell ung und Ansc hluss , Inbetriebnahm e @ 25 \mod_1404985005847_68.doc x @ 186757 @ 2 @ 1 →...

  • Page 23: Hazards Caused By An Improper Connection

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 51 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0060- 0040 Gefahr en durc h uns ac hgem äßen Anschl uss RVC @ 86\mod_1635935971587_68.docx @ 906311 @ 3 @ 1 3.6.4...

  • Page 24: Electrical Safety

    3 Safety 3.7.1 Electrical safety CHRIST rotational vacuum concentrators are units of safety class I. The RVCs are equipped with a three-wire power cord and a 230 VAC safety plug with earthing contact. Please comply with the following points in order...

  • Page 25: Hazards Due To Hot Surfaces

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety 3.7.4 Hazards due to hot surfaces Risk of burns on hot surfaces! During operation of the rotational vacuum concentrator, the housing, lid and rotor chamber of the unit can reach surface temperatures of over +50°C .

  • Page 26: Hazards Caused By Contaminated Condensate (Defrosting Water)

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety 3.7.7 Hazards caused by contaminated condensate (defrosting water) Danger of poisoning/infection due to contact with the condensate (defrosting water) The condensate may contain harmful substances originating from the product.

  • Page 27: Hazards Due To The Evaporation Of Harmful Precursors

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety 3.7.9 Hazards due to the evaporation of harmful precursors If infectious, toxic, pathogenic or radioactive substances are to be evaporated, the user is responsible for ensuring that all applicable safety regulations, guidelines, precautions and safety measures are observed.

  • Page 28: Safety Devices

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 73 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0080 Sic her heitsei nrichtungen------------------------------------------------------ @ 86\m od_1635952536376_68.docx @ 906388 @ 2 @ 1 →...

  • Page 29: Procedures In The Event Of Hazards And Accidents

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Pos : 83 /200 C hrist/370 R VC-BA ( STAND ARDMODU LE) /030 Sic herheit/030-0090 Verhalten bei Gefahr en und U nfällen @ 25\m od_1404985018691_68.docx @ 186925 @ 2 @ 1 →...

  • Page 30: Maintenance And Cleaning Of The Rotational Vacuum Concentrator

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 3 Safety Chemical burns: • Eyes: Rinse the eyes thoroughly with plenty of water with the lid gap wide open for at least 15 minutes (eyewash bottle). Consult an ophthal- mologist immediately even if there are no immediate symptoms. If possible, continue rinsing the eyes during the transport to the ophthal- mologist.

  • Page 31: Measures To Ensure The Safe Operation Of The Rotational Vacuum Concentrator

    Take the rotational vacuum concentrator immediately out of operation in the event of malfunctions. Eliminate the faults (see chapter 7 - "Malfunctions and error correction")or contact the service department of Martin Christ Gefriertrocknungsanlagen GmbH (see chapter 7.2 - "Service contact"). •...

  • Page 32: Remaining Hazards

    3.12 Remaining hazards All Christ rotational vacuum concentrators were built state- of- the- art and according to the accepted safety rules. However, danger to life and limb of the operator, or of third parties, or impairments of the units or other material assets cannot be completely excluded when the units are being used.

  • Page 33: Storage And Transport

    Remove the packaging material. • Lift the RVC upwards and out of the crate/cardboard box. When lifting the unit, always reach under it from the side. The rotational vacuum concentrator RVC 2-33 CDplus with infrared heating weighs approx. 49 kg! CAUTION •...

  • Page 34: Transport Safety Device

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 4 Storage and transport Pos : 99 /200 C hrist/371 R VC-BA ( PROJ EKT E)/R VC 2-33 CD plus IR/040 Lagerung und Tr ansport/040- 0040 Tr ansportsic herung RVC 2-33 IR @ 31\m od_1407484047030_68.docx @ 208985 @ 2 @ 1 →...

  • Page 35: Set-Up And Connection

    The operating voltage on the name plate must correspond to the local supply voltage! DANGER Christ rotational vacuum concentrators are units of protection class I. Rotational vacuum concentrators of this type have a three-wire power cord with an IEC C13 connector.

  • Page 36: Aeration And Air Injection Valve (Valve Block)

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 5 Set-up and connection Pos : 112 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/050 Aufstellung und Ansc hl uss/050- 0030 Ventilbloc k R VC 2-33 IR @ 31\mod_1407484066036_68.docx @ 209028 @ 2 @ 1 →...

  • Page 37: Vacuum Connections

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 5 Set-up and connection 3. Connection for aeration and air injection with inert gas 1 Aeration hose connection 2 Air injection hose nozzle 3 Fastener for non-required connection element; here: air filter If gas (e.g.

  • Page 38: Option: Pressure Control Valve And Vacuum Sensor

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 5 Set-up and connection Pos : 116 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/050 Aufstellung und Ansc hl uss/050- 0050 Option: Drucks teuerventil und Vakuumm esss onde R VC 2-33 IR @ 31\mod_1407484066541_68.docx @ 209042 @ 2 @ 1 →...

  • Page 39: Connection Of A Vacuum Pump And/Or A Cooling Trap

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 5 Set-up and connection Pos : 118 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/050 Aufstellung und Anschl uss /050- 0060 Ansc hlus s v on Vak uum pumpe und/oder Kühlfalle @ 25\m od_1404985088297_68.docx @ 187065 @ 2 @ 1 →...

  • Page 40: Condensation Of The Vapours Upstream Of The Vacuum Pump In A Cooling Trap

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 5 Set-up and connection Pos : 122 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/050 Aufstellung und Ansc hl uss/050- 0060- 0020 Kondensation der D äm pfe über Kühlfall e R VC 2-33 IR @ 31\m od_1407484067433_68.docx @ 209070 @ 3 @ 1 →...

  • Page 41: Option: Remote Control Of The Fd Cooling Trap Via Rvc

    5.6.2.1 Option: Remote control of the FD cooling trap via RVC If Christ freeze dryers are used as a cooling trap, they can be remote- controlled by the rotational vacuum concentrator. In this case, the cooling trap will be automatically activated by the rotational vacuum concentrator during the warm-up and evaporation phase.

  • Page 42: Operation

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 127 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/060 Betrieb======================================== @ 25\m od_1404985112182_68.docx @ 187092 @ 1 @ 1 Operation Pos : 128 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/060-0010 Erste Inbetriebnahm e++++++++++++++++++++++++++ @ 25\m od_1404985113012_68.docx @ 187106 @ 2 @ 1...

  • Page 43: Installation Of Rotors And Accessories

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 134 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/060-0040 Einsetzen v on R otoren und Z ubehör-------------------------------------- @ 25\m od_1404985115794_68.docx @ 187149 @ 2 @ 1 →...

  • Page 44: Installation Of Swing-Out Rotors

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 137 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/060-0040- 0020 Ei nsetz en von Aussc hwingrotor en ( außer 2-18) @ 25\m od_1404985117860_68.docx @ 187177 @ 3 @ 1 →...

  • Page 45: Tubes

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Evaporation with low capacity The tubes must be installed symmetrically so that the buckets and their inserts are loaded evenly to avoid imbalance. correct incorrect Fig. 15: Permissible loading of swing-out rotors with low capacity Pos : 140 /010 Univ ers almodul e/ Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1...

  • Page 46: Rotor Blocks

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 143 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/060-0040- 0030-0020 Aufnahm eblöck e ( auß er 2-18) @ 25\m od_1404985120658_68.docx @ 187219 @ 4 @ 1 →...
  • Page 47 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation • The balance point of the loaded bucket must be located considerably below the pivotal point. If the balance point is too near the pivotal point, the loaded bucket can be levered out of the bearings.

  • Page 48: Cdplus Control System

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 148 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050 CD plus Gerätes teuer ung--------------------------------------------- @ 25\mod_1404985146086_68.doc x @ 187260 @ 2 @ 1 CDplus control system The control system CDplus (“Concentrator Display plus”) stands for a...
  • Page 49 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Display (5) The main window of the display is divided into three areas: the values windows, the assignment of the function keys and the status bar. The main window shows the process data, e.g. set values and actual values, menues and process-relevant information (see figure).
  • Page 50 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Status bar (8) The status bar shows information regarding the lid status, the operating mode, the active phase, and pending information. The status bar is visible at all times.

  • Page 51: Mode

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 152 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050-0020 M odus (außer 2- 18) @ 25\mod_1404985148005_68.doc x @ 187288 @ 3 @ 1 6.5.2...
  • Page 52 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation • Close the lid. A menu appears: Fig. 26: Continuing the evaporation • Continue the process by selecting "Evaporation manual" or "Evaporation program". Stopping the warm-up phase prematurely During the warm-up phase, the functions "Open lid", "Continue with phase"...

  • Page 53: Main Menu

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 154 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050-0030 H auptmenü (außer 2- 18) @ 25\mod_1404985148924_68.doc x @ 187303 @ 3 @ 1 →...
  • Page 54 In the case of a set vacuum between 100 and 1,000 mbar, the set value of the safety pressure should be 10 mbar above the set vacuum. Alarm temperature (only for RVC 2-33 CDplus with infrared heating) The product temperature enables conclusions to be drawn concerning the end of the drying phase: When the medium has evaporated, the product sensor will no longer be cooled.

  • Page 55: Program Administration

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 158 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050-0030- 0020 Pr ogrammverw altung (Standar d) @ 64\m od_1556615179030_68.docx @ 689458 @ 4 @ 1 →...
  • Page 56 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Creating a new program A new program can be created based on a fixed program template and adapted to specific needs by changing the set values and by adding and deleting certain sections.
  • Page 57 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation The sections of a program can be adapted under "Edit program sections". The set values and sections are displayed in a tabular form. Fig. 36: Program section table •...

  • Page 58: Special Functions

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Program memory information • Select "Program memory information" from the program administration menu and confirm. Information concerning free program locations and sections are displayed: Fig. 39: Program memory information Pos : 159 /010 Univ ers almodul e/ Leerz eile @ 0\mod_1202116244500_0.docx @ 114 @ @ 1...

  • Page 59: Process And Equipment Information

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 162 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050-0030- 0040 Pr ozess- und Anl agen-Inform ationen @ 25\m od_1404985152870_68.docx @ 187359 @ 4 @ 1 →...

  • Page 60: Options

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Pos : 164 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/060 Betrieb/CD plus /060-0050-0030- 0050 Opti onen (auß er 2- 18) @ 25\mod_1404985153904_68.doc x @ 187373 @ 4 @ 1 →...
  • Page 61 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation Timer Warm-up You can set a warm-up time between 5 and 99 minutes. Temperature Warm-up During the warm-up phase, the rotor temperature is set to the set temperature. Click at button push If this function is activated, a brief sound signal can be heard whenever a key is pressed.
  • Page 62 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 6 Operation CDplus configuration In this menu, accessories (options) have to be configured: • VaCuum sensor • Remote control cold trap • Air injection • Triple TMM (not available for all RVC types) •...

  • Page 63: Malfunctions And Error Correction

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Pos : 167 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/070 Störungen und Fehlers uc he/070 Störungen und Fehlers uc he=========================== @ 25\m od_1404985185894_68.docx @ 187415 @ 1 @ 1 →...

  • Page 64: Process Messages

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Error Possible reason Correction • • Permissible imbalance exceeded The rotor will be stopped Balance the load and restart the immediately, the process will rotational vacuum concentrator.

  • Page 65: System Messages

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Pos : 176 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/070 Störungen und Fehlers uc he/070-0010-0030 Systemmel dungen @ 25\mod_1404985189332_68.docx @ 187471 @ 3 @ 1 →...
  • Page 66 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction • Pull the unit slightly over the edge of the desktop. Fig. 47: Pulling the unit slightly over the edge of the desktop • Tilt the unit upwards.
  • Page 67 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction • Prop the unit up. Fig. 49: Propping the unit up • Ensure that the centre of gravity of the unit is still above the desktop. If necessary, the unit must be held or secured by a second person.
  • Page 68 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction The emergency release system is actuated by way of two plugs. They are located under the unit and connected to the lid lock via a release cord.
  • Page 69 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction • Unscrew the plastic screws on the right and left halfway (approx. 4 mm). Fig. 53: Loosening the plastic screw with a cross-point screwdriver (left) Fig. 54: Loosening the plastic screw with a cross-point screwdriver (right) Version 08/2009, Rev.
  • Page 70 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Fig. 55: Loosened plastic screws • Grab the plastic screw and pull it out of the opening together with the plug. Fig. 56: Pulling out the plugs •...
  • Page 71 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Fig. 57: Unlock the lid locks The lid opens. Fig. 58: Opened RVC • After you have used the emergency lid release system, install the two plugs in reverse order.

  • Page 72: Small Flange Connections

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Pos : 181 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/070 Störungen und Fehlers uc he/070-0010-0050 Klei nflansc hv erbi ndungen @ 25\m od_1404985190199_68.docx @ 187485 @ 3 @ 1 →...

  • Page 73: Service Contact

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 7 Malfunctions and error correction Pos : 183 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/070 Störungen und Fehlers uc he/070-0020 Kontakt im Servicefall @ 25\mod_1404985191412_68.doc x @ 187499 @ 2 @ 1 →...

  • Page 74: Maintenance And Service

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Pos : 186 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/080 W artung und Instandhaltung/080 W artung und Ins tandhaltung=========================== @ 25\m od_1404985234940_68.docx @ 187513 @ 1 @ 1 →...
  • Page 75 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Cleaning of the rotational vacuum concentrator Risk of burns on hot surfaces After a drying process, some or all of the surfaces inside the chamber may still be hot.

  • Page 76: Rotor Chamber

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Pos : 191 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/080 W artung und Ins tandhaltung/080-0010- 0020 Rotork ammer R VC 2-33 IR - Ü bersc hrift @ 45\m od_1473323807471_68.docx @ 442078 @ 3 @ 1 8.1.2...
  • Page 77 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Fig. 65: Unit with an open lid • Set the mains power switch to OFF and disconnect the mains power cable. Danger of burns on hot surfaces!
  • Page 78 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service • Loosen all four fastening screws. Fig. 67: Loosening the fastening screws • Remove the magnetic coupling by lifting it up and off the rotor holder. Fig. 68: Removing the magnetic coupling •...
  • Page 79 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Fig. 69: Chamber and rotor holder to be cleaned Installing the rotor holder and rotor-side magnetic coupling Risk of crushing when installing the magnetic coupling The magnets of the magnetic coupling and the ones of the motor attract...

  • Page 80: Accessories

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service → 8.1.3 Accessories For the care of the accessories, special safety measures must be considered as these are measures that will ensure operational safety at the same time.

  • Page 81: Glass Breakage

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service 8.1.4 Glass breakage In the case of glass breakage, immediately remove all glass particles (e.g. with a vacuum cleaner). Replace the rubber cushions since even thorough cleaning will not remove all glass particles.

  • Page 82: Autoclaving

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Autoclaving The service life of the accessories essentially depends on the frequency of autoclaving and use. • Remove the existing O-rings so that the trapezoid notch can be reached by the hot steam.

  • Page 83: Return Of Defective Parts

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service Outside Germany: • Contact our agency in your country. All agencies are listed at www.martinchrist.de → [Sales Partners] If you would like to utilise our service, please state the type of your RVC and its serial number.
  • Page 84 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 8 Maintenance and service 2. Form for the return of defective parts This form is for the product-related data. They facilitate the assignment, and they enable the quick processing of the return. If several parts are returned together in one packaging, please enclose a separate problem description for every defective part.

  • Page 85: Disposal

    Pos : 212 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/090 Ents orgung/090- 0010 Ents orgung des R otati ons- Vakuum-Konzentr ators @ 26\m od_1404985276559_68.docx @ 187681 @ 2 @ 1 → Disposal of the RVC Martin Christ Gefriertrocknungsanlagen GmbH is a registered manufacturer of electric and electronic devices that are solely intended for commercial use.

  • Page 86: 10 Technical Data

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 10 Technical data Pos : 217 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/100 T ec hnisc he D aten/100 Tec hnische D aten R VC 2-33 IR ======================================= @ 31\m od_1407484103830_68.docx @ 209115 @ 1 @ 1 →...

  • Page 87: Ambient Conditions

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 10 Technical data Equipment connections Vacuum connection: Small flange connection DN25KF (ISO 28403, DIN 2861) Aeration valve: Hose nozzle, outside diameter 4.5mm max. (DN2.5) or with air filter Micro injection valve: Hose nozzle, outside diameter 4.5mm max.

  • Page 88: 11 Appendix

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Pos : 226 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/110 Anhang/110 Anhang================================================= @ 26\mod_1404985342887_68.docx @ 187751 @ 1 @ 1 → 11 Appendix Pos : 227 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/110 Anhang/110- 0010 M athem atis che Z us ammenhänge @ 26\mod_1404985343615_68.doc x @ 187765 @ 2 @ 1 →...

  • Page 89: Rotor Program

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Pos : 229 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/110 Anhang/110- 0020 Rotor programm - Ü berschrift @ 43\m od_1466141499940_68.docx @ 431655 @ 2 @ 1 11.2 Rotor program Pos : 230 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/110 Anhang/110- 0021 Rotor programm - T ex t BA ( nur Hinw eis) @ 45\m od_1476436222632_68.docx @ 443708 @ @ 1...

  • Page 90: Overview Of Evaporation Times (Rvc 2-33 Cdplus With Infrared Heating)

    Pos : 232 /200 Chris t/370 R VC-BA (ST ANDARDM ODU LE)/110 Anhang/110- 0032 Übersic ht Abdampfzeiten 2-33 IR @ 64\m od_1560241178838_68.docx @ 691212 @ 2 @ 1 → 11.3 Overview of evaporation times (RVC 2-33 CDplus with infrared heating) Water...
  • Page 91 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Methanol 100 ml test tube RC 6 100 ml test tube RC 6 100 ml test tube RC 6 100 ml test tube RC 6 n-Hexan 100 ml test tube...

  • Page 92: Brief Operating Instructions

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Pos : 234 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/110 Anhang/110-0040 Kurzbedi enungsanlei tung RVC 2- 33 IR @ 31\mod_1407484116865_68.doc x @ 209144 @ 2 @ 1 →...
  • Page 93 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix • Rotor decelerates until it is at a standstill. After the standstill of the rotor the lid can be opened in order to remove the rotors. Functional and operating elements...
  • Page 94 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Pos : 236 /200 Chris t/371 R VC-BA (PR OJEKT E)/RVC 2- 33 CDpl us IR/110 Anhang/110-0050 Konformitäts erklär ung en R VC 2-33 CD pl us IR @ 31\m od_1407484117577_68.docx @ 209158 @ 2 @ 1 →...

  • Page 95: Ec Declaration Of Conformity

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix 11.5 EC declaration of conformity Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 95 / 105 Translation of the original operating manual...
  • Page 96 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 96 / 105 Translation of the original operating manual...

  • Page 97: Declaration Of Conformity - China Rohs 2

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Declaration of conformity – China RoHS 2 11.6 Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 97 / 105 Translation of the original operating manual...
  • Page 98 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 11 Appendix Pos : 237 /010 Univ ers almodul e/ Seitenwechs el @ 0\mod_1202116244312_0.docx @ 105 @ @ 1 Version 08/2009, Rev. 3.6 of 22/11/2021 • sb-bs 98 / 105 Translation of the original operating manual...

  • Page 99: 12 Glossary

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating 12 Glossary Pos : 238 /010 Univ ers almodul e/901 Glos sar R VC=================================== @ 53\m od_1510554099821_68.docx @ 534697 @ 1 @ 1 → 12 Glossary Boiling retardation The temperature of a liquid can rise above the boiling point without the liquid actually starting to boil.
  • Page 100 Safety pressure Since the vacuum has a dominating influence on the product temperature, Martin Christ Gefriertrocknungsanlagen GmbH has integrated a so-called safety pressure function into their units in order to protect the products. If the pressure inside the rotor chamber rises too quickly – above the safety limit –...

  • Page 101: 13 Index

    Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Index 13 Index Cleaning of the rotational vacuum concentrator ........... 75 Accessories ......... 12, 32 Cleaning the rotor chamber ......76 Accessories, cleaning and care ....80 Cleaning the RVC and the accessories ..74 Accident prevention ........
  • Page 102 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Index Dimensions of the rotor chamber ....86 Dimensions of the unit ....... 86 General conditions ........11 Direct hazard to the life and health ..... 18 General malfunctions ......... 63 Disinfection of the rotor chamber and General work (maintenance) ......
  • Page 103 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Index Installation site ........... 35 Nominal rotor speed not reached ....64 Intended use ..........9 Nominal voltage ......... 14 IO communication error......65 Notes on safety and hazards ....... 9 IP code ............
  • Page 104 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Index Products, harmful (Hazards) ...... 27 Safety notes concerning the transport ..22 Products, solvent-containing ...... 11 Safety pressure ........54, 100 Program administration ......55 Safety pressure not reached ...... 64 Program memory information .....
  • Page 105 Rotational Vacuum Concentrator RVC 2-33 CDplus with infrared heating Index Up and down keys ........48 User interface ..........48 Technical data ........... 86 UV radiation ......... 35, 74 Technical documentation ......87 Teflon tubes ..........82 Temperature ........54, 86 Vacuum .............

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