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Summary of Contents for Thermo Scientific Savant SpeedVac SPD140DDA
- Page 1 SpeedVac™ SPD140DDA Vacuum Concentrator Installation and Operation 80302134 • Revision A • July 2018...
- Page 2 IMPORTANT: Read this instruction manual. Failure to follow the instructions in this manual can result in damage to the unit, injury to operating personnel, and poor equipment performance. CAUTION: All internal adjustments and maintenance must be performed by qualified service personnel. DISCLAIMER: Thermo Fisher Scientific Inc.
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Page 3: Table Of Contents
Contents Introduction ..............1 Safety Precautions ............2 Operating Standards............ 3 Product Specifications ..........3 Environmental Conditions......... 3 Installation..............4 Contents ..............4 Installation of SPD140DDA........4 Operation..............6 Description Of Control Panel ........6 Manual Run.............. 8 Auto Run..............9 Drying Rate .............. - Page 4 Appendix 2 ..............17 Additional SPD140DDA System Setup for DMSO Applications ..........17 Warranty ..............18...
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Page 5: Introduction
Introduction Thermo Scientific Savant SpeedVac™ SPD140DDA vacuum concentrator offers fast, reliable processing of samples. It effectively removes a broad range of aggressive and volatile solvents to concentrate or dry solutes, analytes and residues while providing complete sample recovery. The combination of vacuum, applied to the sample chamber... -
Page 6: Safety Precautions
Safety Precautions In this manual, the following symbols and conventions are Below are important safety precautions that apply to this used: product: This symbol when used alone indicates WARNING: Disconnect the unit from all power important operating instructions which reduce sources before cleaning, troubleshooting, or the risk of injury or poor performance of the unit. -
Page 7: Operating Standards
Operating Standards Product Specifications Operative Power* 115 VAC; 60 Hz; 6 amps 230 VAC; 50 Hz; 3 amps ® Vacuum Chamber TEFLON coated, chemical resistant aluminum casting, includes two built-in radiant lamps Cover Heated cover - includes a safety interlock Induction Motor Maintenance free ®... -
Page 8: Installation
Inspection. Inspect the unit and accessories for damage that may have occurred during shipment. Should there be any damage, report it to the carrier and contact Thermo Scientific immediately. Make sure the carrier inspects the damage and leaves an inspection report. Register any claims for shipping damage against the carrier or his agent. - Page 9 Table 2. Recommended DDA components Solvents To Be Vacuum System Evaporated Volatile, low boiling solvents (MeCl2), corrosive solvents (TFA) UVS850DDA Universal and mixtures, Vacuum System Small amounts of high boiling solvents (DMSO, DMF) RVT450 Refrigerated Vapor Large volumes of high Trap + VLP80DDA High boiling solvents (DMSO, Vacuum Pump...
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Page 10: Operation
Operation Connect the power cord to the power inlet on the back of the Rotor installation. Open the lid of the rotor chamber. unit and plug it into the appropriate outlet. Turn on the main Visually align the pin on the drive shaft with the groove on the power switch located on the front of the unit in the lower right bottom of the rotor. - Page 11 Loading a user-defined program is achieved by pressing a continuous heating throughout the execution of a run. the corresponding “Program” button once or twice. The The setting of “CCC” can be reached under 0.01 [1 min.] first button press will load the first program associated or over 9.59 [9 hours, 59 minutes].
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Page 12: Manual Run
Ramp: The rate at which vacuum is achieved can be set Manual Run for preventing bumping. There are 5 adjustable levels that can be set as required depending upon your solvent. 1. Connect the unit to its required voltage. 2. Turn the power switch located on the front of the UNIT, to Setting Vacuum Rate (Approximate) the ON position, (light on switch indicates ON). -
Page 13: Auto Run
11. Press RL On/Off for radiant chamber heat. Press at any Note: If the cover is not closed, the display will show time to turn OFF and ON. (As long as there is time left in “Lid” and the run will not start. the heat timer and if the temperature set point is not set c. -
Page 14: Exporting Live Run Data
Table 4. Preset Program Settings CAUTION: USB lead length less than 3 meters shall be used to connect to the computer. Temperature: 45°C Heat time: 2.00 When a run is ongoing, the unit exports the following “Low Boiling” information via the USB port every minute. Preset 2 Run time: 2.00 ACN/MEOH... -
Page 15: Lid Stay Mechanism
5. In the “COM Port Properties” box \ “Port Settings” folder Other Topics select the following options: Bits per second: _ 115200 Chamber Cover. The cover must be closed before Data bits: _ 8 beginning a run. If you press Manual Run or Auto Run and the cover is open, the display shows “lid”... - Page 16 Petroleum ether n-propyl alcohol Propanol-1 Pyridine Trifluoroacetic acid 0.1% Trifluoroacetic acid Toluene In the event that your choice of solvents and applications are unique and not listed above, please contact Thermo Scientific Customer Support for advice. 12 | Operation SpeedVac™ SPD140DDA...
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Page 17: Rotors
Rotors Traditional Rotors for SPD140DDA Vacuum Concentrator Sample Format Working Traditional Rotor Number Description Type Volumes (ml) Model 1.2 - 1.6 1.5 -2.0 ml RH40-11 1.2 - 1.6 1.5 -2.0 ml RH64-11 MICROCENTRIFUGE TUBES 1.2 - 1.6 1.5 -2.0 ml RH120-11 17 X 60 mm (5 ml) RH10-15... -
Page 18: Sumax Spd Maintenance
Tighten the rotor hold down knob firmly with one quarter turn after flush with knob support Magnet If you encounter difficulties with this procedure, please contact Thermo Scientific technical service. Figure 5. SUMAX SPD Upper Magnetic Assembly Drawing Every two weeks or dependent upon usage, please execute the following steps: •... -
Page 19: Additional Spd140Dda System Setup
Appendix 1 Additional SPD140DDA System Setup SpeedVac™ Concentrator SPD140DDA Vacuum Tubing From SPD140DDA to UVS850DDA Vacuum Tubing From RVT450 to UVS850DDA SPD140DDA Vacuum Tubing Carrying Vapors From back of SPD140DDA to RVT450 ANT100 Exhaust recovery Post trap RVT450 UVS850DDA Vacuum Tubing UVS850DDA to back of SPD140DDA Figure 6. - Page 20 SpeedVac™ Concentrator SPD140DDA Vacuum Tubing From SPD140DDA to VLP80 Vacuum Tubing Vacuum Tubing Carrying Vapors From From RVT5105 to back of SPD140DDA to back of SPD140DDA RVT450 DVG50-Vacuum SPD140DDA Gauge VLP80 VPOF110 RVT450 RVT5105 Vacuum Tubing From RVT450 to the RVT5105 Cold Trap Figure 7.
- Page 21 Appendix 2 Additional SPD140DDA System Setup for DMSO Applications SpeedVac™ Concentrator SPD140DDA Vacuum Tubing From RVT5105 to back of SPD140DDA Vacuum Tubing From SPD140DDA to OFP400 Vacuum Tubing Carrying Vapors From back of SPD140DDA to SPD140DDA RVT450 RVT450 RVT5105 OFP400 Vacuum Tubing From RVT450 to the RVT5105 Cold Trap Figure 8.
- Page 22 Warranty All Thermo Fisher Scientific products mentioned in this manual (excluding glassware) are warranted against defects in workmanship for one year after the date of delivery to the original purchaser. This warranty is limited to defective materials and workmanship and does not cover incidental or consequential damages.
- Page 23 Ulteriori informazioni sulla conformità di Thermo Fisher Scientific con queste Direttive, l’elenco delle ditte di riciclaggio nel Vostro paese e informazioni sui prodotti Thermo Scientific che possono essere utili alla rilevazione di sostanze soggette alla Direttiva RoHS sono disponibili sul sito www.thermofisher.com/WEEERoHS in Servizi e Supporto.
- Page 24 IF YOU NEED ASSISTANCE: Thermo Fisher Scientific products are backed by a global technical support team ready to support your applications. Visit www.thermofisher.com/ or call: Countries Sales Services North America +1 866 984 3766 (800) 438-4851 India 1800 22 8374, +91 22 6716 2200 +91 22 6716 2200 China +800 810 5118, +400 650 5118...
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