Large Peak At M/Z 19 - HP 5973 MSD Hardware Manual

Large peak at m/z 19

If the abundance of the peak at m/z 19 is more than twice the abundance of the
peak at m/z 17, then there is probably too much water in the system.
Possible Cause
The system was not baked out sufficiently after it was last vented.
Action Bake out the system as described in the Maintenance chapter of this manual.
Possible Cause
Moisture left over in the reagent gas supply tubing and flow module.
Action
Purge the reagent gas supply lines for at least 60 minutes. See the Maintenance
chapter.
Possible Cause
Contaminated reagent gas supply.
Action Replace the reagent gas supply and purge the lines and flow module.
Possible Cause
Saturated methane / isobutane gas purifier.
Action
Replace the gas purifier.
 Troubleshooting
/DUJH SHDN DW P] 
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