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ANALYZER SERIES B A L A N C E S A N D S C A L E S RADWAG 26 – 600 Radom, Bracka 28, POLAND Phone: +48 (0-48) 38 48 800, fax. +48 (0-48) 385 00 10 export@radwag.com...
TABLE OF CONTENTS 1. TECHNICAL DATA ................6 2. BASIC INFORMATION................. 7 2.1. Intended use ................7 2.2. Inappropriate use ..............8 2.3. Principles of safety use ............8 2.4. Warranty ................... 9 2.5. Monitoring metrological parameters of the instrument ..... 9 2.6.
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8.3.2. Setting time format ............30 8.3.3. Setting time ..............30 8.3.4. Setting date ..............31 8.3.5. Setting displaying criteria for date and time ....31 8.4. Setting moisture analyzer operating parameters ....31 8.4.1. Entering menu group P4 Readout ....... 31 8.4.2.
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11. TESTING PROCEDURE USING A DRYING PROGRAM FROM THE LIBRARY OF DRYING PROGRAMS ..........65 12. SAMPLE PREPARATION FOR A DRYING PROCESS ....67 12.1. Principles of humidity content determination in a moisture analyzer ....................67 12.2. Sampling and preparation ............67 13.
TECHNICAL DATA MAX 50/1 MAX 50 MAX 60 Type Reading interval 0,1 mg 1 mg Max. capacity 50 g 60 g Reading interval of 0,0001% 0,001% moisture content Tare range - 50 g - 60 g Max. sample mass 50 g...
BASIC INFORMATION CAUTION! Use of moisture analyzer MAX series conversely to safety provisions and other than following guidelines of this user manual may be hazardous to human health and life. Never use the moisture analyzer is explosive area. Moisture analyzer is not intended to use in areas with danger of explosion.
2.2. Inappropriate use CAUTION! Do not open the drying chamber during drying process. Moisture analyzer features a halogen lamp which is a very powerful heat source. Thus, user should pay special attention no to touch those elements of a moisture analyzer that get hot while drying procedure (i.e.: disposable pan, pan handle, and inner shields of the drying chamber).
2.4. Warranty Warranty does not cover the following cases: • Not observing the regulation listed in user manual, • Using the moisture analyzer conversely to its intended use, • Any modifications of moisture analyzer or cases when its housing is opened (damaged protective stickers), •...
TRANSPORT AND STORAGE 3.1. Delivery check Please check the packaging immediately upon delivery and the device during unpacking for any visible signs of external damage. 3.2. Packaging Please retain all parts of the original packaging should the moisture analyzer be transported in the future. Only the original packaging should be used for dispatching the moisture analyzer.
4.2. Unpacking Carefully remove the moisture analyzer from its packaging, remove the plastic and foil transport protective elements. Gently place the moisture analyzer in its intended place of use. Assembly the components of drying chamber, following guidelines from below figure: Assembling moisture analyzer components: Assembly insert of the drying chamber’s basis...
4.3. Level setting Before plugging to mains, level the moisture analyzer using adjustable feet. Turn the feet in a way that the air bubble of the level is located centrally. 4.4. Standard delivery components • A moisture analyzer MAX series •...
4.7. Connecting peripheral equipment The moisture analyzer must be unplugged from the mains before connecting or disconnecting any peripheral equipment (printer, PC computer). Use only peripheral equipment recommended by the manufacturer with your moisture analyzer. These have been ideally coordinated to your moisture analyzer. On connecting a peripheral device, plug the moisture analyzer to mains.
Zero / Tare key – zeroing moisture analyzer’s indication. On/Off key – switch on/off display of moisture analyzer. On switching off the display of the device, other subassemblies are continuously supplied, and the moisture analyzer is in standby mode. Display key – changes type of data displayed during and after drying process.
P2 06 Print project name P6 13 Text 1 P2 07 Print ID P6 14 Text 2 P2 08 Print adjustment data P7 Other P3 Date/Time P7 01 Password P3 01 Date format P7 02 Database of drying P3 02 Time format programs P3 03 Time P7 03 Beep sound...
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Exit menu without saving changes: Press Esc key. Entering moisture analyzer’s main menu: Press Setup key to get access to user menu and its parameters. Exit menu without saving changes: Press Esc key for two times. Selecting a desired option in the menu: Press one of navigating keys (marked with black coloured arrows) on...
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of measurement result while the drying process is in progress or on its completion. The measuring units are previewed by pressing DISPLAY key. Each pressing of the key changes in turns the measuring unit and automatic recalculation of measurement result. Available measuring units: %M (percent loss of mass in tested sample);...
7.2. Menu operation using external computer keyboard All keys present on moisture analyzer’s overlay have their equivalents on a computer keyboard PS type, described in below table: - function keys Description Overlay Start / End drying process in an active drying mode. Entering main menu.
USER MENU User menu is accessible on pressing SETUP key on moisture analyzer’s overlay. The user enables: moisture analyzer adjustment, setting transmission parameters, setting time and date and their format, and also other user parameters. This section of the user manual presents software possibilities of the moisture analyzer and means of changing the parameter settings.
The moisture analyzer gives a command on determining mass of an empty pan, followed by a command to place a 50 g weight (standard) on the pan. After completing adjustment process the moisture analyzer returns to submenu P1 - Adjustment Press ESC for a few times until the display indicates below message Depending on needs press ENTER or ESC key.
The moisture analyzer gives a command on determining mass of an empty pan, followed by a command to place a weight with pre-determined mass. On placing the weight on the pan accept the process by pressing Enter key. After completing the user adjustment process the moisture analyzer returns to submenu P1 - Adjustment.
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temperature adjustment process, install the adjustment set inside the drying chamber following below figures. Step 1. Remove from the drying chamber the following: • Disposable pan • Pan holder • Pan bracket • Chamber cover Step 2. Place in the drying chamber the components of the temperature adjustment set: •...
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Step 3. After assembling the adjustment set close drying chamber’s lid and start the temperature adjustment process. CAUTION: remember to carry out all the processes with great care not to damage the mass measuring mechanism of a moisture analyzer. Enter menu group P1 Adjustment. Set the marker next to a parameter 04 Temperature adjustment.
following step of drying chamber adjustment process. The moisture analyzer continutes heating the drying chamber for another 8 minutes and simultaneously indicates on its display the current temperature value. After the 8 minute time interval the moisture analyzer’s display indicates the flashing temperature value.
An example of a printout of a report from adjustment process: printout content depends parameters set in group P2 GLP (see point 8.2 of this user manual). Variables that are printed have an attribute set to 1: yes. Apart from the content set in this menu group, a report contains the following data: mass of an adjustment weight stored in moisture...
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The moisture analyzer displays another message for entering the permissible temperature error that is acceptable by an operator. Use the navigating keys to enter the desired error size and press ENTER button to accept. The moisture analyzer displays another message for entering the factory number of the adjustment set used for carrying out the test.
---------------------------------------- Test the drying chamber ---------------------------------------- The test result can be printed on 17/04/2013 15:03:42 a printer connected to a moisture Balance Id: 01 analyzer by pressing PRINT Number of calibration kit: button. An example of a report Temperature setpoint: from drying chamber test is The final temperature: presented in the table on the left.
closed circuit. Select a neede character. Next move the cursor to the right and enter the following character. On entering all of the characters press ENTER key. Using external computer keyboard PS/2 type Press F2 key to enter the main menu, press F3 key or use navigating arrows to set the marker next to a parameter 01 User and press F2 key to enter parameter settings (flashing first character of an existing number or flashing cursor if not number is specified).
Data to be printed must have an attribute set to “1 yes”. EXAMPLES OF PRINTOUTS FOR DIFFERENT GLP SETTINGS: P2 03 print time: 1:yes Date : 16/01/2002 P2 04 print date: 1: yes Time : 13:12:30 P2 05 print user: 1: yes User : R.
8.3.2. Setting time format Press navigating arrow key to enter submenu 02 Time format. Select one of available values: Time format – 12 hours Time format – 24 hours On selecting the appropriate value accept it by pressing ENTER key. 12 hour time format is differentiated by letters PM or AM visible on a printout.
8.3.4. Setting date Press navigating arrow key to enter settings of parameter 04 Date Following procedure described in point 8.3.3 set current date value. After setting the date return to the weighing mode following procedure specified in point 7.1 of this user manual. 8.3.5.
movement) it is recommended to set the filter value to slow or very slow (set value of parameter 01 Filter to 4 or 5). The efficiency of filter operation differs in relation to the measuring range. The filter operates with lower accuracy while the mass indication is quickly increasing after placing a load on the pan, Filter accuracy is increased when weighed mass is within filter’s set operation range (parameter: filter operation range is available only in balance’s service menu, and it is...
In case of parameter set to P5 07 – 3 : PC – the data sent to a printer is only a line. The data from the header and the footer is not printed. For parameter set to P5 07 – 4 : PC-RADWAG – each printout is proceeded by a special controlling signs, which enable moisture analyzer cooperation with the computer software E2R MOISTURE ANALYZER.
8.6. Printouts User of a moisture analyzer MAX series can set up to 5 different printout templates which are sent from the instrument to a connected peripheral device (a printer or a computer) through the RS 232 slot. A single STANDARD printout containing data enabled in the GLP procedures Four NON-STANDARD...
8.6.2. Non-standard printout templates Principles of creating non-standard printout templates: Moisture analyzer MAX series enables creating up to 4 custom printout templates; each template must have the string of text start and end specified, e.g. Printout no. 1 Start – 1 and Printout no. 1 Stop – 40. In this case the Printout no.
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Variables available in drying mode only Drying chamber temperature Drying time Drying result – humidity content Start mass of a sample Drying result – dry mass End mass of a sample Drying result – humid/dry ratio Parameters of an enabled drying mode Drying result –...
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Example no. 2: “RADWAG” Balances & Scales Date: Hour: Load mass *****Signature:..***<active working mode >*** Enter text strings settings and input 8 characters from the above text into each of the text strings until completing the printout. Text Text string no.
Place the cursor next to a selected text string (from string 1 to string 80). od tekst 1 do tekst 80). Press navigting arrow key to enter parameter settings (if the selected field was empty, then the first available space for a character starts flashing. If a text is inserted to a string, then the first character of a line starts flashing).
3 : printout 3 4 : printout 4 On selecting an appropriate value accept it by pressing ENTER key. 8.6.5. Enabling non-standard printout templates Enabling a non standard printout template, e.g. printout no. 1: Enter group of parameters P6 Printouts. In a parameter determining printout type 01 Printout no.
8.7. Moisture analyzer parameter settings. Depending on user needs the moisture analyzer enables setting parameters influencing its operation. These parameters are grouped in menu P7 Other, for instance: beep sound on pressing a key/button, screen contrast, etc. 8.7.1. Entering menu group P7 Other Enter submenu group P7 Other.
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06 Screen brightness Enables changing the brightness of the balance’s graphic display – entering the function opens a window for setting brightness level using buttons on the balance’s overlay 07 Screen contrast Enables changing the contrast of the balance’s graphic display – entering the function opens a window for setting contrast level using buttons on the balance’s overlay 08 Balance no.
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quickly change parameter values. After saving made changes, the updated file is sent from the computer level to balance’s software. On completing of uploading process and saving changes the balance accepts new parameter settings. The procedure requires that a user is familiar with balance parameters and has good knowledge of computers.
DRYING PROCESS WITH USE OF SHORTENED MENU This section of the user manual presents the means of carrying a moisture content determining process using the shortened procedures. Menu of drying mode enables setting the following parameters: Drying mode with its profile (temperature, time) Means of drying process finish mode Type of displayed measurement result Frequency of printing data from a drying process...
On returning to the main window (with procedure of saving changes) the use can carry out a drying process after setting the basic parameters for drying a sample to be tested. There is no need to select a specific drying program from the database.
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Press UP or DOWN navigating arrow keys to select one of available drying modes: Standard, Quick, Mild or Step. If selected drying mode is QUICK, then set the drying temperature and heating time in temperature exceeded by 30 % than the actual drying temperature. The heating time is calculated from the moment of reaching the set temperature by the moisture analyzer.
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Press right arrow navigating key to change parameter value (the displayed value starts flashing) Press UP or DOWN navigating arrow keys to select needed parameter value. After setting the parameter value accept it by pressing ENTER key (the value stops flashing). If a Mild or Step drying mode is selected then go to other mode settings.
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After setting the Finish mode criteria go to setting the following parameters of a drying process. In order to set other parameters of the drying process press ENTER key. The software returns to displaying the initial window. Press DOWN navigating arrow key to go to the following step of drying process determination, i.e.
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After setting the Result criterion go to setting the following parameters of a drying process. In order to set other parameters of the drying process press ENTER key. The software returns to displaying the initial window. Press DOWN navigating arrow key to go to the following step of drying process determination, i.e.
Once more press ENTER key. The software does to displaying the main window in a level which enables determining humidity content of a sample to be tested. 9.3. Means of drying process according to parameters set in the shortened menu The left side of the display presents selected pictograms with set criteria of the drying process.
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Place the disposable drying pan in its intended holder and place the assembly on the cross-shaped support. support. The display indicates mass of a fitted drying pan. In order to ensure stable measurement conditions it is recommended to close the moisture analyzer’s lid before tarring mass of the drying pan.
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Place a sample to be tested on the drying pan. Mass of a sample should be selected according to previously conducted experiments and features of the tested substance. After stabilization of the indication (followed by appearing of a stability pictogram on the display) close the moisture analyzer’s lid.
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The indications on the display change and indicate data on conducted process. The moisture analyzer automatically carries out the drying process with drying parameters as set in the drying criteria. The instrument automatically conducts all needed mass measurement and calculating processes resulting from changes mass of the tested sample.
10. DRYING PROCESS WITH USE OF DRYING PROGRAM LIBRARY This section of the user manual specifies in details the procedures for determining a new drying procedure saved in the memory of the moisture analyzer MAX series.. Each drying procedure contains: name Profile (drying mode) Drying temperature...
with data. Press RIGHT arrow navigating key to open an entry with data on drying program. The opened window contains data saved in the selected drying program. Following the means of moving in the user menu and carrying out changes set required parameters for a drying program.
After entering the new name accept it by pressing ENTER key. The last entered character stops flashing. After accepting the newly entered name go to setting another parameters of the drying program. 10.3. Drying mode selection The moisture analyzer MAX series enables selecting one of four available drying modes: Standard, Quick, Mild, Step.
the set temperature by the moisture analyzer Set drying temperature for drying mode Mild and time in which the moisture analyzer should reach the set temperature value. In Step profile set the drying temperatures for thresholds 1 and 2 and the drying temperature and their corresponding time intervals for each of the thresholds.
After setting and saving the new temperature value, it is also set to a drying mode. 10.5. Finish mode settings Finishing of a drying mode can be carried out as: - Automatic 1 (change ratio 1mg/10s) - Automatic 2 (change ratio 1mg/25s) - Automatic 3 (change ratio 1mg/60s) - Automatic 4 (change ratio 1mg/90s) - Automatic 5 (change ratio 1mg/120s)
10.7. Setting printout interval This parameter determines the interval of sending a measurement result on humidity content of a tested sample. Procedure: Go to software menu. Use DOWN navigating arrow key to place the cursor (black triangle) next to a parameter Printout interval.
In case option Optional is enabled the user has to enter required sample mass and tolerance value for the material to be weighed / dried. If sample mass option is enabled, the moisture analyzer displays prompts for the user on placing a required size of a sample to be tested on the drying pan. If a user neds to dry a sample with different mass, then drying process can be started even if the mass does not comply with set parameter criterion.
Procedure: Go to software menu. Use DOWN navigating arrow key to place the cursor (black triangle) next to a parameter Corrective Coefficient. Use function keys on moisture analyzer keyboard, or an external computer keyboard, to set needed coefficient value. Set the coefficient value in accordance with above specified means of moving in the user menu.
On restoring the default parameters the software moves back to the previous window. Pressing Esc key abandons restoring of the default parameter. The software returns to previous window without saving changes. 10.11. Printout of software settings The parameter enables printing all current drying mode settings on a connected printer.
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Press RIGHT arrow navigating key causes displaying a message to confirm printout of parameters. Press ENTER key to accept the process. The moisture analyzer sends data on drying mode parameter values to a connected printer, and returns to the previous window. ------- Software parameters ------ Software no.: 1 Name: Wheat flour 100...
10.12. Saving drying mode settings moisture analyzer’s permanent memory When determining parameters of a drying mode, all the settings are saved in the moisture analyzer’s volatile memory. Permanent saving of the settings requires returning to the main window with procedure of saving changes. Procedure: Press Esc key.
11. TESTING PROCEDURE USING A DRYING PROGRAM FROM THE LIBRARY OF DRYING PROGRAMS A moisture analyzer MAX series enables carrying out a drying process using programs saved in the library of drying programs. This means of using the device considerably speeds up the preparation for a testing process, as all the parameters on drying process of a material are already determined in the program, i.e.
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Press ENTER key to return to the main window. The moisture analyzer is ready to start testing procedure with programmed drying parameters. The upper bar of the display indicates name of the selected drying program and its number from the library of drying programs. On the left side of the display there are pictograms indicating pre-set values of drying parameters (i.e.
RADWAG moisture analyzer comprises two components: a precision balance and a drying chamber. Compared to standard moisture content determining methods, the measurements with application of RADWAG moisture analyzer is much quicker and does not require additional mathematical calculations (a result of moisture content is previewed on an ongoing basis during product testing process).
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Final measurement result is vastly conditioned by precise and considered sample preparation. A sample used for analysis has to represent the total structure of tested material. Sampling process should determine: sampling means, sample disintegrating, particle size after disintegration, sample uniformity and other. The sampling process should be carried out as quickly as possible, so that a sample does not loose or absorb humidity from surrounding area.
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Liquid substances It refers to liquid substances, which by creation of drops on their surface, caused by surface tension, may render difficulties in drying process. In such cases, it is proved to use a glass fiber filter to shorten measurement time. The filter causes separating tested liquid around the fibers, and increasing active evaporating surface.
13. SELECTION OF DRYING PARAMETERS 13.1. Selecting optimum sample mass Sample mass influences the accuracy of measurement result and measurement time. Higher mass of a sample, causes higher amount of water (moisture content) which needs to evaporate, and therefore measurement time is also longer. Obtaining short measurement time is feasible in case of small sample mass, but sample mass cannot be too small, as it may negatively influence required measurement accuracy.
time. Too high drying temperature causes burning of dried sample (sample overheating, chemical decomposition). Drying temperature of traditional method (using a furnace) is specified in applicable industry or company standards. Unless standards apply, then temperature should be adjusted by tests. On selecting the value of drying temperature, use the following procedure: •...
temperature). Overheating compensates heat loss during evaporation of large moisture content in the test’s initial stage. STEP mode Enables determining up to three steps with random drying temperature. Step mode is recommended for drying substances with moisture content over 15%. Temperature and heating time in each step have to be adjusted by tests.
13.6. Drying mode analysis In the first case the drying mode is an asymptote. The humidity content in a sample reaches a constant and it does not change after long drying time. Using this drying mode enables easy obtaining of repeatable humidity content in a tested sample.
14. COOPERATION WITH A PRINTER OR A COMPUTER Each pressing of < PRINT > key causes sending to a connected printer or computer a signal corresponding to current mass indication (display status) with enabled measuring unit. The default baud rate setting of a balance is 9600 bit/sec.
15. LIST OF COMMANDS COMPUTER - BALANCE Function INTERFACE RESET Command R CR LF (zeroing currently carried out commands, restoring factory default settings) Function SEND ALL IMPLEMENTED COMMANDS Command PC CR LF (sends information on all commands implemented in the balance’s software) Function SEND MEASUREMENT RESULT IN BASIC MEASURING UNIT Command...
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Function GIVE SOFTWARE REVISION Command RV CR LF (sends software name) Function GIVE OR CHANGE DATE IN A BALANCE Command PD CR LF (causes sending data on set date or changes the date) Function GIVE OR CHANGE TIME IN A BALANCE Command PD CR LF (causes sending data on set time or changes the time) Function...
16. USER GUIDELINES The measurement of relative humidity content of materials to be tested using a moisture analyzer MAX series is much shorter and simpler if compared to a traditional method (weighing – drying – weighing – calculating). It is necessary to remember that it is a different measurement method, this requires an individual selection of drying parameters to each dried substance, such as: •...
17. MOISTURE ANALYZER MAINTENANCE ACTIVITIES This section of the user manual describes procedures of maintaining a moisture analyzer MAX series in good condition, and means of replacing faulty components (filaments, fuses). 17.1. Cleaning moisture analyzer components In order to ensure required measuring accuracy, the moisture analyzer has to be used and stored in clean conditions.
After cleaning, thoroughly dry each of moisture analyzer’s components. Do not allow any contamination or liquid to fall into the moisture analyzer. Assembly cleaned and dried components in accordance with above scheme. 17.2. Temperature sensor cleaning In order to ensure correct temperature measurements during testing procedure, pay special attention to cleanness of the temperature sensor (1).
17.3. Replacing the fuses If after plugging to mains, a signal diode on moisture analyzer’s display does not light up (lack of any reaction on the display), then possibly one of the fuses (or both) is blown. REMEMBER, before initiating any activities relates to fuse replacement switch off the moisture analyzer, and make sure the power cord of the moisture analyzer is unplugged from mains!
17.4. Troubleshooting Problem: no reaction to pressing main switch on/off key (display remains dark). Probable cause: − No voltage in mains − Damaged power cord − Damaged fuse of the moisture analyzer − Moisture analyzer defect Problem: too long pending time for drying process finish. Probable cause:: −...
17.5. Error messages Detecting of an error is signaled by the moisture analyzer by displaying a message corresponding to the error. The message contains number of the error and a short description informing on the possible causes of error occurrence. List of error messages in a moisture analyzer: Error message Error...
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Timeout error for carrying out a given "Time value exceeded " process (e.g. zeroing). CAUTION: If the carried out activities related to dealing troubleshooting or maintenance are other than expected, please immediately contact you locla RADWAG dealer or service point. - 83 -...
18. MEMORY OF CARRIED OUT MEASUREMENTS A moisture analyzer MAX series enables storing Maximum 100 last carried out measurements that comprise the following set of data: date, time, measurement time, name, drying mode, drying temperature, drying time, start mass, end mass, final result. The measurements are saved in a pile. After saving over a 100 a measurement in a pile, the record with no.
19. MEANS USING MOISTURE ANALYZER DRYING TEMPERATURE OVER 160°C In case of drying a sample in a temperature ranging between 161°C – 250°C the maximum time of maintaining the temperature is determined proportionally from the range: 1 hour for 161 °C – 20 minutes for 250°C. When drying a sample in temperature 250°C, the maximum temperature value is maintained by the instrument for 20 minutes, and then the software decreases the temperature value to 160 °C without stopping the drying process.
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