Page 1 User Manual Protos PHU 3400(X)-110 Communication Module Deutsch Deutsch English zur Leitfähigkeitsmessung mit induktiven Sensoren zur Leitfähigkeitsmessung mit induktiven Sensoren For Actuating Probe Controllers (Unical / Uniclean) -Automatic pH Measurement- Aktuelle Produktinformation: www.knick.de Aktuelle Produktinformation: www.knick.de Latest Product Information: www.knick.de...
Page 2: Return Of Products Under Warranty
Trademarks The following trademarks are used in this manual without further marking: CalCheck®, Calimatic®, Protos®, Sensocheck®, Sensoface®, Unical®, VariPower®, Ceramat®, SensoGate® are registered trademarks of Knick Elektronische Messgeräte GmbH & Co. KG, Germany Memosens® is a registered trademark of Endress+Hauser Conducta GmbH & Co. KG, Germany Knick Elektronische Messgeräte GmbH &...
Page 3: Table Of Contents
Table of Contents Protos PHU 3400(X)-110 Module Return of products under warranty ..................2 Disposal ............................2 Trademarks ........................... 2 Intended Use ....................9 Conformity with FDA 21 CFR Part 11 .................. 9 Safety Information ..................10 Application in Hazardous Locations: PHU 3400X-110 Module .......10 Software Version ........................11 Modular Concept ........................13 Short Description ..................
Page 4 Table of Contents Protos PHU 3400(X)-110 Module Parameter Setting for PHU 3400(X)-110 ............. 33 Activating Parameter Setting ....................33 Settings of Sensor Data......................34 Sensoface ............................36 SW 3400-005: Tolerance Adjustment ................39 Activating the Cal Tolerance Band ................40 Documenting Parameter Setting ..................47 ProgaLog 3000 Software (Option) for Configuration and Documentation ..49 Configuration using "ProgaLog 3000"...
Page 5 Table of Contents Protos PHU 3400(X)-110 Module Parameter Setting: Program Flows ..................70 Cleaning (Continuous), Media Monitoring Off .............70 Cal 2point (Continuous), Media Monitoring Off ..........71 Cal 1point (Continuous), Media Monitoring Off ..........72 Parking ..........................74 Measurement (Short-Time), Media Monitoring Off ..........75 Cal 2point (Short-Time), Media Monitoring Off ...........76 Cal 1point (Short-Time), Media Monitoring Off ...........77 Service ..........................78...
Page 6 Table of Contents Protos PHU 3400(X)-110 Module Uniclean 900(X) Parameter Setting ............. 98 Measuring Module ......................99 Time Control ........................99 Parameter Setting: Program Flows ................. 101 Rinsing (Continuous) ....................101 Cleaning (Continuous) ....................102 Parking ..........................104 Measuring (Short-Time) ..................... 105 Service ..........................
Page 7 ISFET Zero Adjustment ....................134 Maintenance of PHU 3400(X)-110 .............. 136 Sensor Monitor ........................136 Temp Probe Adjustment..................... 136 Probe Maintenance via Protos 3400(X) ............. 137 Diagnostics Functions ................. 141 Point of Meas Description ..................141 Logbook ........................... 141 Device Description ....................... 142 Diagnostics of PHU 3400(X)-110 ..................
Page 8 Appendix: ..................... 176 Minimum Spans for Current Outputs ................176 Buffer Table "Mettler-Toledo" .................... 177 Buffer Table "Knick CaliMat" ....................178 Buffer Table "DIN 19267" ....................179 Buffer Table "NIST Standard" (DIN 19266: 2000-01)..........180 Buffer Table "Techn. Buffers to NIST" ................181 Buffer Table "Hamilton"...
Page 9: Intended Use
This results in requirements for measuring devices used for corresponding applica- tions. The following features ensure that the Protos 3400(X) modular process analysis system meets the demands of FDA 21 CFR Part 11:...
Page 10: Safety Information
• When installing the device in a hazardous location, observe the specifica- tions of the EC-Type-Examination Certificate and, if applicable, of the Control Drawing (download: www.knick.de). • Before commissioning you must prove that the device may be connected with other equipment, such as a supply unit including cables and wires.
Page 11: Software Version
Software Version PHU 3400(X)-110 Module Device Software Protos 3400(X) The PHU 3400(X)-110 module is supported by software version 5.0 or higher. Module Software PHU 3400(X)-110 Software version 3.x Query actual device/module software When the analyzer is in measuring mode: Press menu key, open Diagnostics menu: Device description...
Page 13: Modular Concept
Modular Concept Basic unit, measuring modules, additional functions The Protos 3400(X) is an expandable modular process analysis system. The basic unit (FRONT and BASE modules) provides three slots which can be equipped by the user with any combination of measuring or communication modules.
Page 14: Short Description
Short Description Short Description: FRONT Module 4 captive screws Transflective LC graphic display for opening the analyzer (240 x 160 pixels) (Caution! Make sure that the gasket between FRONT and white backlighting, high resolution and BASE is properly seated and clean!) high contrast.
Page 15: Short Description: Menu Structure
Short Description: Menu Structure Basic functions: Calibration, Maintenance, Parameter setting, Diagnostics Menu groups Maintenance Parameter setting Diagnostics Calibration Measure Passcode: 2958 1246 1147 Operator level 1989 Administrator level Selection of BASE SYSTEM Message list Module 1 Point of meas Module 1 further FRONT Module 2...
Page 16 Short Description: FRONT Module View into the open device (FRONT module) Slot for SmartMedia card • Data recording The SmartMedia card expands the measurement recorder capacity to > 50000 records. • Exchange of parameter sets 5 parameter sets can be stored on the SmartMedia card, 2 of them can be loaded simultaneously to the analyzer and be switched by remote control.
Page 17: Short Description: Base Module
Short Description: BASE Module View into the open device (BASE module, 3 function modules installed) Module equipment Module identification: Plug & Play. Up to 3 modules can be combined as desired. Several input and communication modules are available. Note Only one module can be connected in addition to a FIU 3400(X)-140/141 module.
Page 18: Overview Of The System Components
• Unical 9000(X) / Uniclean 900(X) (automatic control of retractable fittings) • Ceramat WA 150(X) (retractable fitting with ceramic sealing to the process) The system is operated from the Protos 3400(X). Four operating modes are provided: calibration, parameter setting, maintenance, diagnostics.
Page 19 Overview of the System Components Protos 3400(X) Basic Unit and Controller Module for Retractable Fittings PHU 3400(X)-110 and Unical 9000(X) / Uniclean 900(X) Probe Controller Protos 3400(X) basic unit. The PHU 3400(X)-110 module is located in one of the 3 module slots available.
Page 20: Phu 3400(X)-110 Module
This instruction manual describes the whole functionality of the PHU 3400(X)-110 module corresponding to the following menu groups: • Calibration • Maintenance • Parameter setting • Diagnostics The Protos 3400(X) is an expandable modular process analysis system. For latest product information, please refer to: www.knick.de...
Page 21: Terminal Plate Phu 3400(X)-110 Module
Terminal Plate PHU 3400(X)-110 Module Terminal Plate PHU 3400-110 Module: Attaching the Terminal Plates The terminal plates of the lower modules can be sticked to the inner side of the door. This facilitates maintenance and service.
Page 22: Inserting The Module
Inserting the Module Note: Be sure to connect the shielding properly! Make sure that the cable The terminals 2 and 8 are glands are tightly closed to covered by an ESD shield. protect against humidity. To connect the sensor cable, just pull it back.
Page 23: Wiring Example Vp And Sixplug
Wiring Example 1 Wiring Example VP and SixPlug Multisense electrode (pH/ORP/temp) with solution ground (SG) PHU 3400-110 UNICAL 9000(X)
Page 24 Wiring Example 2 Wiring Example VP and SixPlug Electrode (pH/temp) without solution ground (SG) PHU 3400-110 Jumper UNICAL 9000(X)
Page 25: Connecting The Probe Controller
RS 485 A RS 485 A Yellow RS 485 B RS 485 B Brown White 6.8 V (supply) Power Unical 9000(X) / Uniclean 900(X) Controller The Unical 9000(X) / Uniclean 900(X) probe controllers come with installation manuals, free download at www.knick.de.
Page 26: Menu Selection
Menu Selection After switching on, the analyzer performs an internal test routine and automatically detects the number and type of modules installed. Then, the analyzer goes to measuring mode. 8.06 pH 25.1 °C Menu selection °C 24.0°C 25.8°C Select: [enter] Return to meas Lingua 1 Pressing menu accesses menu selection.
Page 27: Passcode Entry
Passcode Entry To enter a passcode Select the position using the left/right keys, then edit the number using the up/down keys. When all numbers have been entered, press enter to confirm. To change a passcode • Open the menu selection (menu) •...
Page 28: Configuring The Measurement Display
Configuring the Measurement Display Select menu: Parameter setting/Module FRONT/Measurement display Pressing meas (1) returns the analyzer to the measuring mode from any function. All process variables coming from the modules can be displayed. The table on the next page describes how to configure the measurement display.
Page 29: Measurement Display
Menu Display Configure measurement display Configure measurement display 7.00 pH 25.6 °C Press menu key to select menu. Menu selection Select parameter setting using arrow keys, confirm with enter. Select: “Administrator level”: Passcode 1989 Select: [enter] (default setting). Return to meas Lingua 7.00 pH Parameter setting:...
Page 30: Start-Up
Prerequisite Mechanical and electrical installation of the components has been performed according to the separately enclosed operating and installation instructions (free download at www.knick.de): • Protos 3400(X) • Unical 9000(X) or Uniclean 900(X) • Ceramat WA 150(X) (or other retractable fittings)
Page 31: Parameter Setting: Operating Levels
Parameter setting Parameter Setting: Operating Levels Viewing level, Operator level, Administrator level Note: HOLD mode (Setting: BASE module) Viewing level, Operator level, Menu Display Administrator level 11.03 pH Open parameter setting 25.6 °C From the measuring mode: Menu selection Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm.
Page 32: Parameter Setting: Locking A Function
Parameter Setting: Locking a Function Administrator level: Enabling/locking functions for Operator level Note: HOLD mode (Setting: BASE module) Administrator level: Menu Display Enabling / locking a function Example: Blocking access to the calibration adjustments from the Operator level 11.03 pH Open parameter setting 25.0°C Parameter setting (Administrator)
Page 33: Parameter Setting For Phu 3400(X)-110
Parameter Setting for PHU 3400(X)-110 Activating parameter setting Menu Display Parameter setting Activating Parameter Setting 11.03 pH 25.0°C From the measuring mode: Menu selection Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm. Select: [enter] Passcode as delivered: 1989...
Page 34: Settings Of Sensor Data
Settings of Sensor Data With “Auto“, the tolerance limits for the monitoring criteria are determined by the analyzer. They are displayed in gray. These values cannot be edited. With ”Individual”, the tolerances can be adjusted. Note: HOLD mode active. Parameter Default Selection / Range / Notes Input filter...
Page 35 Parameter Setting of PHU 3400(X)-110 Note: HOLD mode active Menu Display Display Parameter selection Sensor data 7.00 pH 20.1 °C Sensor data are preset depending on Module PHU 3400-110 (Administrator) the sensor type. Input filter Sensor data Gray display lines cannot be edited. Cal preset values Sensoface provides information on TC process medium...
Page 36: Sensoface
Sensoface Sensoface is a graphical indication of the sensor condition – Sensocheck must have been activated during parameter setting. Sensocheck: Automatic monitoring of glass and reference electrode 24.3°C The “smileys” provide information on wear and required maintenance of the sensor (“friendly” - “neutral” - “sad”). Menu Display Activate Sensocheck...
Page 37 Sensoface is “sad” ... The “Diagnostics / Module PHU / Sensor network diagram” shows all current sensor parameters in a graphic diagram. Sensor Network Diagram 7.00 pH 24.1°C “Diagnostics / Module PHU / Sensor network Sensor network diagram diagram”. 1 - Slope 2 - Zero point Tolerance limit violations can be seen at a 3 - Ref impedance...
Page 38 Parameter Setting of PHU 3400(X)-110 Cal preset values Note: HOLD mode active Cal Preset Values Parameter Choices (default in bold print) Knick: 2.00 4.01 7.00 9.21 • Calimatic buffer Merck/Riedel: 2.00 4.00 7.00 9.00 12.00 DIN 19267: 1.09 4.65 6.79 9.23 12.75 NIST standard: 4.006 6.865 9.180...
Page 39: Sw 3400-005: Tolerance Adjustment
SW 3400-005: Tolerance Adjustment Program Flow Start tolerance band Calibration / Adjustment ? First Calibration? Erase tolerance band New entry Zero + Slope T-band check? Zero > Tolerance ? Slope > Tolerance ? Adjustment Calibration Manual check New tolerance band Old tolerance band End of tolerance band...
Page 40: Activating The Cal Tolerance Band
Activating the Cal Tolerance Band Select menu: Parameter setting/System control/Release of options Note: The TAN for releasing an additional function is only valid for the device with the corresponding serial number! Menu Display Activating an additional function 7.00 pH Menu selection 25.6 °C Open parameter setting.
Page 41 20.1 °C solutions is displayed in gray. Cal preset values (Administrator) The “Calimatic buffer” menu shows all Calimatic buffer Knick Mettler-Toledo Knick 2.00 4.01 buffer sets available. Merck/Riedel Drift check Select buffer set with enter. DIN 19267 Calibration timer NIST standard...
Page 42 Parameter Setting of PHU 3400(X)-110 TC process medium, ORP/rH value, delta function: Default settings and selection range Parameter Choices (default in bold print) Off, linear, ultrapure water, table • TC process medium Linear: enter temperature factor +XX.XX %/K • ORP/rH value Reference electrode Ag/AgCl, KCl 1 mol/l Ag/AgCl,KCI 3mol/l...
Page 43 Parameter Setting of PHU 3400(X)-110 TC process medium Note: HOLD mode active Menu Display TC process medium 7.00 pH TC process medium 24.0 °C You can choose from: Module PHU 3400-110 (Administrator) • Linear (entry of TC coefficient) Input filter Sensor data •...
Page 44 Parameter Setting of PHU 3400(X)-110 ORP/rH value, delta function Note: HOLD mode active Menu Display ORP/rH value, delta function ORP/rH value 7.00 pH 20.1 °C • Select type of reference electrode: ORP/rH value (Administrator) Ag/AgCl, KCl 1 mol/l (silver/silver chloride) Ref el Ag/AgCl, KCl 1m Ag/AgCl, KCl 3 mol/l...
Page 45 Parameter Setting of PHU 3400(X)-110 Messages: Default settings and selection range Parameter Choices (default in bold print) Off, device limits max., • pH value Variable limits: - Failure Limit LO - Warning Limit LO - Warning Limit HI - Failure Limit HI Off, device limits max., •...
Page 46 Parameter Setting of PHU 3400(X)-110 Messages Note: HOLD mode active Menu Display Messages Messages 7.00 pH 25.6°C All parameters determined by the Messages (Administrator) measuring module can generate Messages pH value Messages ORP value messages. Messages rH value Messages Temperature Device limits max.
Page 47: Documenting Parameter Setting
Documenting Documenting Parameter Setting You must reproducibly document all parameter settings in the device to achieve a high level of system and device security according to GLP. For that purpose, an Excel file is provided (on the CD-ROM shipped with the basic device) to enter the parameter settings.
Page 48 Documenting Parameter Setting From the application window of the Excel file, select the worksheet for the module the parameter settings of which you want to document. Set the parameters of the respective module and enter the selected values in the corresponding cells of the module worksheet. NOTICE! The "HOLD"...
Page 49: Progalog 3000 Software (Option) For Configuration And Documentation
Documentation The ProgaLog 3000 software is available for convenient configuration of the Protos 3400(X) process analysis system. The user interface can be switched to the Protos display languages English, German, French, Spanish, Italian, Swedish or Portuguese. The software comes on CD-ROM. It runs under Windows® 8 / 7 / XP.
Page 50 ProgaLog 3000 Software for Configuration and Documentation 4. Edit configuration data using ProgaLog 3000 When the configuration data have been loaded, the software lists the connected modules with all available configuration parameters: Fig.: ProgaLog 3000 configuration data The parameters are listed according to the modular device structure. All configuration parameters (except the "Sensor data details", which are deter- mined by digital sensors) can be edited at the PC.
Page 51 Protos 3400(X) Copy configuration (Adminstrator) Parameter setting / System control / Identical module equipment required for transfer Copy configuration. Select “Load configuration” to write the complete Load Configuration device configuration (except the passcodes) to Save the Protos 3400(X). Return Save...
Page 52: Configuration Using "Progalog 3000
3. Now configure the parameters for the selected system components. 4. Save the configuration. You can save the configuration to a memory card that has been pre- formatted in the Protos 3400(X) and transfer them to analyzers with identi- cal module configurations.
Page 53: Logbook, Factory Setting
Logbook Factory setting Logbook, Factory Setting Parameter setting/System control/Logbook Note: HOLD mode Menu Display Logbook, Factory setting 7.00 pH Logbook 25.6 °C Select which messages are to be Logbook (Administrator) logged in the logbook. Log failure Log warning The last 50 events are recorded with Erase logbook date and time.
Page 54: Configuring A Current Output
BASE module Current outputs Current Outputs, Contacts, OK Inputs Select menu: Parameter setting/Module BASE Note: HOLD mode active Parameter setting Display Menu BASE module 7.00 pH To configure current output Configuring a Current Output 19.2°C • Call up parameter setting •...
Page 55: Current Outputs: Characteristics
Current Outputs: Characteristics Select menu: Parameter setting/Module BASE • Linear characteristic The process variable is represented by a linear output current curve. Output current Process variable Start • Trilinear characteristic Two additional vertices must be entered: Output current 2nd vertex Y 1st vertex Y Process variable Start...
Page 56 • Function characteristic Nonlinear output current characteristic: allows measurements over several decades, e.g. measuring very low values with a high resolution and high values with a low resolution. Required: Entering a value for 50 % output current. Output current Entry for “50 % point”: e.g.: 10 % of measured value Process variable...
Page 57: Output Filter
Output Filter Time interval Time averaging filter To smoothen the current output, a low-pass filter with adjustable time interval can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached. The time interval can be set from 0 to 120 sec.
Page 58: Namur Signals: Current Outputs
Current outputs: Behavior during messages NAMUR Signals: Current Outputs Behavior during messages: HOLD, 22mA signal Behavior during messages Depending on the configuration (“Messages”) 83.1 % Air 19.0°C the current outputs switch to: Behavior during messages • Currently measured value HOLD Current meas.
Page 59: Namur Signals: Relay Contacts
NAMUR Signals: Relay Contacts Failure, maintenance request, HOLD (function check) As delivered, the floating relay outputs of the BASE module are assigned to the NAMUR signals: Failure Contact K4, normally closed (signaling current failure) Maintenance request Contact K3, normally open contact HOLD Contact K2, normally open contact NAMUR signals: Factory setting of contacts...
Page 60: Relay Contacts: Protective Wiring
Relay Contacts: Protective Wiring Protective wiring of relay contacts Relay contacts are subject to electrical erosion. Especially with inductive and capacitive loads, the service life of the contacts will be reduced. For suppres- sion of sparks and arcing, components such as RC combinations, nonlinear resistors, series resistors and diodes should be used.
Page 61: Relay Contacts, Usage
Relay contacts Relay Contacts Parameter setting/Module BASE/Relay contacts Menu Display Setting the relay contacts 7.00pH Relay Contacts, Usage 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance Variable NAMUR HOLD • Select “Module BASE” Limit value Limit value •...
Page 62: Relay Contacts: Sensoface Messages
Relay Contacts: Sensoface Messages Parameter setting/Module BASE/Relay contacts/Usage/Sensoface Menu Display Parameter setting (Sensoface) 7.00 pH Assign Sensoface messages to relay 19.0°C contacts Module BASE (Administrator) Output current I1 When more than one measuring Output current I2 module is used, the Sensoface mes- (NAMUR Failure) Contact K4 Contact K3...
Page 63: Rinse Contact
Rinse contact Rinse Contact Parameter setting/Module BASE/Relay contacts/Usage/Rinse contact Menu Display Configuring the rinse contact 7.00 pH Relay contacts, usage 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance Variable NAMUR HOLD • Select “Module BASE” Limit value Limit value •...
Page 64: Limit Value, Hysteresis, Contact Type
Limit value Limit Value, Hysteresis, Contact Type Parameter setting/Module BASE/Relay contacts/Usage Menu Usage as limit value 7.00 pH Relay output: Limit value 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance Variable NAMUR HOLD • Select “Module BASE” Limit value Limit value •...
Page 65: Ok1, Ok2 Inputs: Specify Level
OK1, OK2 Inputs: Specify Level Parameter setting/Module BASE/Inputs OK1, OK2 Note: HOLD mode (Setting: BASE module) Menu Display Setting the OK inputs 7.00 pH OK1 usage 19.2°C • Open parameter setting Inputs OK1, OK2 (Administrator) • Enter passcode For OK2 usage see “Function control matrix”...
Page 66: Selecting Parameter Set (A, B) Via Ok2 Input
Switching Parameter Sets via OK2 Parameter setting / System control / Function control matrix Note: HOLD mode (Setting: BASE module) Parameter Sets 2 complete parameter sets (A, B) can be stored in the analyzer. You can switch between the parameter sets using the OK2 input. The currently activated set can be signaled by a relay contact.
Page 67: Unical 9000(X) Parameter Setting
Setting the Unical 9000(X) parameters Unical 9000(X) Parameter Setting Functional Capabilities Setting Adjustable parameters Page • Control Off, Unical 9000, Uniclean 900 Pg 68 • Cal preset values Buffer set as configured in the PHU 3400-110 Cal Buffer 1 Calimatic (automatic) or selection of a buffer Cal Buffer 2 Calimatic (automatic) or selection of a buffer Adjustment, Calibration...
Page 68: Cal Preset Values Unical 9000
7.05 pH 25.6 °C taken over. Cal preset values (Administrator) Measuring module Module PHU 3400-110 Cal timer program Knick 2.00 4.01 Module PH 3400-032 Starts the selected program after Cal Buffer 1 Adjustment Cal Buffer 2 cal timer expiry. Calibration...
Page 69 Time control (fixed interval / week program) Menu Display Time control configuration 7.05 pH Time control: Fixed interval 25.6 °C The “Fixed interval” menu allows selec- Fixed interval (Administrator) Program tion of up to three programs. An indi- Clean Interval vidual time interval an be assigned to Program Cal 2point...
Page 70: Parameter Setting: Program Flows
Parameter setting: Program flows Cleaning program Parameter Setting: Program Flows Cleaning (Continuous), Media Monitoring Off Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Probe in MEASURE 0005 s 06: Program end...
Page 71: Cal 2Point (Continuous), Media Monitoring Off
Calibration program Parameter Setting: Program Flows Cal 2point (Continuous), Media Monitoring Off Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Buffer I 0000 s 06: Cal Buffer 1 07: Rinse water ON...
Page 72: Cal 1Point (Continuous), Media Monitoring Off
Parameter Setting: Program Flows Cal 1point (Continuous), Media Monitoring Off Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0003 s 03: Rinse water 0010 s 04: Rinse water 0002 s 05: Buffer I 0000 s 06: Cal buffer 1 (pH 4.01) 07: Rinse water 0010 s 08: Rinse water...
Page 73 DCS inputs BIN 1 ... BIN 3 of Unical 9000 Program is executed completely. Wait position is skipped. Notice: If the programs are started by the Protos 3400(X) from the Calibration or Maintenance menu, the wait position will be skipped.
Page 74: Parking
Parameter Setting: Program Flows Parking Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 s 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Purge air ON 0010 s 06: Purge air OFF 0002 s 07: Cal buffer 1 (pH 4.01) 08: Wait position...
Page 75: Measurement (Short-Time), Media Monitoring Off
Parameter Setting: Program Flows Measurement (Short-Time), Media Monitoring Off Display text Time [s] 01: Rinse water ON 0010 s 02: Rinse water OFF 0002 s 03: Probe in MEASURE 0005 s 04: Meas duration 0030 s 05: Probe in SERVICE 06: Cleaning agent 0020 s 07: Rinse water ON...
Page 76: Cal 2Point (Short-Time), Media Monitoring Off
Parameter Setting: Program Flows Cal 2point (Short-Time), Media Monitoring Off Display text Time [s] 01: Rinse water ON 0010 s 02: Rinse water OFF 0002 s 03: Buffer I 0000 s 04: Cal Buffer 1 05: Rinse water ON 0010 s 06: Rinse water OFF 0002 s 07: Buffer II...
Page 77: Cal 1Point (Short-Time), Media Monitoring Off
Parameter Setting: Program Flows Cal 1point (Short-Time), Media Monitoring Off Display text Time [s] 01: Rinse water ON 0010 s 02: Rinse water OFF 0002 s 03: Buffer I 0000 s 04: Cal buffer 1 (pH 4.01) 05: Rinse water ON 0010 s 06: Rinse water OFF 0002 s...
Page 78: Service
Service program Parameter Setting: Program Flows Service Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 s | Measure -> Service 03: Rinse water ON 0060 s 04: Rinse water OFF 0002 s 05: Purge air ON 0005 s 06: Purge air OFF 0002 s...
Page 79: Configuring The Program Flow
Parameter setting Menu Display Program flow 7.05 pH Configuring the Program Flow 25.6 °C Parameter setting / Probe control / Program flow (Administrator) Clean approx. 2:02 min Program flow / User 2: Cal 2point approx. 2:50 min Select “Edit” using arrow keys, Cal 1point approx.
Page 80: Configuring A Function
• Configure function Menu Display • Activate monitoring Configuring a Function 7.05 pH 25.6 °C Select a function using arrow keys, Program flow (Administrator) confirm with enter Cal Buffer 1 Function Cal Buffer 2 Program end Purge air On Probe in SERVICE Purge air Off Aux medium On Probe in MEASURE...
Page 81: Parameter Setting: Installation
Parameter setting: Installation Parameter Setting: Installation Configuration of Unical 9000 Functions Installation Default setting Adjustable parameters • Measurement procedures Continuous (Short-time) • Ext. control (DCS) (Polarity / Output settings) - Signal level of inputs Active: 10 ... 30 V (Active: 10 ... 30 V / active < 2V) DCS (36 ...
Page 82: Selecting The Measurement Procedure
• Meas. procedure Menu Display • External control via DCS Selecting the Measurement 7.05 pH 25.6 °C Procedure Installation (Administrator) • Continuous measurement: Meas. procedure Continuous Ext. control (DCS) With continuous measurement Short-time Sensor detection the pH electrode is located in the Access manual control Probe process medium and is retracted for...
Page 83: Control Via Process Control Cystem (Dcs)
Control via process control system Control via Process Control Cystem (DCS) Inputs/Outputs of Unical 9000(X) Designation I / O Level Function Probe moves to measure position Measuring/ Service Probe moves to service position Automat. interval control from Unical Auto / Manual Automat.
Page 84: Control Programs And Meas. Procedures
Further requests are stored and executed subse- quently. When you control the Unical 9000(X) via Protos 3400(X), you can block the Bin 1, Bin 2, Bin 3 signal lines as well as M/S and A/M to prevent conflicts (Parameter setting / Probe control / Installation / Ext.
Page 85: Sensor Detection
• Sensor detection Menu Display • Probe Sensor Detection 7.05 pH 25.6 °C Sensor detection “On” prevents Installation (Administrator) Meas. procedure Continuous accidental probe movement when the Ext. control (DCS) electrode has been removed. Sensor detection Immersion lock This is done by checking whether the Access manual control temperature detector integrated in Probe...
Page 86: Configuring Media Monitoring
Configuring media monitoring Configuring Media Monitoring Parameter setting / Unical 9000 / Installation Media Monitoring For perfect system control, the pH value (or temperature) of the media used (buffer solutions, cleaning solution, rinsing water ...) can be checked against a specified value in the calibration chamber.
Page 87: Media Adapter
• Media adapter, Additional media Menu Display • Start-up Media Adapter 7.05 pH 25.6 °C • Specifying the equipment Media adapter (Administrator) (Metering pump, Off, or Cleaner) Port I Metering pump Medium Buffer - I ------- • Designation of medium Displacement volume 25 ml Residual volume...
Page 88: System Forecast (Ceramat, Sensogate)
System forecast System Forecast (Ceramat, SensoGate) Monitoring the probe travel behavior of retractable fittings (with Unical 9000(X) software version 4.3 or higher) The "System Forecast" function enables monitoring of the probe travel behavior of the Ceramat or SensoGate retractable fittings. Possible signs of wear are detected in good time to prevent failure or down- times ("predictive maintenance").
Page 89: Reference / Probe Travel Profiles
System Forecast: Probe Travel Profiles Reference / Probe Travel Profiles Following installation of a system or after a repair, several cycles are run by call- ing the "System forecast / Edit reference profile" function. The travel behavior (probe travel profile) detected is saved as a "reference profile" with time and date.
Page 90: Setting The System Forecast Parameters
Setting the system forecast parameters Setting the System Forecast Parameters Menu: Parameter setting / Probe control / Installation / System forecast Menu Display System forecast Setting the system forecast 07.00 pH 25.6 °C parameters System control (Administrator) (only Ceramat and SensoGate types) Probe Rinse water Select a Ceramat or SensoGate...
Page 91: System Forecast: Reference Profile
System Forecast: Reference Profile Menu: Parameter setting / Probe control / Installation / System forecast System forecast: Menu Display Active reference profile Active reference profile “Auto” 7.00 pH 25.6 °C A reference profile is recorded System forecast in the background during the Active reference profile Auto 12/21/16 12:37 S a06 b17 c2...
Page 92: Setting Tolerances
System forecast: create reference profile System Forecast: Creating a Reference Profile Menu: Parameter setting / Probe control / Installation / System forecast System forecast: Menu Display Active reference profile: “User” Creating a “User” reference profile 7.00 pH 25.6 °C By selecting "Edit reference profile", System forecast you can create an individual “User”...
Page 93: System Forecast: Tolerance Specifications
System forecast: Tolerance specifications System Forecast: Tolerance Specifications Menu: Parameter setting / Probe control / Installation / System forecast Menu Display System forecast: Tolerances Tolerance specifications 7.00 pH 25.6 °C For monitoring during operation, System control (Administrator) permissible deviations in the sep- Active reference profile WA150 12/21/16 12:37 S a06 b17 c25 d33 e02 CM...
Page 94 System Forecast: Reference Profiles, Messages Menu: Parameter setting / Probe control / Installation / System forecast Menu Display System forecast Reference profiles, messages 7.00 pH 25.6 °C Monitoring allows forecast messages Messages to be switched off (“Off”) Monitoring Maintenance or to be output as U160 Pressure loss/Air sensor Active Active...
Page 95: System Forecast: Diagnostic Messages
System Forecast: Diagnostic Messages Menu: Diagnostics / System forecast Menu Display System forecast: Diagnostics Message list UNICAL active When you have activated "Monitoring Message list 1 messg. On" in the System forecast menu, a U168 SP SERVICE position not functioning violation of a preset tolerance will generate a message text.
Page 96: System Forecast: Recording On Smartmedia Card
System forecast: Record on SmartMedia card System Forecast: Recording on SmartMedia Card Menu: Parameter setting / Probe control / Installation / System forecast Menu Display System forecast: SmartMedia card Record on SmartMedia card 7.00 pH 25.6 °C If a SmartMedia card is installed, System control (Administrator) probe travel times can be saved on it 12/21/16 12:37 S a06 b17 c25 d33 e02 CM...
Page 97 System forecast: Messages System Forecast: Messages "System forecast" message Cause U160 SP Pressure loss/Air sensor Air leaking uncontrolled – air sensor defective U161 SP Probe valve not functioning Pilot valve does not switch; probe valve possibly does not switch U162 SP Air sensor not functioning Air sensor does not switch U163...
Page 98: Uniclean 900(X) Parameter Setting
Setting the Uniclean 900(X) parameters Uniclean 900(X) Parameter Setting Functional Capabilities Setting Adjustable parameters Page Pg 99 Off, Unical 9000, Uniclean 900 • Control Fixed interval, Week program: • Time control Fixed interval: Select program, interval Week program: Configuration of program flows Pg 100 •...
Page 99: Measuring Module
Time control (fixed interval / week program) Uniclean 900 Menu Display parameter setting 7.05 pH Open parameter setting 25.6 °C From the measuring mode: Menu selection Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm. Select: [enter] Return to meas...
Page 100 Week program Menu Display Time control configuration 7.05 pH Time control: Fixed interval 25.6 °C The “Fixed interval” menu allows selec- Fixed interval (Administrator) Program tion of up to three programs. An indi- Rinse Interval vidual time interval an be assigned to Clean Parking each program.
Page 101: Parameter Setting: Program Flows
Parameter setting: Program flows Rinse program Parameter Setting: Program Flows Rinsing (Continuous) Display text Time [s] 01: Probe in SERVICE 02: Rinse water ON 0060 sec 03: Rinse water OFF 0002 sec 04: Probe in MEASURE 0005 sec 05: Program end Cleaning (continuous) can also be started via a DCS input signal at input BIN1 of the Uniclean 900 probe controller.
Page 102: Cleaning (Continuous)
Cleaning program Parameter Setting: Program Flows Cleaning (Continuous) Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 sec 03: Rinse water ON 0060 sec 04: Rinse water OFF 0002 sec 05: Probe in MEASURE 0005 sec 06: Program end Cleaning (continuous) can also be started via a DCS input signal at input BIN1 of the Uniclean 900 probe controller.
Page 103 DCS inputs BIN 1 ... BIN 3 of Uniclean 900 Program is executed completely. Wait position is skipped. Note: If the programs are started by the Protos 3400(X) from the Calibration or Maintenance menu, the wait position will be skipped.
Page 104: Parking
Parameter Setting: Program Flows Parking Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 sec 03: Rinse water ON 0060 sec 04: Rinse water OFF 0002 sec 05: Purge air ON 0010 sec 06: Purge air OFF 0002 sec 07: Wait position >...
Page 105: Measuring (Short-Time)
Measuring program (short-time) Parameter Setting: Program Flows Measuring (Short-Time) Display text Time [s] 01: Rinse water ON 0010 sec 02: Rinse water OFF 0002 sec 03: Probe in MEASURE 0005 sec 04: Meas duration 0030 sec 05: Probe in SERVICE 06: Cleaning agent 0020 sec 07: Rinse water ON...
Page 106: Service
Service Program Parameter Setting: Program Flows Service Display text Time [s] 01: Probe in SERVICE 02: Cleaning agent 0020 sec | Measure -> Service 03: Rinse water ON 0060 sec 04: Rinse water OFF 0002 sec 05: Purge air ON 0005 sec 06: Purge air OFF 0002 sec...
Page 107: Editing A Program Step
Program flow Menu Display Function 7.05 pH Editing a Program Step 25.6 °C Select the program step you want Example (Administrator) Example Program name to edit using the arrow keys. 01: Probe in SERVICE Press enter: Edit: 03: Rinse water ON Insert Now you can choose between Delete...
Page 108: Parameter Setting: Installation
Parameter setting: Installation Parameter Setting: Installation Configuration of Uniclean 900 Functions Installation Default setting Adjustable parameters • Measurement procedures Continuous (Continuous / Short-time) • Ext. control (DCS) (Polarity / Output settings) - Signal level of inputs Active: 10 ... 30 V (Active: 10 ...
Page 109: Selecting A Measurement Procedure
• Meas. procedure Menu Display • External control via DCS Selecting a Measurement Procedure 7.05 pH 25.6 °C • Continuous measurement: Installation (Administrator) With continuous measurement Meas. procedures Continuous Ext. control (DCS) the pH electrode is located in the Short-time Sensor detection process medium and is retracted for Access manual control...
Page 110: Control Via Process Control System (Dcs)
Control via process control system Control via Process Control System (DCS) Inputs/Outputs of Uniclean 900(X) Designation I / O Level Function Probe moves to measure position Measuring/ Service Probe moves to service position Automatic interval control from Uniclean Auto / Manual Automatic intervals locked Program selection and start, manual / DCS * **...
Page 111: Control Programs And Meas. Procedures
Further requests are stored and executed subsequently. When you control the Uniclean 900(X) via Protos 3400(X), you can block the Bin 1, Bin 2, Bin 3 signal lines as well as M/S and A/M to prevent conflicts (Parameter setting / Uniclean 900 / Installation / Ext.
Page 112: Sensor Detection
• Sensor detection Menu Display • Probe Sensor Detection 7.05 pH 25.6 °C Sensor detection “On” prevents acci- Installation (Administrator) Continuous dental probe movement when the Meas. procedures Ext. control (DCS) electrode has been removed. Sensor detection Immersion lock This is done by checking whether the Access manual control temperature detector integrated in Probe...
Page 113: Media Adapter
• Media adapter, Additional media Menu Display • Start-up Media Adapter 7.05 pH 25.6 °C • Metering Pump Media adapter (Administrator) (On, Off ) Metering pump Medium Cleaning agent • Designation of medium, Displacement volume 50 ml Residual volume 250 ml •...
Page 114: Calibration / Adjustment
Calibration and adjustment Calibration / Adjustment Note: HOLD mode active Current outputs and relay contacts behave as configured • Calibration: Detecting deviations without readjustment • Adjustment: Detecting deviations with readjustment Caution: Without adjustment every pH meter delivers an imprecise or wrong output value! Every pH electrode has its individual zero point and its individual slope.
Page 115 Adjustment Adjustment means that the values determined by a calibration are taken over. The values determined for zero and slope are entered in the calibration record. (Cal record can be called up in the Diagnostics menu for the PHU 3400(X)-110 module).
Page 116: Calibration Methods
Calibration / Adjustment Calibration Methods One-Point Calibration The electrode is calibrated with one buffer solution only. Here, only the electrode zero point is detected and taken into account by the Protos. One-point calibration is appropriate and permissible whenever the measured values lie near the electrode zero point so that slope changes do not have much of an impact.
Page 117: Temperature Compensation
Calimatic tion with a temperature probe (Pt 100/Pt 1000/ Cal medium: Buffer solution Knick 2.00 4.01 7.00 9.21 NTC 30 kΩ/NTC 8.55 kΩ). If you work with When changing sensors perform automatic temperature compensation during...
Page 118: Automatic Calibration
Automatic Calibration Probe Control Calibration Procedures The probe controller (e.g. Unical 9000) allows automatic execution of calibra- tions either at fixed intervals or time-controlled according to a week program. The week program is defined in the “Parameter setting” menu. It can automatically start up to 10 programs flows for each weekday. Program Flows for One- and Two-Point Calibration The program flows for one- and two-point calibrations are preset but can be modified in the “Parameter setting”...
Page 119 Menu Display Probe control - Start program Open calibration 7.00 pH 25.6 °C Press menu key to select menu. Menu selection Select calibration using arrow keys, press enter to confirm, passcode 1147 (To change passcode, select: Parameter setting/System control/ Select: [enter] Passcode entry).
Page 120: Manual Electrode Calibration
Manual Electrode Calibration Probe Control Manual electrode calibration (zero, slope) must be performed with the elec- trode removed. For that purpose, the sensor lock-gate automatically moves into SERVICE position when the calibration menu is opened. Electrode located in the process medium. Warning! Before working on the sensor lock-gate, it must be moved into SERVICE position.
Page 121 Menu Display Probe in SERVICE position Select calibration method: 7.00 pH 25.6 °C (For descriptions see Pg 124 et seq.) Module PHU 3400-110 When you open the Calibration menu, Calimatic: automatic calibration the Protos automatically proposes the Manual: entry of buffer values Product calibration previous calibration method.
Page 122: Hold Function During Calibration
HOLD Function During Calibration Behavior of the signal and relay outputs during calibration Measuring Calibration K2 contact Module A Selecting the "HOLD" is Module B measuring module active The current output of Module A Module B the selected Calibration Calibration module is in "HOLD"...
Page 123: Selecting A Calibration Method
Menu Display Select calibration method (pH) Open calibration 7.00 pH 25.6 °C Press menu key to select menu. Menu selection Select calibration using arrow keys, confirm with enter, passcode 1147 (To change passcode, select: Parameter setting/System control/ Select: [enter] Passcode entry). Return to meas Lingua 7.00 pH...
Page 124: Calimatic Automatic Buffer Recognition
Calimatic Automatic Buffer Recognition Automatic Buffer Recognition (Calimatic) Automatic calibration using Knick Calimatic is performed with one, two, or three buffer solutions. Protos automatically detects the nominal buffer value on the basis of the electrode potential and the measured temperature.
Page 125 Menu Display Automatic buffer recognition Display of nominal buffer value. 7.00 pH 25.6 °C You can press “End” to reduce the Calimatic waiting time before stabilization of the Drift check with 1st buffer running Zero correction electrode potential (reduced accuracy Electrode potential -0000 mV of calibration values).
Page 126: Calibration With Manual Entry Of Buffer Values
Calibration with manual entry of buffer values Calibration / Adjustment Calibration with Manual Entry of Buffer Values Calibration with Manual Entry of Buffer Values Calibration with manual entry of buffer values is performed with one, two, or three buffer solutions. Protos displays the measured temperature.
Page 127 Menu Display Manual entry Calibration with first buffer solution. 4.00 pH 25.6 °C You can press “End” to reduce the Manual entry waiting time before stabilization of the Drift check with 1st buffer running. Zero correction electrode potential (reduced accuracy Electrode potential -0224 mV of calibration values).
Page 128: Product Calibration
Product calibration Calibration / Adjustment Product Calibration Product Calibration (Calibration with Sampling) When the electrode cannot be removed – e.g. for sterility reasons – its zero point can be determined with “sampling”. To do so, the currently measured pro- cess value is stored by the Protos. Immediately afterwards, you take a sample from the process.
Page 129 Menu Display Product calibration Product calibration 7.00 pH 25.6 °C Product calibration is performed Product calibration in 2 steps. Cal medium: Product Cal by taking sample Prepare sampling, and input of pH value Start with softkey or enter. Start Return 7.00 pH Step 1 25.0°C...
Page 130: Calibration By Entering Data From Premeasured Electrodes
Data entry - premeasured electrode Calibration / Adjustment Calibration by Entering Data from Premeasured Electrodes Data Entry of Premeasured Electrodes Entry of values for zero point, slope, and isothermal potential of a pH electrode. The values must be known, e.g. determined beforehand in the laboratory. Caution! Input of an isothermal potential V also applies to the calibration methods...
Page 131 Isothermal Potential The isothermal intersection point is the point of intersection between two cali- bration lines at two different temperatures. The potential difference between the electrode zero point and this intersection point is the isothermal potential “Viso“. It may cause measurement errors depending on the temperature. These errors can be compensated for by defining the “Viso“...
Page 132: Orp Calbration/Adjustment
ORP calibration Calibration / Adjustment ORP calbration/adjustment ORP Calbration/Adjustment The potential of a redox electrode is calibrated using a redox (ORP) buffer solu- tion. In the course of that, the difference between the measured potential and the potential of the calibration solution is determined. This potential difference is printed on the calibration solution bottle and is defined as the voltage across the redox electrode and a reference electrode.
Page 133 Menu Display ORP adjustment The type of reference electrode is 200 mV 25.6 °C selected during parameter setting. ORP adjustment Immerse electrode in calibration Reference electrode Ag/AgCl,KCl 1m Temperature +25.5°C medium and wait until the ORP value ORP input +200 mV has stabilized.
Page 134: Isfet Zero Adjustment
ISFET zero adjustment Calibration / Adjustment ISFET Zero Adjustment ISFET Zero Adjustment Notice: The PHU 3400(X)-110 module does not supply the power for operating the ISFET adapter. When measuring with an ISFET sensor (Durafet, InPro 3300), the nominal zero point must be adjusted each time a new sensor is connected (to adjust the operating point).
Page 135 Menu Display ISFET zero adjustment Immerse sensor in a zero point buffer 7.00 pH 25.6°C (6.5 ... 7.5). ISFET zero adjustment Enter temperature-corrected pH value Dip sensor in buffer solution! Enter temperature-corrected pH in the (see buffer table). range pH 6.5...7.5 then ‘’Start’’...
Page 136: Maintenance Of Phu 3400(X)-110
Maintenance Sensor monitor Temperature probe Maintenance of PHU 3400(X)-110 Sensor monitor, Temp probe adjustment Note: HOLD mode is active. Menu Display Maintenance Open Maintenance 7.00 pH 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select Maintenance (maint) using arrow keys, confirm with enter.
Page 137: Probe Maintenance Via Protos 3400(X)
Maintenance of Unical 9000(X), Uniclean 900(X) Probe maintenance Probe Maintenance via Protos 3400(X) “Maintenance / Probe control” Menu Menu Display Maintenance 7.00 pH Select “Probe control”. 25.6 °C The maintenance menu shows the Maintenance probe controller as a component of...
Page 138 Default: 2958. Warning for Use of Manual Control! Make sure that the probe is separated from the process! Manual control via Protos 3400(X) allows actuating the probe controller for servicing. Rinsing water, media supply, and valve functions can be tested...
Page 139 Single step control Single Step Control “Maintenance / Probe control” Menu Menu Display Maintenance Single step control UNICAL 7.00 pH 25.6 °C Each program can be executed in Unical 9000 single-step mode. A safety prompt is Start probe maintenance Manual control displayed before the program starts.
Page 140 Probe wear Probe Wear “Maintenance / Probe control” Menu Menu Display Maintenance Probe wear 7.00 pH 25.6 °C There are 2 counters: Probe wear • Check counter 2101 Probe travel total Check counter 750 of 20000 • Maintenance counter Maintenance counter 750 of 100000 In the menu Reset check counter...
Page 141: Diagnostics Functions
Diagnostics Diagnostics Functions General status information of the measuring system Select menu: Diagnostics - Logbook Menu Display Diagnostics functions Open diagnostics 7.00 pH 25.6°C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm with enter.
Page 142: Device Description
Menu Display Diagnostics functions Device Description 7.00 pH 22.7 °C Select module using arrow keys: Device description Module PHU 3400-110 Provides information on all modules pH, °C, and probe control installed: Function, serial number, Hardware: 1. Software: 3.0 Serial number 0000313 hardware and software version, Module FRONT...
Page 143: Diagnostics Of Phu 3400(X)-110
Diagnostics of PHU 3400(X)-110 Module diagnostics / Sensor monitor Module diagnostics / Menu Display Sensor monitor 7.00 pH Open diagnostics 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm with enter. Select: [enter] Then select "Module PHU".
Page 144: Calibration Timer
Diagnostics of PHU 3400(X)-110 Calibration timer, Tolerance band recorder, Cal record, Sensor network diagram, Statistics Menu Cal timer, Tolerance band recorder Display Calibration Timer After expiration of a presettable inter- val (Parameter setting, Module PHU, Cal preset values), the calibration timer generates a warning message as a °C reminder that calibration is required.
Page 145: Cal Record
Cal record, Sensor network diagram, Menu Display Statistics Cal Record 7.00 pH 24.2°C Data of last adjustment/ calibration, Cal record suitable for documentation to Active adjustment 05.04.10 09:34 Sensor type InPro3200SG ISO 9000 and GLP/GMP Serial number 08151234 Cal mode Data entry (Date, time, calibration method, zero and slope, iso- Zero...
Page 146: Diagnostics Of Unical 9000(X)
Diagnostics of Unical 9000(X) Unical status Unical network diagram Diagnostics of Unical 9000(X) Unical status, Unical network diagram Unical status, Menu Display Unical network diagram 7.00 pH Open diagnostics 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm with enter.
Page 147: Diagnostics Of Uniclean 900(X)
Uniclean 900(X) diagnostics Uniclean status Diagnostics of Uniclean 900(X) Uniclean Status Menu Display Uniclean status 7.00 pH Open diagnostics 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm with enter. Select: [enter] Then select Probe control.
Page 148: Diagnostic Messages Of System Forecast
System forecast System forecast Diagnostic Messages of System Forecast Menu: Diagnostics / System forecast Menu Display System forecast: Diagnostics Message List UNICAL active When you have activated "Monitoring Message list 1 messg. On" in the System forecast menu, a U168 SP SERVICE position not functioning violation of a preset tolerance will generate a message text.
Page 149: Setting Diagnostics Messages As Favorite
Setting diagnostics messages as favorite Setting Diagnostics Messages as Favorite Select menu: Parameter setting/System control/Function control matrix Secondary displays (1) Here, additional values are displayed in the measuring mode according to the factory setting. When the respective softkey (2) is pressed, the process variables measured by the modules plus date or time are displayed.
Page 150 Menu Display Select favorites Favorites menu Diagnostics functions can be called directly from the measuring mode using a softkey. The “Favorites” are selected in the °C Diagnostics menu. Favorites menu 09.03.10 7.00 pH Select favorites 25.6 °C Press menu key to select menu. Menu selection Select diagnostics using arrow keys, confirm with enter.
Page 151: Message List
Message list Diagnostics Functions General status information of the measuring system Select menu: Diagnostics - Message list Menu Display Diagnostics functions Opening the diagnostics menu 7.00 pH 25.6°C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter.
Page 152: Messages
Error messages Messages FRONT 3400-011 Module FRONT 3400(X)-015 Module FRONT messages Message type F008 Meas. processing (factory settings) FAIL F009 Module failure (Firmware Flash check sum) FAIL F060 KI process window exceeded (acknowledgeable message) User-defined F061 KI recorder parameter WARN F080 ComFu®-E Channel 1 –...
Page 153 Messages FRONT messages Message type F216 AuditTrail card FAIL F220 Calibration active Text F221 Maintenance active Text F222 Parameter setting active Text F223 Diagnostics active Text F225 Measurement active Text F226 Power supply OFF Text F227 Power supply ON Text F228 Software update Text...
Page 154 Messages BASE 3400-021 Module BASE 3400(X)-025/VPW Module BASE 3400(X)-026/24V Module BASE messages Message type B008 Meas. processing (factory settings) FAIL B009 Module failure (Firmware Flash check sum) FAIL B070 Current I1 Span WARN B071 Current I1 <0/4 mA WARN B072 Current I1 >...
Page 155 Messages PHU 3400(X)-110 Module pH messages Message type P008 Meas. processing (factory settings) FAIL P009 Module failure (Firmware Flash check sum) FAIL P010 pH range FAIL P011 pH Alarm LO_LO FAIL P012 pH Alarm LO WARN P013 pH Alarm HI WARN P014 pH Alarm HI_HI...
Page 156 Messages pH messages Message type P047 mV Alarm LO WARN P048 mV Alarm HI WARN P049 mV Alarm HI_HI FAIL P050 man. Temperature range FAIL P060 SENSOFACE SAD: Slope User-defined P061 SENSOFACE SAD: Zero User-defined P062 SENSOFACE SAD: Ref impedance (Sensocheck) User-defined P063 SENSOFACE SAD: Glass impedance (Sensocheck)
Page 157 Messages pH messages Message type P202 Cal: Buffer unknown Text P203 Cal: Identical buffers Text P204 Cal: Buf interchanged Text P205 Cal: Sensor unstable Text P206 Cal: Slope WARN P207 Cal: Zero WARN P208 Cal: Sensor failure (ORP check) FAIL P254 Module reset Text...
Page 158 Messages Unical 9000 with PHU 3400(X)-110 Module Probe control messages Message type U190 Probe control Buffer I almost empty WARN U191 Probe control Buffer II almost empty WARN U192 Probe control Cleaner almost empty WARN U194 Probe control Buffer I empty FAIL U195 Probe control Buffer II empty...
Page 159 Messages Probe control messages Message type U243 Check buffer II WARN U244 Check cleaner WARN U245 Check Add. medium 1 WARN U246 Check Add. medium 2 WARN U248 Probe control Water valve WARN U249 Proble check counter WARN U250 Proble maintenance counter WARN U251 Probe control Calibration error...
Page 161: System Forecast Messages
Error messages of system forecast System Forecast Messages "System forecast" message Cause U160 SP Pressure loss/Air sensor Air leaking uncontrolled – air sensor defective U161 SP Probe valve not functioning Pilot valve does not switch; probe valve possibly does not switch U162 SP Air sensor not functioning Air sensor does not switch...
Page 162: Error Messages Of Unical 9000(X)
Error messages of Unical 9000(X) Error Messages of Unical 9000(X) NAMUR Protos contacts DCS34 Message (PROTOS) class Fct.chk Failure Maint req. Alarm MAINT REQ. active Probe move time SERVICE (U234) MAINT REQ. active Probe Move time MEASURE (U231) FAIL active active Probe limit position SERVICE (U227)
Page 163 Cause System reaction Reset Remark – Low air pressure None, message By next smooth probe Limit position not – Probe sluggish only movement reached at the first trial. – Filter choked – Move time too long – Low air pressure None, message By next smooth probe Limit position not...
Page 164 Error Messages of Unical 9000(X) NAMUR Protos contacts DCS34 Message (PROTOS) class Fct.chk Failure Maint req. Alarm FAIL active Sensor dismounted (U221) FAIL active active Undefined security status (U222) MAINT REQ. active Safety valve defective (U235) MAINT REQ. active Sensor dismount guard defective (U229) MAINT REQ.
Page 165 Cause System reaction Reset Remark – Sensor dismounted Probe does not - When sensor has been Message can only – Probe cylinder untight move into MEAS remounted appear in SERVICE – Probe lines untight position, position – Dismount guard defective Message Sensor can only be removed in SERVICE...
Page 166 Error messages of probe control Error Messages of Unical 9000(X) NAMUR Protos contacts DCS34 Message (PROTOS) class Fct.chk Failure Maint req. Alarm MAINT REQ. active UNICAL Switch Water pressure (U220) MAINT REQ. active Probe cylinder untight (U228) MAINT REQ. active Proble check counter / Proble maintenance counter (U249 / U250)
Page 167 Cause System reaction Reset Remark – No water All programs Automatic as soon as Start immediately when – Water pressure too low requiring water water pressure OK intervals have expired are blocked – Probe cylinder untight None, message Automatic as soon as Probe cylinder or probe –...
Page 168: Error Messages Of Uniclean 900(X)
Error messages of Uniclean 900(X) Error Messages of Uniclean 900(X) NAMUR Protos contacts DCS34 Message (PROTOS) class Fct.chk Failure Maint req. Alarm MAINT REQ. active Probe move time SERVICE (U234) MAINT REQ. active Probe move time MEASURE (U231) FAIL active active Probe limit position SERVICE (U227)
Page 169 Cause System reaction Reset Remark - Low air pressure None, message By next smooth probe Limit position not - Probe sluggish only movement reached at the first trial. - Filter choked - Move time too long - Low air pressure None, message By next smooth probe Limit position not...
Page 170 Error Messages of Uniclean 900(X) NAMUR Protos contacts DCS34 Message (PROTOS) class Fct.chk Failure Maint req. Alarm FAIL active Sensor dismounted (U221) (Message with Ceramat only!) MAINT REQ. active Sensor dismount guard defective (U229) (Message with Ceramat only!) MAINT REQ. active Cleaner almost empty (U192)
Page 171 Cause System reaction Reset Remark - Sensor dismounted Probe does not - When sensor has been Message can only - Probe cylinder untight move into MEAS remounted appear in SERVICE - Probe lines untight position, position - Dismount guard defective Message Sensor can only be removed in SERVICE...
Page 172: Specifications
Specifications Specifications of PHU 3400(X) 110 Module –––––––––––––––––––––– ––––––––––––––––––––––––––––––––––––––––––––––––– pH/ORP input Simultaneous measurement of pH and ORP (Ex ia IIC) with glass electrode or ISFET Input for glass electrode or ISFET Input for reference electrode Input for redox (ORP) electrode or auxiliary electrode Measuring range (MR) pH value -2.00 ...
Page 173 – Data entry of premeasured electrodes Drift check Fine / standard / coarse Calimatic buffer sets: – Fixed buffer sets: Knick/Mettler-Toledo 2.00 / 4.01 / 7.00 / 9.21 Merck/Riedel 2.00 / 4.00 / 7.00 / 9.00 / 12.00 DIN 19267 1.09 / 4.65 / 6.79 / 9.23 / 12.75...
Page 174 Specifications –––––––––––––––––––––– ––––––––––––––––––––––––––––––––––––––––––––––––– Sensor network diagram Graphic representation of the current sensor parameters in a network diagram on the display: slope, zero, reference impedance, glass impedance, response time, calibration timer, deviation from calibration range (CalCheck) –––––––––––––––––––––– ––––––––––––––––––––––––––––––––––––––––––––––––– Sensor monitor Direct display of measured values from sensor for validation, pH input, ORP input, glass el.
Page 175: General Data
Specifications General data Explosion protection See www.knick.de (Ex module only) NAMUR NE 21 and EN 61326-1 EN 61326-2-3 Emitted interference Class B (residential area) Immunity to interference Industry Lightning protection EN 61000-4-5, Installation Class 2 Nominal operating conditions Ambient temperature: –20 ...
Page 176: Appendix
Appendix: Minimum Spans for Current Outputs The PHU 3400(X)-110 module is a measuring module. It does not provide current outputs. Current outputs are provided by the BASE module (basic device) or by communication modules (e.g. OUT, PID). The corresponding parameters must be set there. The minimum current span shall prevent that the resolution limit of the measurement technology (±...
Page 177: Buffer Table "Mettler-Toledo
Appendix: Buffer Table "Mettler-Toledo"...
Page 178: Buffer Table "Knick Calimat
Appendix: Buffer Table "Knick CaliMat" °C Order No. CS-P0200A/... CS-P0400A/... CS-P0700A/... CS-P0900A/... CS-P1200A/... 2.01 4.05 7.09 9.24 12.58 2.01 4.04 7.07 9.16 12.39 2.01 4.02 7.04 9.11 12.26 2.00 4.01 7.02 9.05 12.13 2.00 4.00 7.00 9.00 12.00 2.00 4.01 6.99...
Page 179: Buffer Table "Din 19267
Appendix: Buffer Table "DIN 19267"...
Page 180: Buffer Table "Nist Standard" (Din 19266: 2000-01)
Appendix: Buffer Table "NIST Standard" (DIN 19266: 2000-01) Notice: The pH(S) values of the individual charges of the secondary reference materi- als are documented in a certificate of an accredited laboratory. This certifi- cate is supplied with the respective buffer materials. Only these pH(S) values shall be used as standard values for the secondary reference buffer materials.
Page 181: Buffer Table "Techn. Buffers To Nist
Appendix: Buffer Table "Techn. Buffers to NIST"...
Page 182: Buffer Table "Hamilton
Appendix: Buffer Table "Hamilton"...
Page 183: Buffer Table "Kraft
Appendix: Buffer Table "Kraft"...
Page 184: Buffer Table "Hamilton A
Appendix: Buffer Table "Hamilton A"...
Page 185: Buffer Table "Hamilton B
Appendix: Buffer Table "Hamilton B"...
Page 186: Buffer Table "Hach
Appendix: Buffer Table "HACH"...
Page 187: Buffer Table "Ciba
Puff ertabellen Appendix: Buffer Table "Ciba" -03- Ciba (94) Puff er Nennwerte: 2,06 4,00 7,00 10,00 °C 2,04 4,00 7,10 10,30 2,09 4,02 7,08 10,21 2,07 4,00 7,05 10,14 2,08 4,00 7,02 10,06 2,09 4,01 6,98 9,99 2,08 4,02 6,98 9,95 2,06 4,00...
Page 188: Buffer Table "Reagecon
Puff ertabellen Appendix: Buffer Table "Reagecon" -09- Reagecon Puff er °C 0°C *2,01 *4,01 *7,07 *9,18 *12,54 5°C *2,01 *4,01 *7,07 *9,18 *12,54 10°C 2,01 4,00 7,07 9,18 12,54 15°C 2,01 4,00 7,04 9,12 12,36 20°C 2,01 4,00 7,02 9,06 12,17 25°C 2,00...
Page 189: Sw 3400-002: Specifiable Buffer Sets
SW 3400-002: Specifiable Buffer Sets Select menu: Parameter setting/System control/Buffer table Individual buffer set (with 3 buffer solutions) for pH measurement Buffer Table You can enter an individual buffer set (with 3 buffer solutions). To do so, you enter the nominal buffer values for the correct temperature (range 0 ... 95 °C, 5°C steps.
Page 190: Overview Of Parameter Setting
Overview of Parameter Setting Overview of Parameter Setting Parameter setting 7.00 pH 25.6 °C Activated from measuring mode: Press menu key to select menu. Menu selection Select parameter setting using arrow keys, confirm with enter. Administrator level Access to all functions, also passcode setting. Releasing or Select: [enter] blocking functions for access from the Operator level.
Page 191 Parameter Setting Menu Display settings: FRONT module Languages Measurement display Representation of measured values on the display: • Main display - Selecting the number of primary values displayed • Display format (one or two) • Viewing angle - Decimal places Measurement recorder Option: 2-channel, selection of process variable, start and end •...
Page 192 - Zero point - Sensocheck ref. el. - Sensocheck glass el. - Response time - Calcheck Cal preset values • Calimatic buffer - Knick - Mettler Toledo - Merck/Riedel - DIN 19267 - NIST standard / technical - Hamilton - Kraft...
Page 193 Parameter Setting Menu Unical 9000 On / Off (automatic calibration) Control Cal preset values Select calibration method for automatic control • Measuring module - Select measuring module • Cal buffer 1 - Menu entry depending on selected sensor type • Cal buffer 2 •...
Page 194 Parameter Setting Menu Unical 9000 • Media adapter - Port II Usage: Metering pump / Off - Medium Buffer 4.01 - Displaced volume 25 / 50 / 75 / 100 ml - Residual volume 0 / 250 / 500 ml - Monitoring Process value / Temperature / Off - Setpoint...
Page 195 Maintenance Menu BASE Module Current source Output current definable 0 ... 22 mA PHU 3400(X)-110 Module Sensor monitor pH / ORP input, RTD, Temp, Impedance glass + ref. el. Temp probe adjustment Compensating for lead length Probe control Start probe maintenance Service program is executed, Cal starts are possible Manual control Access to all control elements, passcode required...
Page 196: Index
Index Activate monitoring (Unical program) ................80 Adaptive calibration timer (diagnostics) ............... 144 Adaptive calibration timer (parameter setting) .............41 Additional media (Unical parameter setting) ..............87 Additional media (Uniclean parameter setting) ............113 Add-on function, activation ....................40 Adjustment ..........................115 Administrator level ........................31 Appendix ...........................
Page 197 Index Cal preset values ........................38 Cal preset values (Unical 9000) ....................68 Cal record ..........................145 Cal timer program (Unical 9000) ..................68 Change passcode ........................27 Check counter ......................... 140 Check interval (Unical 9000) ....................85 Check interval (Uniclean 900) .................... 112 Cleaning, continuous (Unical program) ................70 Cleaning, continuous (Uniclean program) ..............
Page 198 Index Diagnostics menu ........................141 Diagnostics messages ......................151 Diagnostics messages as favorite..................149 Diagnostics messages (system forecast) ................95 Disposal ............................2 Documenting parameter setting .................47, 48 Drift check ............................38 Edit program step (Unical 9000) ..................79 Edit program step (Uniclean 900) ..................107 EMC .............................
Page 199 Index Generating messages (measuring module) ..............46 Graphic display ..........................14 Hardware and software version ...................11 HOLD mode ..........................59 Hysteresis .............................64 Icons ............................208 Individual buffer set ......................189 Inserting the module .......................22 Intended use ..........................9 ISFET zero adjustment ......................134 LED ..............................14 Limit value ...........................64 Limit value, icons in the measurement display ..............64...
Page 200 Index Measurement procedures (Uniclean 900) ..............111 Measuring, short-time (Unical program) ................75 Measuring, short-time (Uniclean program) ..............105 Media adapter (Unical 9000) ....................87 Media adapter (Uniclean 900) ................... 113 Media at media adapter (Unical program) ..............86 Media monitoring (Unical program) ..................86 Menu selection ...........................26 Menu structure ...........................15 Message list ..........................
Page 201 Index One-point calibration ......................116 Operating levels .........................31 Operator level ..........................31 Option release ..........................40 ORP calbration/adjustment ....................132 ORP related to the standard hydrogen electrode ............132 Output filter ..........................57 Overview of parameter setting ..................190 Overview of system components ..................18 Parameter setting ........................47 Parameter setting (overview) ....................
Page 202 Index Program flow: Cal 1point, continuous (Unical 9000) ...........72 Program flow: Cal 1point, short-time (Unical 9000) .............77 Program flow: Cal 2point, continuous (Unical 9000) ...........71 Program flow: Cal 2point, short-time (Unical 9000) .............76 Program flow: Cleaning, continuous (Unical 9000) ............70 Program flow: Cleaning, continuous (Uniclean 900) ..........
Page 203 Index Safety information ........................10 Screw clamp connector ....................... 175 Sealing, enclosure ........................16 Sealing water (Unical parameter setting) ................85 Sealing water (Uniclean parameter setting) ..............112 Secondary displays ........................28 Select measurement procedure (Unical 9000) ...............82 Select measurement procedure (Uniclean 9000) ............109 Sensocheck, parameter setting ...................36 Sensoface .............................36 Sensoface criteria ........................37...
Page 204 Index Specifications ........................... 172 Start (4 mA) and end (20 mA) ....................54 Start-up ............................30 Start-up (Unical parameter setting) ...................87 Start-up (Uniclean parameter setting) ................113 Statistics ............................. 145 Switching parameter sets via OK2 ..................66 System forecast ..........................88 System forecast, messages ....................94 System forecast, parameter setting ..................90 System forecast, probe travel profiles ................89 System forecast, reference profiles ..................91...
Page 205 Index Tolerance specifications, system forecast ................93 Trademarks ............................ 2 Travel behavior of retractable fittings ................88 Two-point calibration ......................116 Unical 9000(X), connection ....................25 Unical 9000(X) error messages ..................162 Unical network diagram ...................... 146 Unical parameter setting ......................67 Unical status ..........................146 Uniclean 900(X), connection ....................25 Uniclean 900(X) error messages ..................
Page 206 Index...
Page 207 Index...
Page 208 Overview of icons Explanation of icons important for the Icon PHU 3400(X)-110 module The analyzer is in measuring mode. The analyzer is in calibration mode. HOLD mode active for currently calibrated module. The analyzer is in maintenance mode. HOLD mode active. The analyzer is in parameter setting mode.
Page 209 Overview of icons Overview of icons Explanation of icons important for the Icon probe controller The probe is in MEASURE position (“PROCESS”) The probe is in SERVICE position Rinse water active Metering pump at media adapter port I active. Metering pump at media adapter port II active. Metering pump at media adapter port III active.
Page 210: Menu Selection
Menu Selection PHU 3400(X)-110 Module Parameter setting ..............31 Documenting ....................47 Logbook ......................53 Factory setting ....................53 BASE module ....................54 Current outputs ....................54 Current outputs: Behavior during messages ........58 Relay contacts ....................61 Rinse contact ....................63 Limit value ......................64 Calibration and adjustment ..........114 Calimatic: automatic calibration ............
Page 211: Quick Access
Quick Access Functions for Uniclean 900(X) Controller Setting the Uniclean 900(X) parameters .......98 Time control (fixed interval / week program) ........99 Week program .................... 100 Parameter setting: Program flows ............101 Rinse program .................... 101 Cleaning program ..................102 Park program ....................103 Measuring program (short-time) ............
Page 212 Quick Access Functions for Unical 9000(X) Controller (For Uniclean 900(X) probe controller, see previous page.) Setting the Unical 9000(X) parameters .........67 Cal preset values ...................68 Time control ....................68 Time control (fixed interval / week program) ........69 Parameter setting: Program flows ............70 Cleaning program ..................70 Calibration program ..................71 Park program ....................73...

This manual is also suitable for:

Protos 3400x Protos phu 3400-110 Protos phu 3400x-110

Knick Protos 3400 User Manual

Intended Use

Safety Information

Short Description

Terminal Plate PHU 3400(X)-110 Module

Inserting the Module

Connecting the Probe Controller

Menu Selection

Menu Structure

Passcode Entry

Configuring the Measurement Display

Start-Up

Parameter Setting: Operating Levels

Parameter Setting for PHU 3400(X)-110

Unical 9000(X) Parameter Setting

System Forecast (Ceramat, Sensogate)

Uniclean 900(X) Parameter Setting

Calibration / Adjustment

Maintenance of PHU 3400(X)-110

Probe Maintenance Via Protos 3400(X)

Diagnostics Functions

Setting Diagnostics Messages as Favorite

Messages

Specifications

Appendix

Overview of Parameter Setting

Index

Menu Selection

Quick Access

Quick Links

Need help?

Questions and answers

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Summary of Contents for Knick Protos 3400