Knick Protos 3400(X) User Manual
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Knick Protos 3400(X) User Manual

Process analysis system
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Betriebsanleitung
Betriebsanleitung
User Manual
Aktuelle Produktinformation: www.knick.de
Aktuelle Produktinformation: www.knick.de
Latest Product Information: www.knick.de
Analysenmesssystem
Analysenmesssystem
Protos 3400(X)
Protos 3400(X)
Protos 3400(X)
Process Analysis System
Messmodul Protos CONDI 3400 (X)-051
Messmodul Protos CONDI 3400 (X)-051
Communication Module Protos MS 3400(X)-160
Deutsch
Deutsch
English
zur Leitfähigkeitsmessung mit induktiven Sensoren
zur Leitfähigkeitsmessung mit induktiven Sensoren
For Memosens Sensors
The Art of Measuring.
The Art of Measuring.
SENS
MEMO

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  • Page 1 Messmodul Protos CONDI 3400 (X)-051 User Manual Communication Module Protos MS 3400(X)-160 Deutsch Deutsch English zur Leitfähigkeitsmessung mit induktiven Sensoren zur Leitfähigkeitsmessung mit induktiven Sensoren For Memosens Sensors SENS MEMO Aktuelle Produktinformation: www.knick.de Aktuelle Produktinformation: www.knick.de Latest Product Information: www.knick.de...

  • Page 2: Return Of Products Under Warranty

    Trademarks The following trademarks are used in this manual without further marking: CalCheck®, Calimatic®, Protos®, Sensocheck®, Sensoface®, Unical®, VariPower®, Ceramat®, SensoGate® are registered trademarks of Knick Elektronische Messgeräte GmbH & Co. KG, Germany Memosens® is a registered trademark of Endress+Hauser Conducta GmbH & Co. KG, Germany Knick Elektronische Messgeräte GmbH &...

  • Page 3: Table Of Contents

    Table of Contents Protos MS 3400(X)-160 Module Return of Products under Warranty ..................2 Disposal ............................2 Trademarks ........................... 2 Intended Use ....................7 Safety Information ..................8 Application in hazardous locations: MS 3400X-160 module ........8 Conformity with FDA 21 CFR Part 11 .................. 9 Software Version ........................10 Modular Concept ........................11 Short Description ..................
  • Page 4 Table of Contents Protos MS 3400(X)-160 Module Memosens PH Maintenance ................. 50 Sensor monitor .........................50 Temp probe adjustment ......................50 Memosens PH Diagnostics Functions ............51 Message list ..........................51 Logbook ............................51 Sensor monitor .........................52 Cal record ............................52 Sensor network diagram .......................53 Sensor wear ..........................53 Calibration timer ........................54 Adaptive calibration timer ....................54...
  • Page 5 Table of Contents Protos MS 3400(X)-160 Module Product Calibration (Calibration with Sampling) ............84 Data entry of premeasured sensors .................86 Zero correction ..........................87 Maintenance (Memosens OXY) ..............88 Sensor monitor .........................88 Temp probe adjustment ......................88 Sensor maintenance .......................88 Diagnostics (Memosens OXY) ..............89 Sensor monitor .........................89 Cal record ............................90 Sensor network diagram OXY .....................90...
  • Page 6 Table of Contents Protos MS 3400(X)-160 Module CONDI Calibration / Adjustment ..............129 Temperature compensation ....................131 HOLD Function During Calibration ................132 Automatic calibration with standard calibration solution ........134 Manual entry of cal solution ..................... 136 Product calibration ....................... 138 Data entry of premeasured sensors ................

  • Page 7: Intended Use

    Intended Use The module provides an RS-485 interface for connecting Memosens sensors. An analog current input can accept a signal from a pressure transmitter for pressure compensation of oxygen sensors. A galvanically isolated switch- ing input allows the connection of monitoring equipment, such as a flow monitoring system.

  • Page 8: Safety Information

    • When installing the device in a hazardous location, observe the specifica- tions of the EC-Type-Examination Certificate and, if applicable, of the Control Drawing (download: www.knick.de). • Before commissioning you must prove that the device may be connected with other equipment, such as a supply unit including cables and wires.

  • Page 9: Conformity With Fda 21 Cfr Part 11

    Conformity with FDA 21 CFR Part 11 In their directive “Title 21 Code of Federal Regulations, 21 CFR Part 11, Electronic Records; Electronic Signatures“ the US American health agency FDA (Food and Drug Administration) regulates the production and processing of electronic documents for pharmaceutical development and production.

  • Page 10: Software Version

    Software Version MS 3400(X)-160 Module Protos 3400 device software The MS 3400(X)-160 module is supported by software version A.1 or higher. Module software MS 3400(X)-160 Software version 2.x Query actual device/module software When the analyzer is in measuring mode: Press menu key, open Diagnostics menu: Device description Menu Display Device description Device hardware and software...

  • Page 11: Modular Concept

    • FIU (Memosens and probe controller) (software occupies 2 slots) • Unical/Uniclean probe controller Documentation The basic unit is accompanied by a CD-ROM containing the complete documentation. Latest product information as well as user manuals for earlier software releases are available at www.knick.de.

  • Page 12: Short Description

    Short Description Short Description: FRONT Module 4 captive screws Transflective LC graphic display for opening the analyzer (240 x 160 pixels) (NOTICE! Make sure that the gasket between FRONT white backlighting, high resolution and BASE is properly seated and clean!) and high contrast.

  • Page 13: Short Description: Menu Structure

    Short Description: Menu Structure Basic functions: Calibration, maintenance, parameter setting, diagnostics Menu groups Calibration Maintenance Diagnostics Parameter setting Measuring Passcode: 2958 1246 1147 Operator level 1989 Administrator level Selection of BASE SYSTEM Message list Module 1 Point of meas Module 1 further menu FRONT Module 2...
  • Page 14 Short Description: FRONT Module View into the open device (FRONT module) Slot for SmartMedia card • Data recording The SmartMedia card expands the measurement recorder capacity to > 50,000 records. • Exchange of parameter sets 5 parameter sets can be stored on the SmartMedia card, 2 of them can be loaded simultaneously to the analyzer and be switched by remote control.

  • Page 15: Short Description: Base Module

    Short Description: BASE Module View into the open device (BASE module, 3 function modules installed) Module equipment Module identification: Plug & Play. Up to 3 modules can be combined as desired. Several input and communica- tion modules are available. BASE module 2 current outputs (free assignment of process variable) and 4 relay contacts, 2 digital inputs.

  • Page 16: Terminal Plate

    Terminal Plate Terminal plate of MS 3400-160 module: Attaching the terminal plates The terminal plates of the lower modules can be sticked to the inner side of the door. This facilitates maintenance and service.

  • Page 17: Wiring And Memosens Cable

    Wiring and Memosens Cable Terminal Wire color Wiring for Memosens or M12 cable Brown (BN) Power supply + Transparent Shield Green (GN) RS485 (A) Yellow (YE) RS485 (B) White (WH) Power supply – (GND) The connecting cable consists of an inductive connector for digital Memosens® sensors (bayonet lock).

  • Page 18: Parameter Setting: Operating Levels

    Parameter Setting: Operating Levels Viewing level, Operator level, Administrator level Note: HOLD mode (Setting: BASE module) Viewing level, Operator level, Menu Display Administrator level Open parameter setting 11.03 pH 25.6 °C From the measuring mode: Menu selection Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm.

  • Page 19: Parameter Setting: Locking A Function

    Parameter Setting: Locking a Function Administrator level: Enabling/locking functions for Operator level Note: HOLD mode (Setting: BASE module) Administrator level: Menu Display Enabling / locking a function Example: Blocking access to the calibration adjustments from the Operator level 82.3 % Air Open parameter setting 25.6°C Parameter setting (Administrator)

  • Page 20: Configuring The Measurement Display

    Configuring the Measurement Display Select menu: Parameter setting/Module FRONT/Measurement display Pressing meas (1) returns the analyzer to the measuring mode from any function. All process variables coming from the modules can be displayed. The table on the next page describes how to configure the measurement display. Measurement display Typical measurement display Secondary displays...
  • Page 21 Configuring the Menu Display measurement display Configuring the measurement display 8.06 pH 25.6°C Press menu key to select menu. Menu selection Select parameter setting using arrow keys, confirm with enter. Select: “Administrator level”: Passcode 1989 Select: [enter] (default setting). Lingua Return to meas 8.06 pH Parameter setting:...

  • Page 22: Documenting Parameter Setting

    Documenting Documenting Parameter Setting You must reproducibly document all parameter settings in the device to achieve a high level of system and device security according to GLP. For that purpose, an Excel file is provided (on the CD-ROM shipped with the basic device) to enter the parameter settings.
  • Page 23 Documenting Parameter Setting From the application window of the Excel file, select the worksheet for the module the parameter settings of which you want to document. Set the parameters of the respective module and enter the selected values in the corresponding cells of the module worksheet. NOTICE! The "HOLD"...

  • Page 24: Progalog 3000 Software (Option) For Configuration And Documentation

    ProgaLog 3000 Software (Option) for Configuration and Documentation The ProgaLog 3000 software is available for convenient configuration of the Protos 3400(X) process analysis system. The user interface can be switched to the Protos display languages English, German, French, Spanish, Italian, Swedish or Portuguese.
  • Page 25 ProgaLog 3000 Software for Configuration and Documentation 4. Edit configuration data using ProgaLog 3000 When the configuration data have been loaded, the software lists the connected modules with all available configuration parameters: Fig.: ProgaLog 3000 configuration data The parameters are listed according to the modular device structure. All configuration parameters (except the "Sensor data details", which are deter- mined by digital sensors) can be edited at the PC.
  • Page 26 ProgaLog 3000 Software for Configuration and Documentation Configuring the parameters, e.g. relay contact usage: Input errors are indicated by red highlighting: 5. Save the configuration data to SmartMedia card 6. Load the configuration data to the 7.00 pH 25.6 °C Protos 3400(X) Copy configuration (Adminstrator) Parameter setting / System control /...
  • Page 27 ProgaLog 3000 Software for Configuration and Documentation Configuration using "ProgaLog 3000" In the "Configurator" menu you can preconfigure a complete Protos 3400(X) process analysis system with up to 3 modules at your PC. 1. Select your configuration from the modular system components offered in the left-hand field.

  • Page 28: Module Configuration: Operating Mode

    Module Configuration: Operating Mode Open parameter setting Note: “HOLD” mode active. Menu Display Parameter setting Open parameter setting 7.00 pH 25.0°C From the measuring mode: Menu selection Press menu key to select menu. Select parameter setting using arrow keys, press enter to confirm. Select: [enter] Passcode 1989 (To change passcode:...

  • Page 29: Memosens Ph Parameter Setting

    8.06 pH 24.0 °C sent to the analyzer. Sensor identified These are, for example, the measuring range, Sensor: SE 555-Memosens zero and slope of the sensor. Without any Knick Manufacturer: MEMO SENS Serial number: 0000313 further parameter setting, measurement starts Adjustment:...
  • Page 30 Parameter Setting (Memosens PH) Note: HOLD mode active Menu Display Display Parameter selection Sensor data 7.00 pH 20.1 °C Memosens sensors provide most of Memosens PH (Administrator) the parameters automatically. Input filter Sensor data Sensoface provides information on Cal preset values the sensor condition (evaluating the TC process medium Delta function...
  • Page 31 - SIP counter (default: Off ) - Sensor operating time (default: Off ) Cal preset values Calimatic buffer Knick CaliMat Knick CaliMat, Mettler-Toledo, DIN 19267, NIST stan- dard, NIST technical, Hamilton, Kraft, Hamilton A, Hamilton B, Hach, Ciba, Reagecon, Table Drift control Standard Fine: 1.2 mV/min (Abort after 180 sec)

  • Page 32: Activating The Cal Tolerance Band (Memosens Ph)

    Activating the Cal Tolerance Band (Memosens PH) Select menu: Parameter setting/System control/Release of options Note: The TAN for releasing an additional function is only valid for the device with the corresponding serial number! Menu Display Activate additional function 7.00 pH Menu selection 25.6°C Open parameter setting.
  • Page 33 Parameter Setting (Memosens PH) TC process medium Note: HOLD mode active Menu Display TC process medium 7.00 pH TC process medium 24.0 °C You can choose from: Memosens PH (Administrator) • Linear (input of TC coefficient) Input filter Sensor data •...
  • Page 34 Parameter Setting (Memosens PH) TC process medium, delta function Note: HOLD mode active Temperature compensation of process medium Linear temperature compensation, reference temp fixed at 25 °C + TC/100 % (25 °C - T (25 °C) pH value compensated to 25 °C (25 °C) Measured pH value (temperature-corrected) Temperature factor [%/K]...
  • Page 35 Parameter Setting (Memosens PH) Messages Note: HOLD mode active Menu Display Messages Messages 7.00 pH 25.6°C All parameters determined by the Messages (Administrator) measuring module can generate Messages pH value Messages mV value messages. Device limits max.: Messages are generated when the Return process variable (e.g.

  • Page 36: Memosens Ph Calibration / Adjustment

    Calibration and adjustment Memosens PH Calibration / Adjustment Note: HOLD mode active for the currently calibrated module Current outputs and relay contacts behave as configured The calibration data are stored in the sensor. This allows calibrating, adjusting, regenerating or cleaning the sensors in a lab, far from the point of measure- ment.
  • Page 37 Adjustment (Memosens PH) Adjustment means that the values determined by a calibration are taken over. The values determined for zero and slope are entered in the calibration record. (Diagnostics / Module MS 3400-160 / Memosens PH / Cal record). These values are only effective for calculating the measured variables when the calibra- tion has been terminated with an adjustment.

  • Page 38: Calibration Methods

    Calibration / Adjustment (Memosens PH) Calibration methods With Memosens sensors, the calibration data are stored in the sensor. This allows using precalibrated sensors. When the Protos is used for precalibrating sensors in the lab, you can use the calibration routines described below. One-point calibration The electrode is calibrated with one buffer solution only.

  • Page 39: Temperature Compensation

    Protos measures the temperature of the 7.00 pH 25.6°C buffer solution using the temperature Calimatic detector integrated in the Memosens Calibration medium: buffer solution Knick 2.00 4.01 7.00 9.21 sensor. When changing sensors perform First adjustment for statistics! Measured cal temp +025.6°C Sensor replacement...

  • Page 40: Hold Function During Calibration

    HOLD Function During Calibration Behavior of the signal and relay outputs during calibration Measuring Calibration K2 contact Module A Selecting the "HOLD" is Module B measuring module active The current output of Module A Module B the selected Calibration Calibration module is in "HOLD"...
  • Page 41 Menu Display Select calibration method (pH) Open calibration 7.00 pH 25.6°C Press menu key to select menu. Menu selection Select calibration using arrow keys, press enter to confirm, passcode 1147 (To change passcode, select: Parameter setting/System control/ Select: [enter] Passcode entry). Lingua Return to meas 7.00 pH...

  • Page 42: Calimatic Automatic Buffer Recognition

    Calimatic automatic buffer recognition Automatic buffer recognition (Calimatic) Automatic calibration using Knick Calimatic is performed with one, two or three buffer solutions. Protos automatically detects the nominal buffer value on the basis of the electrode potential and the measured temperature. Any sequence of buffer solutions is possible, but they must belong to the buffer set defined during parameter setting.
  • Page 43 Menu Display Automatic buffer recognition Display of nominal buffer value. 7.00 pH 25.6°C You can press “End” to reduce the Calimatic waiting time before stabilization of the Drift check with 1st buffer running Zero correction electrode potential (reduced accuracy Electrode potential -0056 mV of calibration values).

  • Page 44: Calibration With Manual Entry Of Buffer Values

    Calibration with manual entry of buffer values Calibration / Adjustment (Memosens PH) Calibration with manual entry of buffer values Calibration with manual entry of buffer values Calibration with manual entry of buffer values is performed with one, two or three buffer solutions. Protos displays the measured temperature.
  • Page 45 Menu Display Manual entry Calibration with first buffer solution. 4.00pH 25.6°C You can press “End” to reduce the Manual entry waiting time before stabilization of the Drift check with 1st buffer running. Zero correction electrode potential (reduced accuracy Electrode potential -0224 mV of calibration values).

  • Page 46: Product Calibration

    Product calibration Calibration / Adjustment (Memosens PH) Product calibration Product calibration (calibration with sampling) When the electrode cannot be removed – e.g. for sterility reasons – its zero point can be determined with “sampling”. To do so, the currently measured pro- cess value is stored by the Protos.
  • Page 47 Menu Display Product calibration The module is in HOLD mode. 7.00 pH 25.6°C Product calibration Product calibration Cal medium: product Product calibration is Cal by taking sample and input of pH value performed in 2 steps. Prepare sampling, start by pressing softkey or enter. Start Return 7.00 pH...

  • Page 48: Calibration By Entering Data From Premeasured Electrodes

    Data entry - premeasured electrode Calibration / Adjustment (Memosens PH) Calibration by entering data from premeasured electrodes Data entry of premeasured electrodes Entry of values for zero point and slope of a pH electrode. The values must be known, e.g. determined beforehand in the laboratory. During calibration the module is in HOLD mode.
  • Page 49 Calibration / Adjustment (Memosens PH) Monitoring functions for calibration Protos provides comprehensive functions for monitoring proper calibration performance and the electrode condition. This allows documentation for quality management to ISO 9000 and GLP/GMP. • Sensocheck monitors the electrode condition by measuring the glass electrode impedance.

  • Page 50: Memosens Ph Maintenance

    Maintenance Sensor monitor Temperature probe Memosens PH Maintenance Sensor monitor, temp probe adjustment Note: HOLD mode active Menu Display Maintenance Opening the maintenance menu 7.00 pH 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select maintenance using arrow keys, confirm by pressing enter.

  • Page 51: Memosens Ph Diagnostics Functions

    Memosens PH Diagnostics Functions General status information of the measuring system Select menu: Diagnostics Menu Display Diagnostics functions Opening the diagnostics menu 7.20 pH 23.7 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter.

  • Page 52: Sensor Monitor

    Sensor monitor Cal record Diagnostics (Memosens PH) Sensor monitor, cal record Menu Display Sensor monitor, cal record Sensor monitor 7.00 pH 22.3 °C Shows the values currently measured Sensor monitor by the sensor. Important function for pH input -56.8 mV diagnostics and validation.

  • Page 53: Sensor Network Diagram

    Sensor network diagram Sensor wear Diagnostics (Memosens PH) Sensor network diagram PH, sensor wear Sensor network diagram PH, Menu Display sensor wear 7.00 pH Sensor network diagram 24.1°C Graphical representation of the Sensor network diagram PH 1 - Slope sensor parameters. Tolerance limit 2 - Zero point 3 - Ref impedance violations can be seen at a glance.

  • Page 54: Calibration Timer

    Calibration timer Tolerance adjustment Diagnostics (Memosens PH) Cal timer, adaptive cal timer, tolerance adjustment Menu Display Cal timer, tolerance band recorder Calibration timer After expiration of a presettable inter- val (Parameter setting, Memosens PH, Cal preset values), the calibration timer generates a warning message as a reminder that calibration is required.

  • Page 55: Memosens Ph/Orp Parameter Setting

    8.06 pH 24.0 °C sent to the analyzer. Sensor identified These are, for example, the measuring range, Sensor: SE 56K-MS_V1 zero and slope of the sensor. Without any Knick Manufacturer: MEMO SENS Serial number: 4711-0816 further parameter setting, measurement starts Adjustment:...
  • Page 56 Parameter Setting (Memosens PH/ORP) Note: HOLD mode active Menu Display Display Parameter selection Sensor data 7.00pH 20.1 °C Memosens sensors provide most of Memosens PH/ORP (Administrator) the parameters automatically. Input filter Sensor data Sensoface provides information on Cal preset values the sensor condition (evaluating the TC process medium Delta function...

  • Page 57: Memosens Orp Parameter Setting

    24.0 °C sent to the analyzer. Sensor identified These are, for example, the measuring range, Sensor: SE564X/1-NMSN zero and slope of the sensor. Without any Manufacturer: Knick MEMO SENS Serial number: 380815 further parameter setting, measurement starts Adjustment: 05/20/10 09:13 at once, the measuring temperature is simulta- neously detected.
  • Page 58 Parameter Setting (Memosens ORP) Note: HOLD mode active Menu Display Display Parameter selection Sensor data 200 mV 20.1 °C Memosens sensors provide most of Memosens ORP (Administrator) the parameters automatically. Input filter Sensor data Cal preset values Delta function Messages Sensoface provides information on Block Return...
  • Page 59 Parameter Setting (Memosens ORP) Parameter Default Selection / Range Input filter Pulse suppression On, Off Sensor data Sensoface On, Off Sensor monitoring details Sensor parameters SIP cycles and sensor operating time Cal preset values Cal timer monitoring Auto: 0168h Auto, Off, Individual ORP check Test period 10 s Off, On...
  • Page 60 Parameter Setting (Memosens ORP) Delta function Note: HOLD mode active Menu Display Delta function 200 mV Delta function 20.1 °C When a delta value is entered, the Delta function (Administrator) system calculates the difference Delta function mVORP Delta value Output value = measured value – delta value The output value controls all outputs Return and is shown on the display.
  • Page 61 Parameter Setting (Memosens ORP) Messages Note: HOLD mode active Menu Display Messages Messages 200 mV 25.6°C All parameters determined by the Messages (Administrator) measuring module can generate Messages ORP value messages. Device limits max.: Messages are generated when the Return process variable (e.g.

  • Page 62: Memosens Orp Calibration / Adjustment

    ORP calibration Memosens ORP Calibration / Adjustment ORP calbration/adjustment ORP calbration/adjustment The potential of a redox electrode is calibrated using a redox (ORP) buffer solu- tion. In the course of that, the difference between the measured potential and the potential of the calibration solution is determined. This potential difference is printed on the calibration solution bottle and is defined as the voltage across the redox electrode and a reference electrode.

  • Page 63: Temperature Dependence Measured Against She (Standard Hydrogen Electrode)

    Menu Display ORP adjustment The module is in HOLD mode! 249 mV 25.6°C ORP adjustment Immerse electrode in calibration Reference electrode Ag/AgCl,KCl 3m Temperature +25.5°C medium and wait until the ORP value ORP input 249 mV has stabilized. Enter the nominal ORP value (bottle). ORP setpoint +220 mV Return...

  • Page 64: Memosens Orp Maintenance

    Maintenance Sensor monitor Temperature probe Memosens ORP Maintenance Sensor monitor / Temp probe adjustment Note: HOLD mode active Menu Display Maintenance Opening the maintenance menu 220 mV 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select maintenance using arrow keys, confirm by pressing enter.

  • Page 65: Memosens Orp Diagnostics Functions

    Memosens ORP Diagnostics Functions General status information of the measuring system Select menu: Diagnostics Menu Display Diagnostics functions Opening the diagnostics menu 220 mV 23.7 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter.

  • Page 66: Sensor Monitor

    Sensor monitor Cal record Diagnostics (Memosens ORP) Sensor monitor Menu Display Sensor monitor 220 mV Opening the diagnostics menu 22.3 °C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter. Select: [enter] Then select Memosens ORP.

  • Page 67: Cal Record

    Sensor network diagram Sensor wear Diagnostics (Memosens ORP) Cal record Menu Display Cal record Cal record 220 mV 22.3 °C Data of last adjustment/ calibration, Cal record suitable for documentation to Active adjustment 05/23/10 15:35 Sensor model SE564X/1-NMSN ISO 9000 and GLP/GMP Serial No.

  • Page 69: Memosens Oxy (Tan Required)

    Memosens OXY (TAN required) SW3400-015: Oxygen measurement SW3400-016: Oxygen trace measurement For connecting Memosens OXY sensors to the MS 3400(X)-160 module, you require the additional function SW 3400-015. For measuring oxygen traces, you require the additional function SW 3400-016. The additional functions are device-specific. When ordering an additional func- tion, you therefore have to specify the serial number of your FRONT module in addition to the respective order number.

  • Page 70: Activating An Additional Function

    Activating an Additional Function Select menu: Parameter setting/System control/Release of options Note: The TAN for releasing an additional function is only valid for the device with the corresponding serial number (see previous page). Menu Display Activate additional function 83.3 %Air Menu selection 25.6 °C Open parameter setting.

  • Page 71: Parameter Setting (Memosens Oxy)

    24.0 °C sent to the analyzer. Sensor identified These are, for example, the measuring range, SE 707-Memosens Sensor: zero and slope of the sensor. Without any Manufacturer: Knick SENS MEMO 0001013 Serial number: further parameter setting, measurement starts Adjustment: 04/24/10 11:07 at once, the measuring temperature is simulta- neously detected.
  • Page 72 Parameter Setting (Memosens OXY) Note: HOLD mode active. Menu Display Display Parameter selection Sensor data 83.3 %Air 20.1 °C Memosens sensors provide most of Memosens OXY (Administrator) the parameters automatically. Input filter Sensor data Cal preset values Pressure correction Salinity correction Messages Return Block...
  • Page 73 Parameter Setting (Memosens OXY) Note: HOLD mode active. Parameter Default Selection / Range Input filter Pulse suppression Weak Off, Weak, Medium, Strong Input filter 010 sec xxx sec (entry) Sensor data Measure in Liquids Liquids, Gases Sensoface On, Off Sensor monitoring details Sensor parameters SIP cycles and sensor operating time Cal preset values...
  • Page 74 Parameter Setting (Memosens OXY) Messages Note: HOLD mode active Menu Display Messages Messages 83.3 %Air 25.6°C All parameters determined by the Messages (Administrator) measuring module can generate Messages Saturation %Air messages. Messages Saturation %O 2 Messages Concentration Device limits max.: Messages Partial pressure Messages are generated when the process variable (eg, saturation) is...

  • Page 75: Calibration / Adjustment (Memosens Oxy)

    Calibration and adjustment Calibration / Adjustment (Memosens OXY) Note: The HOLD mode is active for the currently calibrated module, the current outputs behave as configured. With Memosens sensors, the calibration data are stored in the sensor. This allows using precalibrated sensors. When the Protos is used for precalibrating sensors in the lab, you can use the calibration routines described below.
  • Page 76 Adjustment (Memosens OXY) Adjustment means that the values determined by a calibration are taken over. The values determined for zero and slope are entered in the calibration record. (Cal record can be called in the Diagnostics menu for Memosens OXY.) These values are only effective for calculating the measured variables when the calibration has been terminated with an adjustment.

  • Page 77: Recommendations For Calibration

    Adjustment (Memosens OXY) Recommendations for calibration It is always recommended to calibrate in air. Compared to water, air is a cali- bration medium which is easy to handle, stable, and thus safe. In the most cases, however, the sensor must be removed for a calibration in air. In certain processes the sensor cannot be removed for calibration.

  • Page 78: Hold Function During Calibration

    HOLD Function During Calibration Behavior of the signal and relay outputs during calibration Measuring Calibration K2 contact Module A Selecting the "HOLD" is Module B measuring module active The current output of Module A Module B the selected Calibration Calibration module is in "HOLD"...
  • Page 79 Menu Display Selecting a calibration method Opening the calibration menu 83.0%Air 25.6°C Press menu key to select menu. Menu selection Select calibration using arrow keys, press enter to confirm, passcode 1147 (To change passcode, select: Parameter setting/System control/ Select: [enter] Passcode entry).

  • Page 80: Automatic Calibration In Water

    Automatic calibration in water Calibration / Adjustment (Memosens OXY) Automatic calibration in water Automatic calibration in water The slope is corrected using the saturation value (100 %) related to air saturation. During calibration the module is in HOLD mode. Current outputs and relay contacts of the module behave as configured (BASE module).
  • Page 81 Automatic calibration Menu Display in water 80.3%Air Display of selected calibration 25.6°C medium (Air-sat. water) Automatic - Water Enter cal pressure if “manual” has been Cal medium: Air-sat. water When changing sensors perform configured. First Adjustment for statistics! Start with softkey or enter Sensor replacement 1013 mbar Input cal pressure...

  • Page 82: Automatic Calibration In Air

    Automatic calibration in air Calibration / Adjustment (Memosens OXY) Automatic calibration in air Automatic calibration in air The slope is corrected using the saturation value (100 %), similar to air satu- ration of water. Since this analogy only applies to water-vapor saturated air (100 % relative humidity) and often the calibration air is less humid, the relative humidity of the calibration air must also be specified.
  • Page 83 Automatic calibration Menu Display in air 80.3%Air Calibration medium: Air 25.6°C Select: First Adjustment Automatic - Air Calibration medium: Air Enter relative humidity, eg: When changing sensors perform First Adjustment for statistics! • Ambient air: 50 % Sensor replacement • Bottled gas: 0 % Relative humidity 0050% 1013 mbar...

  • Page 84: Product Calibration (Calibration With Sampling)

    Product calibration: Saturation Calibration / Adjustment (Memosens OXY) Product calibration (saturation/concentration/partial pressure [hPa, mmHg] – preset in: Parameter setting / Cal preset values) Product Calibration (Calibration with Sampling) When the sensor cannot be removed – eg, for sterility reasons – its slope can be determined with “sampling”.
  • Page 85 Menu Display Product calibration: Saturation Product calibration Sat 80.3%Air 25.6°C Product calibration is performed Product calibration Sat Cal medium: Product in 2 steps. Cal by taking sample Prepare reference measurement and entering saturation (eg, with portable meter), start by pressing softkey or enter Return Start 80.3%Air...

  • Page 86: Data Entry Of Premeasured Sensors

    Data entry of premeasured sensors Calibration / Adjustment (Memosens OXY) Data entry of premeasured sensors Data entry of premeasured sensors Entry of values for slope and zero point of a sensor, related to 25°C, 1013 mbar. During calibration the module is in HOLD mode. Current outputs and relay contacts of the module behave as configured (BASE module).

  • Page 87: Zero Correction

    Zero correction Calibration / Adjustment (Memosens OXY) Zero correction Zero correction For trace measurements below 500 ppb, the zero point should be calibrated. If a zero correction is performed, the sensor should remain for at least 10 to 60 minutes in the calibration medium (media containing CO : at least 120 min) to obtain stable, non-drifting values.

  • Page 88: Maintenance (Memosens Oxy)

    Maintenance (Memosens OXY) Sensor monitor, temp probe adjustment, sensor maintenance Note: HOLD mode active Menu Display Maintenance From the measuring mode: 83.3 %Air 25.6°C Press menu key to select menu. Menu selection Select maintenance using arrow keys, confirm by pressing enter. Passcode 2958 (To change passcode: Select: [enter]...

  • Page 89: Diagnostics (Memosens Oxy)

    Diagnostics (Memosens OXY) Sensor monitor Menu Display Module diagnostics, Sensor monitor 83.3 %Air Opening the Diagnostics menu 25.6°C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, press enter to confirm. Select: [enter] Then select “Memosens OXY”.

  • Page 90: Cal Record

    Diagnostics (Memosens OXY) Cal record, Sensor network diagram, Sensor wear monitor Cal record, Sensor network diagram, Menu Display Sensor wear monitor Cal record 83.3 %Air 25.6°C Data of last calibration, suitable for Cal record Active adjustment 06/09/10 09:06 documentation to ISO 9000 and GLP SE 707 Memosens Sensor model Serial number...

  • Page 91: Memosens Cond Parameter Setting

    All sensor-typical parameters are automatically 0.245 mS/cm 24.0 °C sent to the analyzer. Sensor identified Without any further parameter setting, Sensor: SE 630-Memosens measurement starts at once, the measuring Knick Manufacturer: MEMO SENS 0001013 Serial number: temperature is simultaneously detected. Adjustment: 04/24/10 11:07 With “Plug&Measure”, premeasured Memosens...
  • Page 92 Parameter Setting (Memosens COND) Note: HOLD mode active Menu Display Display Parameter selection Sensor data 0.245 mS/cm 20.1 °C Memosens sensors provide most of Memosens COND (Administrator) the parameters automatically. Input filter Sensor data Cal preset values TC process medium Concentration Messages Return...
  • Page 93 Parameter Setting (Memosens COND) Parameter Default Selection / Range Input filter Pulse suppression On, Off Sensor data Sensoface On, Off Sensor monitoring details Cell constant Auto Auto, Individual Sensocheck Off, On (Message Off/Failure/Maintenance request) CIP counter 0, Max. cycles SIP counter 0, Max.
  • Page 94 Concentration Curves (Memosens COND) Sulfuric acid H c [% by wt] Nitric acid HNO c [% by wt]...
  • Page 95 Concentration Curves (Memosens COND) Hydrochloric acid HCl c [% by wt] Sodium hydroxide solution NaOH c [% by wt]...
  • Page 96 Concentration Curves (Memosens COND) Table salt solution NaCl c [% by wt] Oleum [mS/cm] c [% by wt]...

  • Page 97: Concentration Table (Memosens Cond)

    Concentration Table (Memosens COND) Select menu: Parameter setting/System control/Concentration table Specifying a concentration solution for conductivity measurement Concentration Table To specify the customer-specific solution, 5 concentration values A-E are entered in a matrix together with 5 temperature values 1-5. To do so, first enter the 5 temperature values, then enter the respective conductivity values for each concentration A-E.

  • Page 98: Usp Function (Memosens Cond)

    USP Function (Memosens COND) Monitoring of ultrapure water in the pharmaceutical industry (Select: Parameter setting, Memosens COND) USP function, define switching output 0.003 mS/cm 25.6 °C When a Memosens COND is installed, one of the Contact K1 (Administrator) floating relay outputs of the BASE module (K1, Usage NAMUR maintenance Variable...

  • Page 99: Ph Value Calculation (Memosens Cond)

    pH Value Calculation (Memosens COND) Note: 2 conductivity modules required pH value calculation by means of dual conductivity measurement When monitoring boiler feed water in power plants, the pH value can be cal- culated by means of a dual conductivity measurement. For that purpose, the boiler feed water conductance is measured before and after the ion exchanger.
  • Page 100 pH Value Calculation (Memosens COND) Recommended pH ranges: 10 ± 0.2 for < 136 bar operating overpressure or 9.5 ± 0.2 for > 136 bar operating overpressure Conductivity measured after cation exchanger (COND2) Figure: Conditioning the feed water of natural circulation boilers with sodium hydroxide. Relationship between the pH value and the conductivity measured before and after the cation exchanger.

  • Page 101: Calculation Blocks (Memosens Cond)

    Calculation Blocks (Memosens COND) Select menu: Parameter setting/System control/Calculation Blocks Calculation of new variables from measured variables Calculation Blocks Two measuring modules with all their measured values serve as input for the calculation block. In addition, the general device status (NAMUR signals) is taken into account.
  • Page 102 Activating Calculation Blocks Select menu: Parameter setting/System control/Calculation Blocks Combining 2 COND measuring modules to Calculation Blocks Combining 2 COND modules (e.g. Memosens COND) With three measuring modules the following Calculation Block combinations are possible: Two Calculation Blocks can be activated. Menu Display Activating Calculation Blocks...
  • Page 103 Configuring a Calculation Block Select menu: Parameter setting/System control/Calculation Blocks Setting the process variable to be calculated Menu Display Configuring a Calculation Block Select Calculation Block 40.00 µS/cm 25.6 °C • Open parameter setting Parameter setting (Administrator) • System control System control Module FRONT 3400-011 •...

  • Page 105: Memosens Cond Calibration / Adjustment

    Calibration and adjustment Memosens COND Calibration / Adjustment Note: HOLD mode active for the currently calibrated module Current outputs and relay contacts behave as configured With Memosens sensors, the calibration data are stored in the sensor. This allows using precalibrated sensors. When the Protos is used for precalibrating sensors in the lab, you can use the calibration routines described below.
  • Page 106 Adjustment Adjustment (Memosens COND) Adjustment means that the cell constant determined by a calibration is taken over. It is entered in the calibration record. (Cal record can be called in the Diagnostics menu for Memosens COND.) The value is only effective for calculating the measured variables when the calibration has been terminated with an adjustment and the data have been saved in the Memosens sensor.

  • Page 107: Temperature Compensation

    Temperature compensation Calibration / Adjustment (Memosens COND) Temperature compensation Temperature compensation during calibration The conductivity value of the calibration solution is temperature-dependent. For calibration, the calibration solution temperature must therefore be known in order to choose the actual value from the conductivity table. Automatic temperature compensation For automatic cal temp detection, the Protos 0.249 mS/cm...

  • Page 108: Hold Function During Calibration

    Calibration method HOLD Function During Calibration Behavior of the signal and relay outputs during calibration Measuring Calibration K2 contact Module A Selecting the "HOLD" is Module B measuring module active The current output of Module A Module B the selected Calibration Calibration module...
  • Page 109 Menu Display Selecting a calibration method Open Calibration 0.020 mS/cm 25.6°C Press menu key to select menu. Menu selection Select calibration using arrow keys, press enter to confirm, passcode 1147 (The passcode can be edited by the administrator.) Select: [enter] Return to meas Lingua 0.020 mS/cm...

  • Page 110: Automatic Calibration With Standard Calibration Solution

    Automatic calibration Calibration / Adjustment (Memosens COND) Automatic calibration with standard calibration solution Automatic with standard cal solution For automatic calibration, the conductivity sensor is immersed in a standard calibration solution (NaCl or KCl, selected during parameter setting: From the measured conductance and temperature, the Protos automatically calculates the cell constant.
  • Page 111 Menu Display Automatic calibration 0250 mS/cm Select calibration menu 25.0 °C Select “Memosens COND” Memosens COND Automatic with standard cal solution Manual entry of cal solution Select calibration method: Product calibration Data entry - premeasured sensor “Automatic with standard cal solution“, confirm by pressing enter.

  • Page 112: Manual Entry Of Cal Solution

    Manual entry of cal solution Calibration / Adjustment (Memosens COND) Manual entry of cal solution Manual entry of cal solution For calibration with manual entry of the calibration solution’s conductivity, the sensor is immersed in a calibration solution. Protos determines a conductivity/ calibration temperature value pair.
  • Page 113 Menu Display Manual entry of cal solution 0.020 mS/cm Select calibration menu 25.0 °C Select “Memosens COND” Memosens COND Automatic with standard cal solution Manual entry of cal solution Select calibration method: Product calibration Data entry - premeasured sensor “Manual entry of cal solution”, confirm by pressing enter.

  • Page 114: Product Calibration

    Product calibration Calibration / Adjustment (Memosens COND) Product calibration Product calibration When the sensor cannot be removed, e.g. for sterility reasons (for biotechnical processes), its cell constant can be determined with “sampling”. To do so, the currently measured process value is stored by the Protos. Immediately afterwards, you take a sample from the process.
  • Page 115 Menu Display Product calibration 0.249 mS/cm Select calibration menu 25.0 °C Select “Memosens COND” Memosens COND Automatic with standard cal solution Select calibration method: Manual entry of cal solution ”Product calibration”, Product calibration Data entry - premeasured sensor confirm by pressing enter. The module is in HOLD mode! Return 0.249 mS/cm...

  • Page 116: Data Entry Of Premeasured Sensors

    Data entry of premeasured sensors Calibration / Adjustment (Memosens COND) Data entry of premeasured sensors Data entry of premeasured sensors Entry of cell constant and zero point of a sensor, related to 25°C, 1013 mbar. During calibration the module is in HOLD mode. Current outputs and relay contacts of the module behave as configured (Module BASE).

  • Page 117: Sensor Calibration

    Calibrating the sensors Calibration (Memosens COND) Calibrating the sensors Sensor calibration Since the cell constant is subject to production-related variances, the dismount- ed sensor should be calibrated with a calibration solution (e.g. NaCl saturated). The cell constant of the sensor – particularly of a fringe-field sensor – depends on the type of installation: •...

  • Page 118: Memosens Cond Maintenance

    Memosens COND Maintenance Sensor monitor / Temp probe adjustment Note: HOLD mode active Menu Display Maintenance 0.245 mS/cm From the measuring mode: 25.6°C Press menu key to select menu. Menu selection Select maintenance using arrow keys, confirm by pressing enter. Passcode 2958 (To change passcode: Select: [enter]...

  • Page 119: Memosens Cond Diagnostics

    Memosens COND Diagnostics Sensor monitor Menu Display Sensor monitor 0.245 mS/cm Opening the diagnostics menu 25.6°C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter. Select: [enter] Then select Memosens COND. Return to meas Lingua The Diagnostics menu gives an over-...

  • Page 120: Cal Record

    Diagnostics (Memosens COND) Cal record Menu Display Cal record Cal record 0.245 mS/cm 25.6°C Data of last calibration, suitable for Cal record Active adjustment 06/09/10 14:06 documentation to ISO 9000 and GLP SE604-MS Sensor model Serial number 0077123 Cal mode Product cal Cell constant 0.029...

  • Page 121: Condi Parameter Setting

    Sensor identified Without any further parameter setting, mea- Sensor: SE 670 surement starts at once, the measuring temper- Manufacturer: Knick Serial number: 0000343 ature is simultaneously detected (see also: TICK Adjustment: 05/24/10 11:07 procedure, next page).
  • Page 122 Parameter Setting (CONDI) Note: HOLD mode active Menu Display Display Parameter selection Sensor data 0.245 mS/cm 20.1 °C The SE 670 digital sensor automatically CONDI sensor (Administrator) provides the required parameters. Input filter Sensor data Sensocheck monitors the cell factor Cal preset values for deviation.
  • Page 123 Parameter Setting (CONDI) Parameter Default Selection / Range Input filter Pulse suppression On, Off Sensor data Sensoface On, Off Sensor monitoring details • Cell factor Auto 09900 ... 3.9600 /cm • Sensocheck • CIP counter • SIP counter • Sensor operating time Temperature detection Meas.
  • Page 124 Concentration Curves (CONDI) Sulfuric acid H c [% by wt] Nitric acid HNO c [% by wt]...
  • Page 125 Concentration Curves (CONDI) Hydrochloric acid HCl c [% by wt] Sodium hydroxide solution NaOH c [% by wt]...
  • Page 126 Concentration Curves (CONDI) Table salt solution NaCl c [% by wt] Oleum [mS/cm] c [% by wt]...

  • Page 127: Concentration Table (Condi)

    Concentration Table (CONDI) Select menu: Parameter setting/System control/Concentration table Specifying a concentration solution for conductivity measurement Concentration Table To specify the customer-specific solution, 5 concentration values A-E are entered in a matrix together with 5 temperature values 1-5. To do so, first enter the 5 temperature values, then enter the respective conductivity values for each concentration A-E.

  • Page 129: Condi Calibration / Adjustment

    Calibration and adjustment CONDI Calibration / Adjustment Note: HOLD mode active for the currently calibrated module Current outputs and relay contacts behave as configured With Memosens sensors, the calibration data are stored in the sensor. This allows using precalibrated sensors. When the Protos is used for precalibrating sensors in the lab, you can use the calibration routines described below.
  • Page 130 Adjustment Adjustment (CONDI) Adjustment means that the cell factor determined by a calibration is taken over. It is entered in the calibration record. (Cal record can be called in the Diagnostics menu for the CONDI sensor.) The value is only effective for calculat- ing the measured variables when the calibration has been terminated with an adjustment.

  • Page 131: Temperature Compensation

    Temperature compensation Calibration / Adjustment (CONDI) Temperature compensation Temperature compensation during calibration The conductivity value of the calibration solution is temperature-dependent. For calibration, the calibration solution temperature must therefore be known in order to choose the actual value from the conductivity table. Automatic temperature compensation For automatic cal temp detection, the Protos 0.249 mS/cm...

  • Page 132: Hold Function During Calibration

    Calibration method HOLD Function During Calibration Behavior of the signal and relay outputs during calibration Measuring Calibration K2 contact Module A Selecting the "HOLD" is Module B measuring module active The current output of Module A Module B the selected Calibration Calibration module...
  • Page 133 Menu Display Selecting a calibration method Open Calibration 0.020 mS/cm 25.6°C Press menu key to select menu. Menu selection Select calibration using arrow keys, press enter to confirm, passcode 1147 (The passcode can be edited by the administrator.) Select: [enter] Return to meas Lingua 0.020 mS/cm...

  • Page 134: Automatic Calibration With Standard Calibration Solution

    Automatic calibration Calibration / Adjustment (CONDI) Automatic calibration with standard calibration solution Automatic with standard cal solution For automatic calibration, the conductivity sensor is immersed in a standard calibration solution (NaCl or KCl, selected during parameter setting: From the measured conductance and temperature, the Protos automatically calculates the cell factor.
  • Page 135 Menu Display Automatic calibration 0250 mS/cm Select calibration menu 025.0 °C Select “CONDI sensor” CONDI sensor Automatic with standard cal solution Select calibration method: Manual entry of cal solution "Automatic with standard cal solution", Product calibration Data entry - premeasured sensor confirm by pressing enter.

  • Page 136: Manual Entry Of Cal Solution

    Manual entry of cal solution Calibration / Adjustment (CONDI) Manual entry of cal solution Manual entry of cal solution For calibration with manual entry of the calibration solution’s conductivity, the sensor is immersed in a calibration solution. Protos determines a conductivity/ calibration temperature value pair.
  • Page 137 Menu Display Manual entry of cal solution 0.020 mS/cm Select calibration menu 025.0 °C Select CONDI sensor CONDI sensor Automatic with standard cal solution Select calibration method: Manual entry of cal solution “Manual entry of cal solution”, Product calibration Data entry - premeasured sensor confirm by pressing enter.

  • Page 138: Product Calibration

    Product calibration Calibration / Adjustment (CONDI) Product calibration Product calibration When the sensor cannot be removed, e.g. for sterility reasons (in biotechnical processes), its cell factor can be determined with “sampling”. To do so, the currently measured process value is stored by the Protos. Immediately afterwards, you take a sample from the process.
  • Page 139 Menu Display Product calibration 0.249 mS/cm Select calibration menu 25.0 °C Select CONDI sensor CONDI sensor Automatic with standard cal solution Select calibration method: Manual entry of cal solution "Product calibration", Product calibration Data entry - premeasured sensor confirm by pressing enter. Zero correction The module is in HOLD mode.

  • Page 140: Data Entry Of Premeasured Sensors

    Data entry of premeasured sensors Calibration / Adjustment (CONDI) Data entry of premeasured sensors Data entry of premeasured sensors Entry of cell factor and zero point of a sensor, related to 25°C, 1013 mbar. During calibration the module is in HOLD mode. Current outputs and relay contacts of the module behave as configured (Module BASE).

  • Page 141: Zero Correction (Condi)

    Calibrating the sensors Zero Correction (CONDI) Menu Display Zero correction Select: CONDI sensor 0.225 mS/cm 25.0°C During calibration, the output currents Calibration Module OXY 3400-062 (1 and 2), limit contacts, and controller CONDI sensor output are in HOLD mode. Module PH 3400-032 Press enter to confirm.

  • Page 142: Condi Maintenance

    CONDI Maintenance Sensor monitor / Temp probe adjustment Note: HOLD mode active Menu Display Maintenance From the measuring mode: 0.245 mS/cm 25.6°C Press menu key to select menu. Menu selection Select maintenance using arrow keys, confirm by pressing enter. Passcode 2958 (To change passcode: Select: [enter] Parameter setting/System control/...

  • Page 143: Condi Diagnostics

    CONDI Diagnostics Sensor monitor Menu Display Sensor monitor 0.245 mS/cm Opening the diagnostics menu 25.6°C From the measuring mode: Menu selection Press menu key to select menu. Select diagnostics using arrow keys, confirm by pressing enter. Select: [enter] Then select CONDI sensor. Return to meas Lingua The Diagnostics menu gives an over-...

  • Page 144: Cal Record

    Diagnostics (CONDI) Cal record Menu Display Cal record Cal record 0.245 mS/cm 25.6°C Data of last calibration, suitable for Cal record Active adjustment 06/09/10 14:06 documentation to ISO 9000 and GLP SE670 Sensor model Serial number 0077123 Cal mode Prod. cal. Cell factor S/No transmitter 00013425...

  • Page 145: Calculation Blocks (For All Process Variables)

    Calculation Blocks Calculation Blocks (for all Process Variables) Select menu: Parameter setting/System control/Calculation Blocks Calculation of new variables from measured variables Calculation Blocks Two measuring modules with all their measured values serve as input for the calculation block. In addition, the general device status (NAMUR signals) is taken into account.
  • Page 146 Calculation Blocks (for all process variables) Select menu: Parameter setting/System control/Calculation Blocks Combining measuring modules to Calculation Blocks Combining measuring modules With three measuring modules the following Calculation Block combinations are possible: Up to two Calculation Blocks can be activated. All current outputs can be set to output the new process variables formed by the Calculation Blocks.

  • Page 147: Logbook

    Logbook Factory setting Parameter Setting, General Parameter setting/System control/Logbook Note: HOLD mode Menu Display Logbook, factory setting 83.1 % Air Logbook 25.6 °C Select which messages are to be Logbook (Administrator) logged in the logbook. Log failure Log warning The last 50 events are recorded with Erase logbook date and time.

  • Page 148: Configuring A Current Output

    BASE module Current outputs Current Outputs, Contacts, OK Inputs Select menu: Parameter setting/Module BASE Note: HOLD mode (Setting: BASE module) Menu Display Parameter setting BASE module 85 % Air Configuring a Current Output 19.2°C • Open parameter setting Module BASE (Administrator) •...

  • Page 149: Current Outputs: Characteristics

    Current Outputs: Characteristics Select menu: Parameter setting/Module BASE • Linear characteristic The process variable is represented by a linear output current curve. Output current Process variable Start • Trilinear characteristic Two additional vertices must be entered: Output current 2nd vertex Y 1st vertex Y Process variable Start...
  • Page 150 • Function characteristic Nonlinear output current characteristic: allows measurements over several decades, e.g. measuring very low values with a high resolution and high values with a low resolution. Required: Entering a value for 50 % output current. Output current Entry for “50 % point”: e.g.: 10 % of measured value Process variable...

  • Page 151: Output Filter

    Output Filter Time interval Time averaging filter To smoothen the current output, a low-pass filter with adjustable time interval can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached. The time interval can be set from 0 to 120 sec.

  • Page 152: Namur Signals: Current Outputs

    Current outputs: Behavior during messages NAMUR Signals: Current Outputs Behavior during messages: HOLD, 22mA signal Behavior during messages Depending on the configuration (“Messages”) 83.1 % Air 19.0°C the current outputs switch to: Behavior during messages • Currently measured value HOLD Current meas.

  • Page 153: Namur Signals: Relay Contacts

    NAMUR Signals: Relay Contacts Failure, maintenance request, HOLD (function check) As delivered, the floating relay outputs of the BASE module are assigned to the NAMUR signals: Failure Contact K4, normally closed (signaling current failure) Maintenance request Contact K3, normally open contact HOLD Contact K2, normally open contact NAMUR signals: Factory setting of contacts...

  • Page 154: Relay Contacts: Protective Wiring

    Relay Contacts: Protective Wiring Protective wiring of relay contacts Relay contacts are subject to electrical erosion. Especially with inductive and capacitive loads, the service life of the contacts will be reduced. For suppres- sion of sparks and arcing, components such as RC combinations, nonlinear resistors, series resistors and diodes should be used.

  • Page 155: Relay Contacts, Usage

    Relay contacts Relay Contacts Parameter setting/Module BASE/Relay contacts Menu Display Setting the relay contacts 7.00pH Relay Contacts, Usage 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance! Variable NAMUR HOLD • Select “Module BASE” Limit Limit •...

  • Page 156: Relay Contacts: Sensoface Messages

    Relay Contacts: Sensoface Messages Parameter setting/Module BASE/Relay contacts/Usage/Sensoface Menu Display Parameter setting (Sensoface) 7.00 pH Assigning Sensoface Messages to 19.0°C Relay Contacts Module BASE (Administrator) Output current I1 When more than one measuring Output current I2 module is used, the Sensoface mes- (NAMUR Failure) Contact K4 Contact K3...

  • Page 157: Rinse Contact

    Rinse contact Rinse Contact Parameter setting/Module BASE/Relay contacts/Usage/Rinse contact Menu Display Configuring the rinse contact 7.00 pH Relay Contacts, Usage 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance! Variable NAMUR HOLD • Select “Module BASE” Limit Limit •...

  • Page 158: Icons In The Measurement Display

    Limit Limit Value, Hysteresis, Contact Type Parameter setting/Module BASE/Relay contacts/Usage Menu Display Usage as limit value 7.00 pH Relay output: Limit 19.2°C • Open parameter setting Contact K1 (Administrator) • Enter passcode Usage NAMUR maintenance! Variable NAMUR HOLD • Select “Module BASE” Limit Limit •...

  • Page 159: Ok1, Ok2 Inputs: Specifying The Level

    OK1, OK2 Inputs: Specifying the Level Parameter setting/Module BASE/Inputs OK1, OK2 Note: HOLD mode (Setting: BASE module) Menu Display Setting the OK inputs 83.1 % Air OK1 Usage 19.2°C • Open parameter setting Inputs OK1, OK2 (Administrator) • Enter passcode For OK2 usage see “Function control matrix”...

  • Page 160: Selecting Parameter Set (A, B) Via Ok2 Input

    Switching Parameter Sets via OK2 Parameter setting / System control / Function control matrix Note: HOLD mode (Setting: BASE module) Parameter Sets 2 complete parameter sets (A, B) can be stored in the analyzer. You can switch between the parameter sets using the OK2 input. The currently activated set can be signaled by a relay contact.

  • Page 161: Specifications

    Switching voltage 0 ... 2 V (AC/DC) No flow 10 ... 30 V (AC/DC) Flow okay Explosion protection See www.knick.de (MS 3400X-160) NAMUR NE 21 and EN 61326-1 EN 61326-2-3 Emitted interference Class B (residential area) Immunity to interference...
  • Page 162 Specifications Data retention Parameters > 10 years Nominal operating conditions Ambient temperature -20 ... +55 °C Transport/Storage temp -20 ... +70 °C Relative humidity 10 ... 95% not condensing Power supply (KBUS) 6.8 … 8.0 V / 20 mA...

  • Page 163: Index

    Index Protos MS 3400(X)-160 Module Activating the cal tolerance band (PH) 32 Adaptive calibration timer (PH) 54 Additional function, activation 70 Adjusting the temp probe (COND) 118 Adjusting the temp probe (CONDI) 142 Adjusting the temp probe (ORP) 64 Adjusting the temp probe (PH) 50 Adjustment (CONDI) 130 Adjustment (Memosens COND) 106 Adjustment (Memosens ORP) 62...
  • Page 164 Index Protos MS 3400(X)-160 Module Calibration by entering data from premeasured sensors (PH) 48 Calibration by sampling (OXY) 84 Calibration (CONDI) 129 Calibration (Memosens COND) 105 Calibration (Memosens ORP) 62 Calibration (Memosens OXY) 75 Calibration (Memosens PH) 36 Calibration methods (PH) 38 Calibration, preset values (COND) 93 Calibration, preset values (CONDI) 123 Calibration, preset values (ORP) 59...
  • Page 165 Index Protos MS 3400(X)-160 Module Connecting cable 17 Contacts 148 Contact type 158 Current outputs 148 Current outputs: characteristics 149 Data entry of premeasured sensors 86 Data entry of premeasured sensors (COND) 116 Data entry of premeasured sensors (CONDI) 140 Data entry of premeasured sensors (PH) 48 Delta function (ORP) 60 Delta function (PH) 34...
  • Page 166 Index Protos MS 3400(X)-160 Module Gasket, FRONT module 14 Generating messages (measuring module) (ORP) 61 Generating messages (measuring module) (OXY) 74 Generating messages (measuring module) (PH) 35 Graphic display 12 Hardware and software version 10 Hazardous locations 8 HOLD mode 153 Hydrochloric acid (COND) 95 Hydrochloric acid (CONDI) 125 Hysteresis 158...
  • Page 167 Index Protos MS 3400(X)-160 Module Manual entry of buffer values 44 Manual entry of cal solution (COND) 112 Manual entry of cal solution (CONDI) 136 Measurement display 20 Memory card 14 Memosens cable 17 Memosens COND 91 Memosens ORP 57 Memosens OXY (TAN required) 69 Memosens PH 29 Memosens PH/ORP, parameter setting 55...
  • Page 168 Index Protos MS 3400(X)-160 Module Oleum (COND) 96 Oleum (CONDI) 126 One-point calibration (COND) 105 One-point calibration (CONDI) 129 One-point calibration (OXY) 75 One-point calibration (PH) 38 Operating levels 18 Operating modes 28 Operator level 18 Option release SW 3400-005 32 Option release SW 3400-015/016 70 ORP calbration/adjustment 62 ORP configuration, ranges and presettings 59...
  • Page 169 Index Protos MS 3400(X)-160 Module Reduced limit (USP) 98 Relay contacts: protective wiring 154 Relay contacts, usage 155 Relay output: limit value 158 Release (softkey function) 19 Replacing the front module 14 Return of products under warranty 2 Rinse contact 157 Safety information 8 Salinity correction (OXY) 73 Salt solution (COND) 96...
  • Page 170 Index Protos MS 3400(X)-160 Module Sensor monitoring details (OXY) 72 Sensor monitoring details (PH) 30 Sensor monitor, maintenance (COND) 118 Sensor monitor, maintenance (CONDI) 142 Sensor monitor, maintenance (ORP) 64 Sensor monitor, maintenance (OXY) 88 Sensor monitor, maintenance (PH) 50 Sensor network diagram (OXY) 90 Sensor network diagram (PH) 53 Sensor wear monitor (OXY) 90...
  • Page 171 Index Protos MS 3400(X)-160 Module Temp probe adjustment 88 Terminal compartment 15 Terminal plate 16 Terminal plates of “hidden” modules 14 Three-point calibration (PH) 38 Tolerance adjustment (menu) (PH) 31 Tolerance adjustment (PH) 54 Trademarks 2 Two-point calibration (PH) 38 USP function 98 Viewing level 18 Wiring 17...
  • Page 172 091986 TA-201.160-KNE03 20170731 Software version 2.x...

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