Knick Stratos Pro A4 MSOXY Instruction Manual
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Knick Stratos Pro A4 MSOXY Instruction Manual

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Stratos®Pro
A4... MSPH/MSOXY
Instruction Manual
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Summary of Contents for Knick Stratos Pro A4 MSOXY

  • Page 1 Stratos®Pro A4... MSPH/MSOXY Instruction Manual Latest Product Information: www.knick.de...
  • Page 2 Warranty Warranty Defects occurring within 3 years from delivery date shall be remedied free of charge at our plant (carriage and insurance paid by sender). Sensors, fittings, and accessories: 1 year. Subject to change without notice. Return of Products Under Warranty Please contact our Service Team before returning a defective device.

  • Page 3: Documents Supplied

    Dutch. Быстрый старт ......39 Inicio rápido ........ 51 More languages on CD-ROM and Início rápido ........ 63 Guida rapida ........ 75 on our website: www.knick.de Snabbstart........87 QuickStart ........99 • Installation and commissioning www.knick.de Other languages: • Operation •...

  • Page 4: Table Of Contents

    Contents Documents Supplied ..............3 Introduction ..................7 Intended Use ..................7 Safety Information ................. 8 Overview of Stratos Pro A4... MSPH/MSOXY ......9 Assembly ..................10 Package Contents ................10 Mounting Plan, Dimensions ............11 Pipe Mounting, Protective Hood ..........12 Panel Mounting ..................13 Installation ..................14 Installation Instructions ..............14 Rating Plates / Terminal Assignments ........14...
  • Page 5 Contents Measuring Mode ................50 Current Output 1 ................52 Current Output 2 ................58 Alarm Settings ..................60 Limit Function ..................62 Pulse Length / Pulse Frequency Controller ......71 Controller .....................72 WASH Contact ..................76 Time and Date ..................78 Tag Number ....................78 PH Calibration ................80 Pre-Calibrating Memosens Sensors ..........80 Selecting a Calibration Mode ............81 Zero Adjustment (ISFET) ..............82...
  • Page 6 Contents Error Handling ................121 Error Messages ................122 Sensoface ..................125 FDA 21 CFR Part 11 ..............128 Electronic Signature – Passcodes ..........128 Audit Trail ....................128 Index .....................129 Trademarks ..................139 Passcodes ..................140...

  • Page 7: Introduction

    Introduction Intended Use Stratos Pro A4... MSPH/MSOXY is a two-channel process unit for mea- suring pH and dissolved oxygen and temperature using 2 Memosens sensors. It is used for biotechnology applications, in the pharma- ceutical industry, as well as in the field of industry, environment, food processing and sewage treatment.

  • Page 8: Safety Information

    Safety Information Safety information Be sure to read and observe the following instructions! The device has been manufactured using state of the art technology and it complies with applicable safety regulations. When operating the device, certain conditions may nevertheless lead to danger for the operator or damage to the device.

  • Page 9: Overview Of Stratos Pro A4

    Overview Overview of Stratos Pro A4... MSPH/MSOXY Power supply Sensor A Output 1 (pH) RS 485 A RS 485 B Output 2 GND/Shield Power supply Sensor B "MK-MS" RS 485 A module (OXY) RS 485 B Shield Alarm Current input Wash HOLD input...

  • Page 10: Assembly

    Assembly Package Contents Check the shipment for transport damage and completeness! The package should contain: • Front unit, rear unit, bag containing small parts • Specific test report • Documentation (cf Pg 3) • CD-ROM Fig.: Assembling the enclosure 1) Jumper (3 x) 6) Sealing insert (1 x) 2) Washer (1 x), for conduit 7) Rubber reducer (1 x)

  • Page 11: Mounting Plan, Dimensions

    Assembly Mounting Plan, Dimensions 1) Cable gland (3 x) 2) Knockouts for cable gland or ½" conduit, 21.5 mm dia. (2 knockouts) Conduits not included! 3) Knockout for pipe mounting (4 x) 4) Knockout for wall mounting (2 x) Fig.: Mounting plan (All dimensions in mm!)

  • Page 12: Pipe Mounting, Protective Hood

    Assembly Pipe Mounting, Protective Hood ø40...ø60 1) Hose clamp with worm gear drive to DIN 3017 (2 x) 2) Pipe-mount plate (1 x) 3) For vertical or horizontal posts or pipes 4) Self-tapping screw (4 x) Fig.: ZU 0274 pipe-mount kit (All dimensions in mm!) Fig.: ZU 0737 protective hood for wall and pipe mounting (All dimensions in mm!)

  • Page 13: Panel Mounting

    Assembly Panel Mounting <30 1) Circumferential sealing (1 x) 2) Screw (4 x) 3) Position of control panel 4) Span piece (4 x) 5) Threaded sleeve (4 x) Cutout 138 x 138 mm (DIN 43700) 1...22 Fig.: ZU 0738 panel-mount kit (All dimensions in mm!)

  • Page 14: Installation

    Installation Installation Instructions • Installation of the device must be carried out by trained experts in accordance with this instruction manual and as per applicable local and national codes. • Be sure to observe the technical specifications and input ratings during installation! •...

  • Page 15: Power Supply, Signal Lines

    Power Supply, Signal Lines Connect the power supply for Stratos Pro A4.. MSPH/MSOXY to terminals 21 and 22 (24 ... 230 V AC, 45 ... 65 Hz / 24 ... 80 V DC) Areas for placing the Assignments screwdriver to pull out the terminals Fig.: Terminals, device opened, back of front unit...

  • Page 16: Connecting Sensors A And B

    Connecting Sensors A and B Connect the sensor lines with the corresponding sensor terminals. Sensor B (Oxy) connections Areas for placing the screwdriver to pull out the terminals Sensor A (pH) connections Fig.: Terminals, device opened, back of front unit...
  • Page 17 Memosens Cable CA/MS-... Intended Use Connecting cable for contactless inductive digital transmission of measured signals (Memosens®). The connecting cable consists of an inductive connector for digital Memosens® sensors (bayonet lock). It allows connecting the ferrule- terminated wires from the sensor loop of the transmitter. Contactless inductive digital transmission of signals and energy eliminates the influence of humidity, electromagnetic fields and corrosion.

  • Page 19: Connecting A Memosens Sensor

    Connecting a Memosens Sensor Example: Measuring task: pH, temp and DO, temp Sensors (example): SE532/1-NMSN, SE706 Memosens (both Knick) Cable CA/MS-003-NAA Terminal row 1 Module terminal Channel B / Oxy Channel A / pH...

  • Page 20: User Interface, Keypad

    User Interface, Keypad MEMO SENS 1 IrDA transmitter/receiver 2 Display 3 Keypad 4 Rating plate (enclosure bottom) Function meas • Return to last menu level • Directly to measuring mode (press > 2 s) info • Retrieve information • Show error messages enter •...

  • Page 21: Display

    Display SENS MEMO 1 Temperature 13 Info available 2 Sensocheck 14 Hold mode active 3 Interval/response time 15 Main display 4 Sensor data 16 Secondary display 17 Proceed using enter 5 Sensor worn out 6 Limit values 18 Not used 7 Alarm 19 Diagnostics 8 Service...

  • Page 22: Measuring Mode

    Measuring Mode After the operating voltage has been connected, the analyzer automatically goes to “Measuring“ mode. To call the measuring mode from another operating mode (e.g. Diagnostics, Service): Hold meas key depressed (> 2 s). Sensoface indicator (sensor status) Time Process variable (pH) Mode indicator...

  • Page 23: Selecting The Mode / Entering Values

    Selecting the Mode / Entering Values To select the operating mode: 1) Hold meas key depressed (> 2 s) (measuring mode) 2) Press any arrow key: the selection menu appears 3) Select operating mode using left / right arrow key 4) Press enter to confirm the selected mode Selection menu Selected mode...

  • Page 24: Operating Modes

    Operating Modes Diagnostics Display of calibration data, display of sensor data, performing a device self-test, viewing the logbook entries, display of hardware/software versions of the individual components. The logbook can store 100 events (00...99). They can be displayed directly on the device. The logbook can be extended to 200 entries using a TAN (Option).

  • Page 25: Menu Structure Of Modes And Functions

    Menu Structure of Modes and Functions meas meas meas meas Further displays TAG display CLK display Measuring (if configured) after 60 s after 60 s mode Pressing any arrow key opens the selection menu. Select the menu group using the left/right arrow keys. Pressing enter opens a menu item.

  • Page 26: Hold Mode

    HOLD Mode The HOLD mode is a safety state during configuration and calibration. Output current is frozen (Last) or set to a fixed value (Fix). Alarm and limit contacts are inactive. The HOLD mode is indicated by orange display backlighting. HOLD mode, display icon: Output signal response •...

  • Page 27: Alarm

    Alarm External activation of HOLD (SW-A005) The HOLD mode can be activated from outside by sending a signal to the Hold input (e.g. from the process control system). Power supply HOLD 12...24 V AC/DC input Stratos Pro A4... Process control system HOLD inactive 0...2 V AC/DC HOLD active...

  • Page 28: Overview Of Configuration

    Overview of Configuration The configuration steps are assigned to different menu groups. Using  and  you can jump between the individual menu groups. Each menu group contains menu items for setting the parameters. Pressing enter opens a menu item. The values are edited using  and .

  • Page 29: Setup And Channel Selection On The Device

    Setup and Channel Selection on the Device pH and Oxy measuring point (example) Analyzer Stratos Pro A4... MSPH/MSOXY Connection via Memosens cable Length max. 100 m pH measuring Oxy measuring point: point: PH sensor OXY sensor with fitting with fitting Channel Selection and Display Assignment Display DISPLAY:...
  • Page 30 Configuration Configuration Choices Default PH sensor MEAS MODE ON / OFF CALMODE AUTO AUTO AUTO BUFFER SET -00- ... -09-, -U1- -00- Please note: Pressing info displays nominal values and type of buffer set EDIT BUFFER 1 (NO, YES) NO (For specifiable Enter values for buffer 1 buffer set,...
  • Page 31 Configuration Configuration Choices Default OXY sensor OXY: MEAS MODE dO % dO % dO mg/l dO ppm GAS % CALMODE CAL AIR CAL AIR CAL WTR CAL TIMER OFF, FIX, ADAPT CAL CYCLE 0 ... 9999 h 0168 SALINITY 00.00 ... 45.00 ppt 00.00 ppt PRESSURE UNIT BAR / KPA / PSI...
  • Page 32 Configuration Configuration Choices Default MEAS MODE MES: TEMP UNIT °C / °F °C Output 1 (OUT1) / Output 2 (OUT2) identical, with OXY % as default OT1: RANGE 0–20 mA, 4–20 mA 4-20 mA CHANNEL BEGIN 4 mA (0 mA) –2.00...16 PH 00.00 PH END 20 mA –2.00...16 PH...
  • Page 33 Configuration Configuration Choices Default Alarm (ALARM) ALA: DELAYTIME 0...600 SEC 0010 SEC SENSOCHECK ON/OFF CONTROL IN ON/OFF Relay 1/2 (RL1/RL2) REL: (Selected in text line) LIMITS, CONTROLLER LIMITS RL1: CHANNEL PH / mV / TMP A / OXY / TMP B FUNCTION Lo LEVL, Hi LEVL Lo LEVL...
  • Page 34 Configuration Configuration Choices Default Relay 1/2 (RL1/RL2) -continued- REL: CHANNEL PH / mV / TMP A / OXY / TMP B TYPE PLC/PFC PULSE LEN 0...0600 SEC 0010 SEC PULSE FREQ 0...0180 P/M 0060 P/M SETPOINT –2.00...16 PH 07.00 PH DEAD BAND 0...10.00 PH 01.00 PH...

  • Page 35: Configuration (Original For Copy)

    Configuration (Original for Copy) Please note: Fill in your configuration data on the following pages or use them as original for copy. Parameter PH: Sensor on/off PH: Calibration mode PH: Buffer set selection PH: Calibration timer PH: Calibration cycle PH: TC-LIQUID PH: CIP counter PH: SIP counter OXY: Sensor on/off...
  • Page 36 (Original for Copy) Configuration Parameter OT2: Current range OT2: Channel (process variable) OT2: Current start OT2: Current end OT2: Filter time OT2: 22 mA error current OT2: HOLD mode OT2: HOLD-FIX current ALA: Delay ALA: Sensocheck on/off ALA: "Control" input REL: Usage RL1: Channel (process variable)
  • Page 37 Configuration (Original for Copy) Parameter CTR: Setpoint CTR: Neutral zone CTR: P gain CTR: I time CTR: D time CTR: HOLD mode WSH: Wash cycle WSH: Wash duration WSH: Contact response CLK: Time format CLK: Time hh/mm CLK: Day/month CLK: Year TAG: Tag number...
  • Page 38 Configuration PH Sensor Selecting pH sensor, calibration mode 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_PH menu using  keys, press enter, then select "MEAS_MODE = ON“. MEMO SENS Confirm by pressing enter. 4 All items of this menu group are indicated by the “PH:”...

  • Page 39: Calibration Mode

    Configuration Menu item Action Choices Select sensor SENSOR_PH Select sensor using  SENSOR_OXY keys. MEMO SENS Press enter to confirm. Measuring channel Press enter to select "ON". ON / OFF Switch to "OFF" if you do MEMO SENS not want to use this chan- nel for measuring or if a sensor is not connected.
  • Page 40 Configuration PH Sensor Selecting cal timer, cal cycle 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_PH menu using  keys, press enter, then select "MEAS_MODE = ON“. MEMO SENS Confirm by pressing enter. 4 All items of this menu group are indicated by the “PH:”...
  • Page 41 Configuration Menu item Action Choices Calibration timer OFF/ADAPT/FIX Adjust CALTIMER using  keys: OFF: No timer With ADAPT, the calibra- MEMO SENS ADAPT: Maximum cal tion cycle is automatically cycle (adjust in the next reduced depending on step) the sensor load (high FIX: Fixed cal cycle temperatures and pH (adjust in the next step)
  • Page 42 Configuration PH Sensor Adjusting CIP cleaning cycles, SIP sterilization cycles 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_PH menu using  keys, press enter, then select "MEAS_MODE = ON“. MEMO SENS Confirm by pressing enter. 4 All items of this menu group are indicated by the “PH:”...
  • Page 43 Configuration Menu item Action Choices TC-LIQUID / CIP / SIP Temp compensation, For pH measurement only: Enter temperature process medium compensation of the process medium. Enter value using  keys. Press enter to confirm. Cleaning cycles Select ON or OFF using ON/OFF ...

  • Page 44: Oxy Sensor

    Configuration OXY Sensor Selecting sensor type, measuring mode, calibration medium, calibration timer 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_OXY menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OXY:”...
  • Page 45 Configuration Menu item Action Choices Select measuring dO %, Select measuring mode using  keys. dO mg/l mode dO ppm MEMO SENS Measurement in liquids GAS % GAS: Measurement in gases Press enter to confirm. Calibration medium: CAL_AIR Select calibration medium using ...
  • Page 46 Configuration OXY Sensor Selecting salinity, pressure unit, pressure correction 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_OXY menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OXY:”...
  • Page 47 Configuration Menu item Action Choices Enter salinity Enter salinity of the 00.00...45.00 ppt process medium. Enter value using  MEMO SENS  keys. Press enter to confirm. Enter pressure unit Bar/kPa/PSI Select desired pressure unit using  keys. Then, select manual MEMO SENS MAN / EXT...
  • Page 48 Configuration OXY Sensor Adjusting CIP cleaning cycles, SIP sterilization cycles 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select SENSOR_OXY menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OXY:”...
  • Page 49 Configuration Menu item Action Choices CIP / SIP Cleaning cycles Select ON or OFF using ON/OFF  keys. on/off Activates/deactivates log- ging in extended logbook MEMO SENS Press enter to confirm. Sterilization cycles Select ON or OFF using ON/OFF  keys. on/off Activates/deactivates log- ging in extended logbook...

  • Page 50: Measuring Mode

    Configuration Measuring Mode Specifying the temperature unit 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select MEAS_MODE menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “MES:”...
  • Page 51 Configuration Menu item Action Choices Temperature unit °C / °F Select °C or °F using  keys. MEMO SENS Press enter to confirm.

  • Page 52: Current Output 1

    Configuration Current Output 1 Selecting the output current range 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select OUT1 menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OT1:”...
  • Page 53 Configuration Menu item Action Choices Current range 4-20 mA / 0-20 mA Select 4-20 mA or 0-20 mA range using MEMO SENS  keys. Press enter to confirm. Process variable PH / mV / TMP A / Select using  OXY / TMP B/ keys: MEMO...
  • Page 54 Configuration Current Output 1 Adjusting time interval of output filter 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select OUT1 menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OT1:”...
  • Page 55 Configuration Menu item Action Choices Time averaging filter 0...120 SEC Enter value using  (0000 SEC)  keys. MEMO SENS Press enter to confirm. Time averaging filter To smoothen the current output, a low-pass filter with adjustable filter time constant can be switched on. When there is a jump at the input (100 %), the output level is at 63 % after the time interval has been reached.
  • Page 56 Configuration Current Output 1 Output current during Error and HOLD 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select OUT1 menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OT1:”...
  • Page 57 Configuration Menu item Action Choices Output current dur- Select ON or OFF using ON/OFF  keys. ing error message Press enter to confirm. MEMO SENS Output current LAST/FIX LAST: During HOLD the last measured value is during HOLD maintained at the output. FIX: During HOLD a value MEMO SENS...

  • Page 58: Current Output 2

    Configuration Current Output 2 Selecting the output current range 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select OUT2 menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “OT2:”...
  • Page 59 Configuration Menu item Action Choices Current range 4-20 mA / 0-20 mA Select 4-20 mA or 0-20 mA range using  keys. MEMO SENS Press enter to confirm. Process variable PH / mV / TMP A / Select using  keys: OXY / TMP B/ PH: pH value TMP: Temperature...

  • Page 60: Alarm Settings

    Configuration Alarm Settings Delay, Sensocheck, CONTROL input 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select ALARM menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “ALA:”...
  • Page 61 Configuration Menu item Action Choices Delay 0...600 SEC Enter value using  010 SEC)  keys. Press enter to confirm. MEMO SENS Sensocheck Select Sensocheck ON/OFF (continuous monitoring of sensor). MEMO SENS Select ON or OFF using  keys. Press enter to confirm. CONTROL input Activate CONTROL input ON/OFF...

  • Page 62: Limit Function

    Configuration Limit Function Relay 1 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select REL1/REL2 menu using  keys, press enter, then select LIMITS. 4 All items of this menu group are indicated by MEMO SENS the “RL1:”...
  • Page 63 Configuration Menu item Action Choices Use of relays LIMITS / CONTROLLER Select in the text line using  keys: • Limit function MEMO SENS (LIMITS) • Controller (CONTROLLER) Please note: Selecting CONTROLLER leads to Press enter to confirm. Controller menu group CTR. Select process Select desired process PH / mV / TMP A /...
  • Page 64 Configuration Limit Function Relay 1 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select REL1/REL2 menu using  keys, press enter, then select LIMITS. 4 All items of this menu group are indicated by MEMO SENS the “RL1:”...
  • Page 65 Configuration Menu item Action Choices Limit 1 hysteresis Select hysteresis using 0...10.00 PH (00.50 PH)   keys. MEMO SENS Press enter to confirm. Limit 1 delay The contact is activated 0...9999 SEC (0010 SEC) with delay (deactivated without delay) MEMO SENS Adjust delay using ...
  • Page 66 Configuration Limit Function Relay 2 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select REL1/REL2 menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “RL2:” code. Press enter to select menu, edit using arrow keys (see next page).
  • Page 67 Configuration Menu item Action Choices Select process PH / mV / TMP A / Select desired process variable using  keys. OXY / TMP B/ variable Press enter to confirm. (CHANNEL) Limit 2 Lo LEVL / Hi LEVL Select desired function using arrow keys.
  • Page 69 Controller Functions Typical Applications P controller Application for integrating control systems (e.g. closed tank, batch processes). PI controller Application for non-integrating control systems (e.g. drains). PID controller The additional derivative action compensates for measurement peaks. Controller Characteristic +100% Controller output Yp [%] Relay 1 Neutral zone Yp=0...
  • Page 70 Controller Functions Controller equations Controller output Y = P action I action D action with: Proportional action Reset time [s] Rate time [s] Controller gain [%] Proportional action Y PH constant 5 (for pH) 500 mV (for ORP) Setpoint - Meas. value OXY constant 50% (for %O or %Air)

  • Page 71: Pulse Length / Pulse Frequency Controller

    Controller Functions Pulse Length / Pulse Frequency Controller Pulse length controller (PLC) The pulse length controller is used to operate a valve as an actuator. It switches the contact on for a time that depends on the controller output. The period is constant. A minimum ON time of 0.5 sec is maintained even if the controller output takes corresponding values.

  • Page 72: Controller

    Configuration Controller (For description, see Controller Functions) Process variable, controller type, setpoint. 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select REL1/REL2 menu using  keys, press enter, then select CONTROLLER. 4 All items of this menu group are indicated by MEMO SENS the “CTR:”...
  • Page 73 Configuration Menu item Action Choices Select process PH / mV / TMP A / Select desired process variable using  OXY / TMP B/ variable keys. MEMO SENS Press enter to confirm. Controller type PLC/PFC Pulse length controller (PLC) or pulse frequency MEMO SENS controller (PFC)
  • Page 74 Configuration Controller (For description, see Controller Functions) Neutral zone. P, I, D actions. Behavior during HOLD 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select REL1/REL2 menu using  keys, press enter, then select CONTROLLER. 4 All items of this menu group are indicated by MEMO SENS...
  • Page 75 Configuration Menu item Action Choices Neutral zone Adjust neutral zone using   keys. 0...10.00 PH MEMO SENS (01.00 PH) / 0...2000 mV Press enter to confirm. OXY: 0 ... 50% full scale Controller: P action Adjust P action using 10...9999% ...

  • Page 76: Wash Contact

    Configuration WASH Contact Controlling a rinsing probe 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select WASH menu using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “WSH:”...
  • Page 77 Configuration Menu item Action Choices Cleaning interval 0.0...999.9 h (000.0 h) Adjust value using   keys. MEMO SENS Press enter to confirm. Cleaning duration 0...9999 SEC (0060 SEC) Adjust value using   keys. MEMO SENS Press enter to confirm. Contact type N/O / N/C N/O: normally open...

  • Page 78: Time And Date

    Configuration Time and Date Tag Number 1 Press any arrow key. 2 Select CONF using  keys, press enter. 3 Select CLOCK or TAG using  keys, press enter. 4 All items of this menu group are indicated by MEMO SENS the “CLK:”...
  • Page 79 Configuration Time and Date In measuring mode the time is shown in the lower display. In addition, the logbook entries (cf Diagnostics) are provided with a time stamp. Please note: • After prolonged power outage (> 5 days) the time display is replaced by dashes and cannot be used for processing.

  • Page 80: Ph Calibration

    PH Calibration Please note: • All calibration procedures must be performed by trained personnel. Incorrectly set parameters may go unnoticed, but change the measuring properties. • The response time of the sensor and temperature probe is considerably reduced when the sensor is first moved about in the buffer solution and then held still.

  • Page 81: Selecting A Calibration Mode

    Selecting a Calibration Mode Calibration is used to adapt the device to the individual sensor characteristics, namely asymmetry potential and slope. Access to calibration can be protected with a passcode (SERVICE menu). First, open the calibration menu and select the sensor (SENSOR_PH) and then the calibration mode: SENSOR_PH Calibrating the pH sensor CAL_PH...

  • Page 82: Zero Adjustment (Isfet)

    Zero adjustment Zero Adjustment (ISFET) This adjustment allows the use of ISFET Memosens sensors. The func- tion is available when an ISFET Memosens sensor is connected. The adjustment is made using a zero buffer (pH 7.00). Permitted range for buffer value: pH 6.5 ... 7.5. Maximum zero offset: ±750 mV Display Action...
  • Page 83 Zero Adjustment (ISFET) Display Action Remark At the end of the ad- This is not the final justment procedure calibration value of the zero offset [mV] of the sensor! the sensor is displayed Asymmetry poten- (based on 25 °C). tial and slope must Sensoface is active.

  • Page 84: Automatic Calibration (Calimatic)

    Adjustment (Calimatic) Automatic Calibration (Calimatic) The AUTO calibration mode must have been preset during configura- tion. Make sure that the buffer solutions used correspond to the con- figured buffer set. Other buffer solutions, even those with the same nominal values, may demonstrate a different temperature response. This leads to measurement errors.
  • Page 85 Automatic Calibration (Calimatic) Display Action Remark At the end of the stabil- Please note: ity check, the value will Stability check can be saved and the asym- be stopped after metry potential will be 10 sec (by pressing displayed. enter). However, this Calibration with the first reduces calibration buffer is terminated.

  • Page 86: Manual Calibration With Buffer Entry

    Manual Calibration with Buffer Entry The MAN calibration mode must have been preset during configura- tion. For calibration with manual buffer specification, you must enter the pH value of the buffer solution used in the device for the proper temperature. Any desired buffer solution can be used for calibration. Display Action Remark...
  • Page 87 Manual Calibration with Buffer Entry Display Action Remark At the end of the sta- Please note: bility check, the value Stability check can will be saved and the be stopped after asymmetry potential 10 sec (by pressing will be displayed. enter).

  • Page 88: Data Entry Of Premeasured Sensors

    Data Entry of Premeasured Sensors The DAT calibration mode must have been preset during configuration. You can directly enter the values for slope and asymmetry potential of a sensor. The values must be known. Display Action Remark Select Calibration. Press enter to proceed. “Data Input“...
  • Page 89 Converting Slope to mV Converting slope [%] to slope [mV/pH] at 25 °C mV/pH 46.2 47.4 48.5 49.7 50.9 52.1 53.3 54.5 55.6 56.8 58.0 100 59.2 102 60.4 Converting asymmetry potential to sensor zero point [mV] ZERO = 7 - = Sensor zero ZERO S [mV / pH]...

  • Page 90: Product Calibration (Ph)

    Product calibration Product Calibration (pH) Calibration by sampling (one-point calibration). During product calibration the sensor remains in the process. The measurement process is only interrupted briefly. Procedure: 1) The sample is measured in the lab or directly on the site using a portable meter.
  • Page 91 Product Calibration (pH) Display Action Remark The device returns to From the blinking measuring mode. CAL mode indicator you see that product calibration has not been terminated. Product calibration Display (3 sec) step 2  Now the device is in HOLD mode. The stored value is displayed (blinking) and can be overwritten with...

  • Page 93: Oxy Calibration

    OXY Calibration Calibration adapts the device to the individual sensor characteristics. It is always recommended to calibrate in air. Compared to water, air is a calibration medium which is easy to handle, stable, and thus safe. In the most cases, however, the sensor must be removed for a calibration in air.

  • Page 94: Selecting A Calibration Mode

    Selecting a Calibration Mode Calibration is used to adapt the device to the individual sensor characteristics, namely zero point and slope. Access to calibration can be protected with a passcode (SERVICE menu). First, you open the calibration menu and select the calibration mode: CAL_WTR / Calibration in water/air (as configured)
  • Page 95 Zero calibration Display Action Remark Select calibration, MEMO SENS press enter to proceed. Select Sensor_OXY, press enter to proceed. Select CAL ZERO, press enter to proceed. Ready for calibration. Display (3 sec) MEMO SENS Hourglass blinks. Now the device is in Place sensor in oxygen- HOLD mode.

  • Page 96: Product Calibration

    Product calibration Product Calibration Calibration with Sampling During product calibration the sensor remains in the process. The measurement process is only interrupted briefly. Procedure: During sampling the currently measured value is stored in the device. The device immediately returns to measuring mode. The cal mode indicator blinks and reminds you that calibration has not been terminated.
  • Page 97 Product calibration Display Action Remark The device returns to From the blinking MEMO SENS measuring mode. CAL mode indicator you see that product calibration has not been terminated. Product calibration Display (3 sec) MEMO SENS step 2: Now the device is in When the sample value HOLD mode.

  • Page 98: Slope Calibration (Medium: Water)

    Slope Calibration (Medium: Water) (air-saturated) Display Action Remark Select calibration “Medium water“ MEMO SENS (SLOPE). Immerse or “Medium air“ sensor in cal medium, is selected in the press enter to start. configuration. Default: 1000 bars Enter cal pressure MEMO SENS Unit bar/kpa/PSI Press enter to proceed.

  • Page 99: Slope Calibration (Medium: Air)

    Slope Calibration (Medium: Air) Display Action Remark Select calibration. “Medium water“ MEMO SENS Place sensor in air, or “Medium air“ press enter to start. is selected in the Device goes to HOLD configuration. mode. Enter relative humidity Default for relative MEMO SENS using arrow keys...

  • Page 100: Measurement

    Measurement Display Remark From the configuration or calibration menus, you can switch the device to measuring mode by pressing the meas key. In the measuring mode the main display shows the configured process variable, the secondary display shows the time and the second configured process variable.
  • Page 101 Measurement Display Remark With activated controller you can also step through the following displays by pressing the meas key. When no key has been pressed for 60 sec, the device returns to the standard display. Main display: Controller output Y Secondary display: Setpoint Depending on configuration setting: pH, mV, or temperature.

  • Page 102: Diagnostics

    Diagnostics (DIAG) Diagnostics In the Diagnostics mode you can access the following menus without interrupting the measurement: Viewing PH sensor data Viewing OXY sensor data Starting a device self-test Viewing the logbook entries Displaying currently measured values Displaying device type, software version, serial number Access to diagnostics can be protected with a passcode (SERVICE menu).
  • Page 103 Diagnostics Display Menu item Displaying the calibration data Select SENSOR_PH or SENSOR_OXY, MEMO SENS then select CALDATA usingkeys, press enter to confirm. Use thekeys to select the desired parameter from the bottom line of the display. For SENSOR_PH: MEMO SENS LAST_CAL (ISFET-ZERO) ZERO SLOPE NEXT_CAL For SENSOR_OXY: LAST_CAL ZERO SLOPE NEXT_CAL...
  • Page 104 Diagnostics Display Menu item Device self-test (To abort, you can press meas.) 1) Display test: Display of all segments with changing background colors white/green/red. Proceed by pressing enter 2) RAM test: Hourglass blinks, then display of --PASS-- or --FAIL-- Proceed by pressing enter 3) EEPROM test: Hourglass blinks, then display of --PASS-- or --FAIL-- Proceed by pressing enter...
  • Page 105 Diagnostics Display Menu item Displaying the logbook entries Select LOGBOOK using, press enter to confirm. MEMO SENS Using the  keys, you can scroll backwards and forwards through the logbook (entries -00-...-99-), -00- being the last entry. MEMO SENS If the display is set to date/time, you can search for a particular date using the ...
  • Page 106 Diagnostics Display Menu item Displaying the currently measured values (sensor monitor) MEMO SENS Select MONITOR using, press enter to confirm. Use thekeys to select the desired parameter from the bottom line of the display: mV_PH R_GLASS OPERATION TIME OPERATION TIME (A) SENSOR WEAR (A) LIFETIME (A) I-OXY (B) Display examples: PRESSURE (B) OPERATION TIME (B) SENSOR WEAR (B) LIFETIME (B).

  • Page 107: Service

    Service (SERVICE) A Service In the Service mode you can access the following menus: MONITOR Displaying currently measured values OUT1 Testing current output 1 OUT2 Testing current output 2 RELAY Testing the function of the 4 relays CONTROL Testing the controller function IRDA Activating and communicating via the IrDA interface CODES...
  • Page 108 Service Menu item Remark Displaying the currently measured values (sensor monitor) with HOLD mode activated: MEMO SENS Select MONITOR using, press enter to confirm. Select variable in the bottom text line using. The selected parameter is shown in the main display. As the device is in HOLD mode, you can perform validations using simulators without influencing the signal outputs.
  • Page 109 Service Menu item Remark Controller test (manual specification of controller output): MEMO SENS This function is used to start up control loops or check the actuators. For bumpless changeover to automatic operation (exiting this function), configure an I-action component (reset time). The lower display shows the currently adjusted Controller controller output Y.
  • Page 110 Service Menu item Remark Assigning passcodes: In the “SERVICE - CODES“ menu you can assign pass- codes to DIAG, HOLD, CAL, CONF, and SERVICE modes (Service preset to 5555). When you have lost the Service passcode, you have to request an “Ambulance TAN“ from the manufac- turer specifying the serial number and the hardware number of your device.

  • Page 111: Operating States

    Betriebszustände A Operating States Operating status Measuring DIAG 60 s P_CAL CONF SERVICE SERVICE OUT 1 SERVICE OUT 2 SERVICE RELAIS SERVICE CONTROLLER Cleaning function HOLD Explanation: as configured (Last/Fix or Last/Off ) active manual...

  • Page 112: Product Line And Accessories

    Product Line and Accessories Order Code Stratos Pro A 4... Channel 1 Channel 2 Example 0 1 N - PH 4-wire / 20...254 V AC/DC B,C,E Communication Without (HART retrofittable via TAN) 0 Version number Version Approvals General Safety ATEX / IECEX / FM / CSA Zone 2 / Cl 1 Div 2 B Meas.

  • Page 113: Specifications

    Operating modes Calibration with Calimatic automatic buffer recognition Manual calibration with entry of individual buffer values Display of asymmetry potential and slope Product calibration Calimatic buffer sets -00- Knick 2.00/4.01/7.00/9.21 -01- Mettler-Toledo 2.00/4.01/7.00/9.21 -02- Merck/Riedel 2.00/4.00/7.00/9.00/12.00 -03- Ciba (94) 2.06/4.00/7.00/10.00 -04- NIST technical 1.68/4.00/7.00/10.01/12.46...
  • Page 114 Specifications OXY input Input for Memosens sensors Operating modes Measurement in gases Measurement in liquids Display ranges Saturation (-10 ... 80°C) 0.0 ... 600.0 % Standard Concentration (-10 ... 80°C) 0.00 ... 99.99 mg/l (Dissolved oxygen) 0.00 ... 99.99 ppm Volume concentration in gas 0.00 ...
  • Page 115 Specifications I input Current input 0/4 ... 20 mA / 50 Ω for ext. pressure compensation Characteristic Linear 1.3) Measurement error < 1% current value + 0.1 mA HOLD input Galvanically separated (OPTO coupler) Function Switches device to HOLD mode Switching voltage 0 ...
  • Page 116 Specifications Alarm contact Relay contact, floating Contact ratings < 250 V / < 3 A / < 750 VA < 30 V / < 3 A / < 90 W Contact response N/C (fail-safe type) Response delay 0000 ... 0600 s Wash contact Relay contact, floating For controlling a cleaning system Contact ratings <...
  • Page 117 Specifications Derivative action* Rate time Td: 0000 ... 9999 s (0000 s = no derivative action) Controller type Pulse length controller or pulse frequency controller Pulse period 0001 ... 0600 s, min. ON time 0.5 s (pulse length controller) Max. pulse frequency 0001 ...
  • Page 118 Specifications Diagnostics functions Sensor data Calibration date, zero, slope, response time and wear Device self-test Displaytest, automatic memory test (RAM, FLASH, EEPROM), module test Logbook 100 events with date and time Extended logbook (TAN) AuditTrail: 200 events with date and time Service functions Sensor monitor Display of direct sensor signals (mV/temperature ...)
  • Page 119 Specifications Nominal operating conditions Ambient temperature -20 ... +55 °C Transport/Storage -20 ... +70 °C temperature Relative humidity 10 ... 95% not condensing Power supply 24 (–15%) ... 230 (+10%) V AC/DC (DC ≤ 80V) Frequency for AC 45 ... 65 Hz Enclosure Molded enclosure made of PBT/PC, glass-reinforced Mounting...
  • Page 120 Specifications...

  • Page 121: Error Handling

    Error Handling Alarm condition: • The display backlighting turns red • The alarm icon is displayed • The complete measured-value display blinks • “ERR xxx“ is displayed in the lower menu line Press the [info] key to view a short error text: •...

  • Page 122: Error Messages

    Error codes Error Messages Info text Problem (is displayed in case of Error Possible causes fault when the Info key is pressed) Error in factory settings EEPROM or RAM defective This error message only occurs in the case of a total defect. The device must be repaired and recalibrated at the factory.
  • Page 123 Error Messages Info text Problem Error (is displayed in case of fault Possible causes when the Info key is pressed) pH sensor messages, channel A No sensor (channel A) Sensor defective Sensor not connected Break in sensor cable Both channels switched off Wrong sensor type e.g.
  • Page 124 Error Messages Info text Problem Error (is displayed in case of fault Possible causes when the Info key is pressed) Load error Output current 1 < 3.8 mA Output current 1 < 20.5 mA Output current 2 < 3.8 mA Output current 2 <...

  • Page 125: Sensoface

    Sensoface (Sensocheck must have been activated during configuration.) The smiley in the display (Sensoface) alerts to sensor problems (defective sensor, sensor wear, maintenance request). The permitted calibration ranges and the conditions for a friendly, neutral, or sad Sensoface are summarized in the following table. Additional icons refer to the error cause.
  • Page 126 Sensoface Display Problem Status Asymmetry Asymmetry potential (zero) potential and and slope of the sensor are slope still okay. The sensor should be replaced soon. Asymmetry potential and slope of the sensor have reached values which no lon- ger ensure proper calibration. Replace sensor.
  • Page 127 Sensoface Display Problem Status Sensor wear High temperatures and pH values have caused a wear of over 80%. The sensor should be replaced soon. Wear is at 100%. Replace sensor.

  • Page 128: Fda 21 Cfr Part 11

    FDA 21 CFR Part 11 Conformity with FDA 21 CFR Part 11 In their directive “Title 21 Code of Federal Regulations, 21 CFR Part 11, Electronic Records; Electronic Signatures“ the US American health agency FDA (Food and Drug Administration) regulates the production and processing of electronic documents for pharmaceutical devel- opment and production.

  • Page 129: Index

    Index Access codes 128, 140 Accessories 112 Alarm 27 Alarm settings 60 Ambulance TAN 110 Assembly 10 Asymmetry potential 89 Audit Trail 105, 128 Automatic calibration (Calimatic) 84 Backlighting 21 Buffer set selection 39 Calibration 24, 80, 93 Calibration errors 121 Calibration timer 41, 45, 126 Calibration data 103 Calibration errors 121...
  • Page 130 Index Calimatic 84 CD-ROM 3 Channel selection and display assignment 29 CIP 43, 49 Configuration 24 Alarm 60 Cleaning cycles 42, 48 Controller 72 Current output 1 52 Current output 2 58 Individual configuration data 35 Limit function 62 Output current during Error and HOLD 56 Overview 28, 30, 31 OXY sensor 44 PH sensor 38...
  • Page 131 Index Data entry of premeasured sensors 88 Date 79 Display 100 Device self-test 104 Diagnostics 24, 102 Calibration data 103 Device self-test 104 Logbook 105 Sensor data 103 Sensor monitor 106 Version 106 Dimensions 11 Display 21 Display backlighting 21 Disposal 2 Documentation 3 EEPROM test 104...
  • Page 132 Index Output signal during HOLD 26, 57 Output signal response 26 Hysteresis 65, 67 Installation 14 Intended use 7 IrDA communication 109 Keypad 20 Limit 1 62 Limit 2 66 Logbook 105 Manual calibration with buffer entry 86 Measured values, display 106 Measurement 22, 100, 101 Measuring mode 50 Measuring mode selection 44...
  • Page 133 Index Output current, fixed value 108 Output current range 52, 58 Output filter 54 Output signal during HOLD 26, 57 Overview 9 OXY calibration 93 Oxy calibration mode 94 OXY sensor 44 Package contents 3, 10 Panel mounting 13 Parameter error 121 Passcodes 128, 140 Setting 110 PFC 71...
  • Page 134 Index RAM test 104 Rating plates 14 Registered trademarks 139 Relay 1 62 Relay 2 66 Relay test 108 Release of options 110 Reset to factory settings 110 Return of products under warranty 2 Safety information 7, 8 Safety instructions 3 Salinity 46 Selection menu 23 Sensocheck 60...
  • Page 135 Index Setpoint adjustment (controller) 101 Signal colors 21 Signal lines 15 SIP 43, 49 Slope calibration 98 Slope calibration (air) 99 Specifications 113 Start-up 8 TAG 79 Tag number (“TAG“) 79 TAN options 110, 112 Entering a TAN 110 TC-LIQUID 43 Temperature unit 50 Terminal assignments 14 Terminals 14...

  • Page 139: Trademarks

    Stratos® Sensocheck® Sensoface® Calimatic® GainCheck® InPro® is a registered trademark of Mettler-Toledo. Memosens® is a registered trademark of Endress+Hauser Conducta GmbH and Knick Elektronische Meßgeräte GmbH & Co. KG. HART® is a registered trademark of the HART Communication Foundation.

  • Page 140: Passcodes

    Operating Mode Passcode Service (SERVICE) 5555 Diagnostics (DIAG) HOLD mode Calibration (CAL) Configuration (CONF) Knick Elektronische Messgeräte GmbH & Co. KG P.O. Box 37 04 15 D-14134 Berlin Phone: +49 (0)30 - 801 91 - 0 Fax: +49 (0)30 - 801 91 - 200 Internet: http://www.knick.de...

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