Agilent Technologies 1290 Infinity User Manual
  1. Manuals
  2. Brands
  3. Agilent Technologies Manuals
  4. Laboratory Equipment
  5. 1290 infinity
  6. User manual
Agilent Technologies 1290 Infinity User Manual

Agilent Technologies 1290 Infinity User Manual

Thermostatted column
Hide thumbs Also See for 1290 Infinity:
Table of Contents

Advertisement

Quick Links

See also: User Manual
Agilent 1290 Infinity
Thermostatted Column
Compartment
User Manual
Agilent Technologies

Advertisement

Table of Contents
loading

Related Manuals for Agilent Technologies 1290 Infinity

Summary of Contents for Agilent Technologies 1290 Infinity

  • Page 1 Agilent 1290 Infinity Thermostatted Column Compartment User Manual Agilent Technologies...
  • Page 2 Notices Warranty © Agilent Technologies, Inc. 2008, 2009-2010 receive no greater than Restricted Rights as defined in FAR 52.227-19(c)(1-2) (June No part of this manual may be reproduced The material contained in this docu- 1987). U.S. Government users will receive in any form or by any means (including elec- ment is provided “as is,”...
  • Page 3 In This Guide... In This Guide... This manual covers the Agilent 1290 Infinity Thermostatted Column Compartment (TCC) (G1316C). 1 Introduction to the Column Compartment This chapter gives an introduction to the TCC, instrument overview and internal connectors. 2 Site Requirements and Specifications This chapter provides information on environmental requirements, physical and performance specifications.
  • Page 4 9 Parts and Materials for Maintenance This chapter provides information on parts for maintenance. 10 Identifying Cables This chapter summarizes information on all cables. 11 Appendix This chapter provides addition information on safety, legal and web. 1290 Infinity TCC User Manual...

  • Page 5: Table Of Contents

    4 How to optimize the Column Compartment Optimizing the Column Compartment Using Additional Heater Devices Delay Volume and Extra-Column Volume How to Configure the Optimum Delay Volume How to Achieve Higher Injection Volumes How to Achieve High Throughput 1290 Infinity TCC User Manual...
  • Page 6 9 Parts and Materials for Maintenance Valve Options Overview Heater and Cooling Devices Column Switching Valve 8 Position-9 Port 2 pos/6 Port Ultra High Pressure Valve Head 2Pos/10Port Ultra High Pressure Valve Head 8Pos/9Port Ultra High Pressure Valve Head 1290 Infinity TCC User Manual...
  • Page 7 CAN Cable RS-232 Cable Kit Agilent Module to Printer 11 Appendix General Safety Information The Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Lithium Batteries Information Radio Interference Sound Emission Solvent Information Agilent Technologies on Internet 1290 Infinity TCC User Manual...
  • Page 8 Contents 1290 Infinity TCC User Manual...

  • Page 9: Introduction To The Column Compartment

    1290 Infinity TCC User Manual Introduction to the Column Compartment Overview of the Module System Overview Column-Identification System Column Switching Valve (Optional) Typical Applications Early Maintenance Feedback Instrument Layout Electrical Connections Serial Number Information Rear view of the module Interfaces...

  • Page 10: Overview Of The Module

    The Agilent 1290 Infinity thermostatted column compartments is a stackable temperature-controlled column compartment for LC. It is available as standalone module or as a component of an Agilent 1290 Infinity system. It is used for heating and cooling to meet extreme requirements of retention time reproducibility.

  • Page 11: System Overview

    This depends on several factors: flow rate, setpoint temperature, ambient temperature and column dimensions. The higher the flow rate, the faster the column equilibrates (due to thermostatted mobile phase). 1290 Infinity TCC User Manual...
  • Page 12 The equilibration of the column may take longer. Stability of the pressure signal is a good indication for equilibrium. Figure 1 Equilibration of Heat Exchanger and Column Temperature The temperature calibration and verification is described in the Service Manual. 1290 Infinity TCC User Manual...

  • Page 13: Column-Identification System

    Introduction to the Column Compartment Column-Identification System Column-Identification System The Agilent 1290 Infinity thermostatted column compartment is equipped with a column-identification system. It allows to read and write column-specific information to and from the column-identification tag. Figure 2 Column-Identification System Table 1 on page 14 shows the information that can be stored.
  • Page 14 (and vice versa). If no column switching valve is installed, both sides are updated at the same time. If an 8 Position/9 Port valve is installed, no tag is updated for avoiding ambiguity as more than 2 columns might be installed. 1290 Infinity TCC User Manual...

  • Page 15: Column Switching Valve (Optional)

    Before switching the valve, switch off the pump or set the flow to zero. Keeping the flow on N O T E while the valve is switched can cause exceeding the maximum pressure. This will stop method or sequence execution. 1290 Infinity TCC User Manual...
  • Page 16 The sample is injected into series-connected precolumn and analytical column. After the valve has switched, the analytical column flow continues in normal direction. Only the precolumn is back-flushed, eluting highly retained peaks directly to the detector. 1290 Infinity TCC User Manual...
  • Page 17 Introduction to the Column Compartment Column Switching Valve (Optional) Figure 6 Precolumn Back-flushing 1290 Infinity TCC User Manual...
  • Page 18 Before injection into a LC or LC/MS system, the sample matrix must be separated from the analytes of interest. Otherwise, contaminants can disrupt separation and detection or even damage the analytical column. 1290 Infinity TCC User Manual...
  • Page 19 Introduction to the Column Compartment Column Switching Valve (Optional) Figure 7 Sample enrichment 1290 Infinity TCC User Manual...
  • Page 20 Introduction to the Column Compartment Column Switching Valve (Optional) Figure 8 Sample clean-up 1290 Infinity TCC User Manual...
  • Page 21 After the valve switches, an additional pump backflushes the matrix components out of the pre-column to waste, while the analytes are separated on the main column. Backflushing prepares the pre-column for the next injection. 1290 Infinity TCC User Manual...
  • Page 22 Introduction to the Column Compartment Column Switching Valve (Optional) Alternating Column Regeneration Only 2pos/10port valve (p/n G4232B) Advantages: • High sample throughput • Increased productivity • High efficiency Figure 9 Alternating Column Regeneration 1290 Infinity TCC User Manual...
  • Page 23 LC. Since the gradient elution requires the column to regenerate before subsequent runs, an automated column regeneration system saves valuable analysis time. Agilent’s 2-position/10-port valve for the 1290 Infinity TCC enable the simultaneous analysis of one sample on one LC column while a second, identical column is flushed and equilibrated by an additional regeneration pump.

  • Page 24: Early Maintenance Feedback

    EMF limits, and then reset the EMF counters to zero. The next time the EMF counters exceed the new EMF limits, the EMF flag will be displayed, providing a reminder that maintenance needs to be scheduled. 1290 Infinity TCC User Manual...

  • Page 25: Instrument Layout

    • the plastic layers help cushion the electronic and mechanical parts from physical shock, and • the metal inner cabinet shields the internal electronics from electromagnetic interference and also helps to reduce or eliminate radio frequency emissions from the instrument itself. 1290 Infinity TCC User Manual...

  • Page 26: Electrical Connections

    There are no externally accessible fuses, because automatic electronic fuses are implemented in the power supply. Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations.
  • Page 27 • DE = Germany • JP = Japan • CN = China year and week of last major manufacturing change, e.g. 820 could be week 20 of 1998 or 2008 SSSSS real serial number 1290 Infinity TCC User Manual...
  • Page 28 Introduction to the Column Compartment Electrical Connections Rear view of the module Figure 10 Rear view of the module 1290 Infinity TCC User Manual...

  • Page 29: Interfaces

    The detector with on-board LAN is the preferred access point for control via LAN of the N O T E detector and/or the 1290 Infinity system. The inter-module communication is done via CAN. • CAN connectors as interface to other modules, •...
  • Page 30 There is no configuration possible on main boards with on-board LAN. These are N O T E pre-configured for • 19200 baud, • 8 data bit with no parity and • one start bit and one stop bit are always used (not selectable). 1290 Infinity TCC User Manual...
  • Page 31 9-pin male SUB-D type connector. The pins are defined as: Table 3 RS-232C Connection Table Direction Function Ground Figure 11 RS-232 Cable Analog Signal Output The analog signal output (e.g. detector signal or pump pressure signal) can be distributed to a recording device. 1290 Infinity TCC User Manual...
  • Page 32 APG Remote The APG Remote connector may be used in combination with other analytical instruments from Agilent Technologies if you want to use features as common shut down, prepare, and so on. Remote control allows easy connection between single instruments or systems to ensure coordinated analysis with simple coupling requirements.
  • Page 33 START REQUEST (L) Request to start injection cycle (for example, by start key on any module). Receiver is the autosampler. Special Interfaces Some modules have module specific interfaces/connectors. They are described in the module documentation. 1290 Infinity TCC User Manual...

  • Page 34: Setting The 8-Bit Configuration Switch

    Location of Configuration Switch (example shows a G4212A DAD) To perform any LAN configuration, SW1 and SW2 must be set to OFF. For details on the N O T E LAN settings/configuration refer to chapter LAN Configuration. 1290 Infinity TCC User Manual...
  • Page 35 When selecting the mode TEST, the LAN settings are: Auto-Negotiation & Using Stored. N O T E For explanation of "Boot Resident System" and "Revert to Default Data (Coldstart)" refer to N O T E “Special Settings” on page 39. 1290 Infinity TCC User Manual...
  • Page 36 With the introduction of the Agilent 1260 Infinity, all GPIB interfaces have been removed. N O T E The preferred communication is LAN. The following tables represent the configuration switch settings for the modules without N O T E on-board LAN only. 1290 Infinity TCC User Manual...
  • Page 37 Data Bits Parity Use the following tables for selecting the setting which you want to use for RS-232C communication. The number 0 means that the switch is down and 1 means that the switch is up. 1290 Infinity TCC User Manual...
  • Page 38 Switches Parity No Parity Odd Parity Even Parity One start bit and one stop bit are always used (not selectable). Per default, the module will turn into 19200 baud, 8 data bit with no parity. 1290 Infinity TCC User Manual...
  • Page 39 Exceptions are diagnosis and repair log books which will not be erased. ➔ Save your methods and data before executing a forced cold start. If you use the following switch settings and power the instrument up again, a forced cold start has been completed. 1290 Infinity TCC User Manual...
  • Page 40 Introduction to the Column Compartment Setting the 8-bit Configuration Switch Table 12 Forced Cold Start Settings (without on-board LAN) Mode Select TEST/BOOT No LAN TEST/BOOT 1290 Infinity TCC User Manual...

  • Page 41: Site Requirements And Specifications

    1290 Infinity TCC User Manual Site Requirements and Specifications Site Requirements Physical Specifications Performance Specifications Extended Specifications on G1316C This chapter provides information on environmental requirements, physical and performance specifications. Agilent Technologies...

  • Page 42: Site Requirements

    In case of emergency it must be possible to disconnect the instrument from the power line at any time. ➔ Make sure the power connector of the instrument can be easily reached and unplugged. ➔ Provide sufficient space behind the power socket of the instrument to unplug the cable. 1290 Infinity TCC User Manual...
  • Page 43 Never operate your instrumentation from a power outlet that has no ground connection. ➔ Never use a power cord other than the Agilent Technologies power cord designed for your region. Use of unsupplied cables WA R N I N G Using cables not supplied by Agilent Technologies can lead to damage of the electronic components or personal injury.
  • Page 44 Do not store, ship or use your module under conditions where temperature fluctuations could cause condensation within the module. ➔ If your module was shipped in cold weather, leave it in its box and allow it to warm slowly to room temperature to avoid condensation. 1290 Infinity TCC User Manual...

  • Page 45: Physical Specifications

    Non-condensing Operating Altitude Up to 2000 m (6562 ft) Non-operating altitude Up to 4600 m (15091 ft) For storing the module Safety standards: IEC, CSA, Installation Category II, Pollution Degree 2 For indoor use only. 1290 Infinity TCC User Manual...

  • Page 46: Performance Specifications

    “Column-Identification System” page 13 Housing All materials recyclable. All specifications are valid for distilled water at ambient temperature (25 °C), set point at N O T E 40 °C and a flow range from 0.2–5 ml/min. 1290 Infinity TCC User Manual...

  • Page 47: Extended Specifications On G1316C

    Extended Specifications on G1316C Extended Specifications on G1316C The 1290 Infinity G1316C thermostatted column compartment is usable from 10 °C below ambient up to 80 °C for flow ranges up to 5 ml/min and up to 100 °C for flow ranges up to 2.5 ml/min. Additional heating devices are...
  • Page 48 Site Requirements and Specifications Extended Specifications on G1316C 1290 Infinity TCC User Manual...

  • Page 49: Installing The Module

    1290 Infinity TCC User Manual Installing the Module Unpacking the module Damage to the module Delivery Checklist Optimizing the Stack Configuration One Stack Configuration Two Stack Configuration Installing the Column Compartment Installing Valve Heads Installation of Heater Devices Flow Connections of the Column Compartment...

  • Page 50: Unpacking The Module

    Damage to the module If the delivery packaging shows signs of external damage, please call your Agilent Technologies sales and service office immediately. Inform your service representative that the instrument may have been damaged during shipment. "Defective on arrival" problems C A U T I O N If there are signs of damage, please do not attempt to install the module.

  • Page 51: Optimizing The Stack Configuration

    Optimizing the Stack Configuration Optimizing the Stack Configuration If your column compartment is part of an Agilent 1290 Infinity system, you can ensure optimum performance by installing the following configuration. This configuration optimizes the system flow path, ensuring minimum delay volume.
  • Page 52 Installing the Module Optimizing the Stack Configuration Figure 15 Recommended Stack Configuration (Front View) 1290 Infinity TCC User Manual...
  • Page 53 Installing the Module Optimizing the Stack Configuration Figure 16 Recommended Stack Configuration (Rear View) 1290 Infinity TCC User Manual...

  • Page 54: Two Stack Configuration

    A slightly longer capillary is required between the pump and autosampler. See Figure 17 on page 54 and Figure 18 on page 55). Figure 17 Recommended Two Stack Configuration (Front View) 1290 Infinity TCC User Manual...
  • Page 55 Installing the Module Optimizing the Stack Configuration Figure 18 Recommended Two Stack Configuration (Rear View) 1290 Infinity TCC User Manual...

  • Page 56: Installing The Column Compartment

    Valve properties will not be updated, if the valve head is replaced while the module is on. Selection of valve port positions can fail, if the instrument does not know the properties of the installed valve. Always switch off the instrument when replacing the valve head. 1290 Infinity TCC User Manual...
  • Page 57 1 Remove the 5 screws, which hold the lock in position. 2 Remove the dummy valve head by unscrewing the cap nut and removing it from the valve drive. 3 Place the module on the bench in a horizontal position. 1290 Infinity TCC User Manual...
  • Page 58 6 Connect the power cable to the power connector at the rear of the module. The security lever will prevent that the cover is opened while the power cord is connected to the module. 1290 Infinity TCC User Manual...
  • Page 59 Figure 20 Recommended Stack Configuration (Rear View) 8 If Agilent ChemStation is the controller, connect the LAN connection to the LAN interface in the detector. 9 Connect the APG remote cable (optional) for non-Agilent instruments. 1290 Infinity TCC User Manual...
  • Page 60 When the line power button stands out and the green light is off, the module is turned off. N O T E The module was shipped with default configuration settings. For changing these settings, N O T E please refer to service manual "Setting the 8-bit configuration switch". 1290 Infinity TCC User Manual...

  • Page 61: Installing Valve Heads

    Switching the valve to a wrong position can damage the column or bias measurement results. ➔ Fitting the lobe to the groove is essential for making sure the valve is switched to the correct position. 1290 Infinity TCC User Manual...
  • Page 62 Screw the valve head onto the valve drive using the union fits to the groove. nut. Install all required capillary connections to the valve head. N O T E Fasten the nut manually. Do not use any tools. 1290 Infinity TCC User Manual...
  • Page 63 Installing the Module Installing Valve Heads Push the valve head until it snaps in and stays in the rear position. 1290 Infinity TCC User Manual...

  • Page 64: Installation Of Heater Devices

    If the additional heat exchangers are used as shown in this figure, the column identification N O T E system cannot be used. If the column identification system is required, fix the heater devices in the upper or lower locations or right/left of the current location. 1290 Infinity TCC User Manual...
  • Page 65 (p/n G1316-89200) using 3 screws (Screw 2.5 mm hex (p/n 0515-1052), included to part number for carrier) as shown in Figure 22 page 65. Figure 22 Installing the low dispersion heat exchangers 1290 Infinity TCC User Manual...

  • Page 66: Flow Connections Of The Column Compartment

    ➔ The amount of substances should be reduced to the minimal volume required for the analysis. ➔ Do not operate the instrument in an explosive atmosphere. 1290 Infinity TCC User Manual...
  • Page 67 Or place the column on the right heat exchanger N O T E assembly and connect the capillaries to the column. “Column Switching Valve (Optional)” on page 15 on how to connect the column selection valve. 1290 Infinity TCC User Manual...
  • Page 68 Fix the column with the column clip from the accessory If the column compartment is not part of an Agilent 1290 kit. Infinity system, or if an Agilent 1290 Infinity Autosampler is located on top, connect the corrugated tubing to the waste outlet.
  • Page 69 ➔ The amount of substances should be reduced to the minimal volume required for the analysis. ➔ Do not operate the instrument in an explosive atmosphere. 1290 Infinity TCC User Manual...
  • Page 70 For more information on column identification, see The internal volumes of the heat exchanger assemblies “Column-Identification System” on page 13. comprise a volume of 3 µl (left) and 6 µl (right). The internal capillary diameter is 0.17 mm. 1290 Infinity TCC User Manual...
  • Page 71 Optionally place the column tag in front of the tag reader. Fix the column with the column clip from the accessory N O T E kit. “Column Switching Valve (Optional)” on page 15 on how to connect the column selection valve. 1290 Infinity TCC User Manual...
  • Page 72 If the column compartment is not part of an Agilent 1290 Route tubings from modules above through the openings Infinity system, or if an Agilent 1290 Infinity Autosampler in the funnel holder (top) and the plastic bottom part. is located on top, connect the corrugated tubing to the Remove small plastic plugs first.
  • Page 73 The installation of the column compartment has now been completed. Always operate the TCC with the front cover in place for proper thermostatting conditions N O T E and to protect the column area against strong drafts from the outside. 1290 Infinity TCC User Manual...

  • Page 74: Placing Columns

    Figure 23 on page 74 and Figure 24 on page 74. The Agilent logo should always be at front. Figure 23 Column-Identification Tag for Left Heat Exchanger Figure 24 Column-Identification Tag for Right Heat Exchanger 1290 Infinity TCC User Manual...
  • Page 75 Installing the Module Placing Columns Column Clip For better positioning of the column on the heat exchanger a column clip is available (see “Accessory Kits” on page 162). Figure 25 Column clip 1290 Infinity TCC User Manual...
  • Page 76 Installing the Module Placing Columns 1290 Infinity TCC User Manual...

  • Page 77: How To Optimize The Column Compartment

    1290 Infinity TCC User Manual How to optimize the Column Compartment Optimizing the Column Compartment Using Additional Heater Devices Delay Volume and Extra-Column Volume Delay Volume Extra-Column Volume How to Configure the Optimum Delay Volume How to Achieve Higher Injection Volumes...

  • Page 78: Optimizing The Column Compartment

    • Keep the left and right heat exchanger temperature the same unless you do specific applications. • Assure that the front cover is always closed. 1290 Infinity TCC User Manual...

  • Page 79: Using Additional Heater Devices

    Using Additional Heater Devices Using Additional Heater Devices The optimization, installation, interconnection, and specific settings when using additional heating devices are described in the Agilent 1290 Infinity LC System - System Manual and Quick Reference (p/n G4220-90300). 1290 Infinity TCC User Manual...

  • Page 80: Delay Volume And Extra-Column Volume

    The delay volume in a system includes the volume in the pump from the point of mixing, connections between pump and autosampler, volume of the flow path through the autosampler and connections between autosampler and column. 1290 Infinity TCC User Manual...

  • Page 81: Extra-Column Volume

    The extra-column volume is minimized with the Agilent 1290 Infinity/Agilent 1260 Infinity LC System due to the narrow-bore (0.12 mm i.d.) tubing, the low-volume heat exchangers in the column compartment and the Max-Light cartridge cell in the detector.

  • Page 82: How To Configure The Optimum Delay Volume

    0.12 mm i.d. capillaries. The built-in 3 µl and 6 µl heat exchangers are for backwards compatibility and should only be used in case a conventional method needs to be run on the system even though in this case also the low dispersion heat exchanger could be used. 1290 Infinity TCC User Manual...

  • Page 83: How To Achieve Higher Injection Volumes

    Figure 7 on page 19. The valve can be conveniently located in the Thermostatted Column Compartment. Figure 26 Sample enrichment 1290 Infinity TCC User Manual...

  • Page 84: How To Achieve High Throughput

    The second pump is only required to flush an isocratic mixture through the column and so can be a simpler pump than the 1290 Infinity pumps. For instance a 1200 Series isocratic pump would be sufficient to perform this task. The setup is...
  • Page 85 How to optimize the Column Compartment How to Achieve High Throughput Figure 27 Alternating Column Regeneration 1290 Infinity TCC User Manual...
  • Page 86 How to optimize the Column Compartment How to Achieve High Throughput 1290 Infinity TCC User Manual...

  • Page 87: Troubleshooting And Diagnostics

    1290 Infinity TCC User Manual Troubleshooting and Diagnostics Overview of the Module’s Indicators and Test Functions Status indicators Power Supply Indicator Module Status Indicator Available Tests vs User Interfaces Agilent Lab Advisor Software Overview about the troubleshooting and diagnostic features.

  • Page 88: Overview Of The Module's Indicators And Test Functions

    Normally, temperature calibration is not required throughout the lifetime of the instrument. However, in order to comply with local regulatory requirements, calibration and verification may be required. The following sections describe these functions in detail. 1290 Infinity TCC User Manual...

  • Page 89: Status Indicators

    Figure 28 Location of Status indicators Power Supply Indicator The power supply indicator is integrated into the main power switch. When the indicator is illuminated (green) the power is ON. 1290 Infinity TCC User Manual...

  • Page 90: Module Status Indicator

    • A fast red-blinking (modules with on-board LAN) or fast yellow-blinking (modules without on-board LAN) indicator indicates that the module is in boot loader mode (e.g. during update of main firmware). In such a case try to re-boot the module or try a cold-start. 1290 Infinity TCC User Manual...

  • Page 91: Available Tests Vs User Interfaces

    • Preferred tool should be the Agilent Diagnostic Software, see “Agilent Lab Advisor Software” on page 92. • The Agilent ChemStation B.04.02 and above may not include any maintenance/test functions. • Screenshots used within these procedures are based on the Agilent Lab Advisor Software. 1290 Infinity TCC User Manual...

  • Page 92: Agilent Lab Advisor Software

    Agilent Lab Advisor software may differ from the descriptions in this manual. For details refer to the Agilent Lab Advisor software help files. This manual provides lists with the names of Error Messages, Not Ready messages, and other common issues. 1290 Infinity TCC User Manual...

  • Page 93: Error Information

    1290 Infinity TCC User Manual Error Information What Are Error Messages General Error Messages Timeout Shut-Down Remote Timeout Synchronization Lost Leak Leak Sensor Open Leak Sensor Short TCC Error Messages Compensation Sensor Open Compensation Sensor Short Left Fan Failed Right Fan Failed...

  • Page 94: What Are Error Messages

    (for example, repair, or exchange of consumables is necessary). In the event of such a failure, the red status indicator at the front of the module is switched on, and an entry is written into the module logbook. 1290 Infinity TCC User Manual...

  • Page 95: General Error Messages

    Check the logbook for the occurrence and A not-ready condition was present during a source of a not-ready condition. Restart the sequence or multiple-injection run for a analysis where required. period longer than the timeout threshold. 1290 Infinity TCC User Manual...

  • Page 96: Shut-Down

    Check the vacuum degasser for an error The degasser failed to generate sufficient condition. Refer to the Service Manual for the vacuum for solvent degassing. degasser or the 1260 pump that has the degasser built-in. 1290 Infinity TCC User Manual...

  • Page 97: Remote Timeout

    • Ensure all CAN cables are installed correctly. Exchange the CAN cable. Defective CAN cable. Switch off the system. Restart the system, and Defective main board in another module. determine which module or modules are not recognized by the system. 1290 Infinity TCC User Manual...

  • Page 98: Leak

    Please contact your Agilent service Leak sensor not connected to the main representative. board. Please contact your Agilent service Defective leak sensor. representative. Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. 1290 Infinity TCC User Manual...

  • Page 99: Leak Sensor Short

    Suggested actions Please contact your Agilent service Defective flow sensor. representative. • Please contact your Agilent service Leak sensor incorrectly routed, being representative. pinched by a metal component. • Please contact your Agilent service representative. 1290 Infinity TCC User Manual...

  • Page 100: Tcc Error Messages

    If the resistance across the sensor falls below the lower limit, the error message is generated. Probable cause Suggested actions Please contact your Agilent service Defective main board. representative. 1290 Infinity TCC User Manual...

  • Page 101: Left Fan Failed

    5 seconds, the error message is generated. Probable cause Suggested actions Please contact your Agilent service Fan cable disconnected. representative. Please contact your Agilent service Defective fan. representative. Please contact your Agilent service Defective TCC board. representative. 1290 Infinity TCC User Manual...

  • Page 102: Open Cover

    OFF the peltier elements after a short delay, and the error message is generated. Probable cause Suggested actions Please contact your Agilent service The column compartment was switched on representative. with the top cover and foam removed. 1290 Infinity TCC User Manual...

  • Page 103: Left Temperature Timeout

    The temperature of the right heat exchanger did not reach the temperature setpoint within the timeout threshold. Probable cause Suggested actions Please contact your Agilent service Defective right heater assembly. representative. Please contact your Agilent service Defective TCC board. representative. 1290 Infinity TCC User Manual...

  • Page 104: Defective Temperature Sensor

    Please contact your Agilent service Flex board not connected (only if all left or representative. right sensor error messages appear simultaneously). Please contact your Agilent service Defective heater assembly. representative. Please contact your Agilent service Defective TCC board. representative. 1290 Infinity TCC User Manual...

  • Page 105: Heater Profile

    If the temperature is not changing as expected, the error message is generated. Probable cause Suggested actions Please contact your Agilent service Defective heater assembly. representative. Please contact your Agilent service Defective TCC board. representative. 1290 Infinity TCC User Manual...

  • Page 106: Column Temperature

    70 °C, the current is switched OFF and the error message is generated. Probable cause Suggested actions Please contact your Agilent service Defective heater assembly. representative. Please contact your Agilent service Defective TCC board. representative. 1290 Infinity TCC User Manual...

  • Page 107: Defective Heater Circuit

    Defect in cable connection of valve drive representative. control. Please contact your Agilent service Defect in cable connection of valve actuator representative. encoder reader. Please contact your Agilent service Defect of valve drive or valve actuator representative. encoder reader. 1290 Infinity TCC User Manual...

  • Page 108: Unknown/Unsupported Valve Detected (2872)

    Probable cause Suggested actions Please contact your Agilent service Defect in cable connection of door sensor to representative. main board. Please contact your Agilent service Door sensor defective. representative. 1290 Infinity TCC User Manual...

  • Page 109: Valve Rfid Access Failure (2874)

    Review installation of valve head, see “Installing Valve head not installed correctly. Valve Heads” on page 61. Replace valve head, see Table 18 on page 150. RFID tag defective. Please contact your Agilent service Valve tag reader is damaged. representative. 1290 Infinity TCC User Manual...
  • Page 110 Error Information TCC Error Messages 1290 Infinity TCC User Manual...

  • Page 111: Test Functions And Calibrations

    1290 Infinity TCC User Manual Test Functions and Calibrations Thermostat Function Test Pressure Test Temperature Calibration Temperature Calibration Procedure Calibration Problems Installing the Temperature Sensor This chapter describes the TCC’s built in test functions. Agilent Technologies...

  • Page 112: Thermostat Function Test

    The time required to reach 30 °C is a measure of heating efficiency. Thermostat Function Test Result A typical Thermostat Function Test profile is shown in Figure 29 on page 112. Figure 29 Typical Thermostat Function Test Profile 1290 Infinity TCC User Manual...
  • Page 113 During the cooling phase, the Peltier elements should cool at a rate of >2 °C/minute. During the heating phase, the temperature change should be >3 °C/minute. Defective thermostat components may cause cooling or heating rates to fall outside these limits. 1290 Infinity TCC User Manual...

  • Page 114: Pressure Test

    Do not use the test for modules having a lower maximum pressure than the pump as this will damage the valve. For example do not use 400 bar valve in a TCC in combination with a 600 bar pump (G1312B Binary Pump SL). 1290 Infinity TCC User Manual...

  • Page 115: Temperature Calibration

    The column thermostat is calibrated correctly when the measured temperature (using the external measuring device, “Temperature Calibration Procedure” on page 116) and the cross-over temperature (36 °C) of both heat exchangers (left and right) are within a range of ± 0.5 °C. 1290 Infinity TCC User Manual...

  • Page 116: Temperature Calibration Procedure

    For the measuring and calibration process Agilent Technologies recommends a N O T E thermometer with 0.1 °C precision. Contact the local Agilent Technologies support representative for ordering information. The figures in this procedure refer to a specific type of temperature sensor (Heraeus, N O T E Quat340, quartz surface-temperature measurement sensor).

  • Page 117: Calibration Problems

    Installation of the temperature sensor is required for the temperature calibration and temperature verification procedures. The figures below refer to a specific type of temperature sensor (Heraeus, Quat340, quartz N O T E surface-temperature measurement sensor). Other sensors may require a different fixing. 1290 Infinity TCC User Manual...
  • Page 118 Test Functions and Calibrations Temperature Calibration Remove the front cover. Install the temperature sensor at the measurement position on the left heat exchanger. Route the sensor wire through the slit in the leak tray. Re-install the front cover. 1290 Infinity TCC User Manual...

  • Page 119: Maintenance

    1290 Infinity TCC User Manual Maintenance Introduction to Maintenance and Repair Cautions and Warnings Overview of Maintenance Cleaning the Column Compartment Changing Column Identification Tags Adding Heater Devices Installing the capillaries Correcting Leaks Replacing Valve Heads Preparing the Thermostatted Column Compartment for...

  • Page 120: Introduction To Maintenance And Repair

    There are no serviceable parts inside. N O T E Do not open the module. 1290 Infinity TCC User Manual...

  • Page 121: Cautions And Warnings

    ➔ Remove the power cable from the instrument before opening the cover. ➔ Do not connect the power cable to the Instrument while the covers are removed. 1290 Infinity TCC User Manual...
  • Page 122 C A U T I O N ➔ If you connect external equipment to the instrument, make sure that you only use accessory units tested and approved according to the safety standards appropriate for the type of external equipment. 1290 Infinity TCC User Manual...

  • Page 123: Overview Of Maintenance

    If the valve performance shows page 142 indication of leakage or wear “Preparing the Thermostatted If the TCC shall be transported Column Compartment for Transportation” on page 145 “Replacing the Module If required Firmware” on page 147 1290 Infinity TCC User Manual...

  • Page 124: Cleaning The Column Compartment

    WA R N I N G Liquid in the module electronics can cause shock hazard and damage the module. ➔ Do not use an excessively damp cloth during cleaning. ➔ Drain all solvent lines before opening any fittings. 1290 Infinity TCC User Manual...

  • Page 125: Changing Column Identification Tags

    Figure 31 Column-Identification System When If column is used on the opposite heat exchanger or a tag is added to a new column. Parts required Description 5062-8588 Column identification tag, pack of 3 1290 Infinity TCC User Manual...
  • Page 126 Column-Identification Tag for Right Heat Exchanger 3 For columns with small diameter, a cable tie wrap should be used to fix the column identification tag to the column. Assure that the tie wrap does not block the front cover. 1290 Infinity TCC User Manual...

  • Page 127: Adding Heater Devices

    Adding Heater Devices Adding Heater Devices The additional heater devices can be arranged in the G1316C in various locations depending on the application needs. Some examples are shown below. Figure 34 Arrangements of Heater and Cooling Devices 1290 Infinity TCC User Manual...
  • Page 128 If the column identification system is required, fix the heater devices in the upper or lower locations or fix them right/left of the current location. The heater devices are mounted on a carrier that can be fitted to the left and/or right heat exchangers. 1290 Infinity TCC User Manual...
  • Page 129 For the G1316C, additional heat exchanger devices can be installed on the carrier Carrier for heat exchanger (p/n G1316-89200) using 3 screws (Screw 2.5 mm hex (p/n 0515-1052), included to part number for carrier) as shown in figure below. 1290 Infinity TCC User Manual...
  • Page 130 For the heater device inlet capillary choose fittings which are compatible to your column. Figure 37 Fitting type depends on column type The nut seal tight is pressure tight only up to 600 bar! N O T E 1290 Infinity TCC User Manual...

  • Page 131: Installing The Capillaries

    2pos/6port valve G4232B 2pos/10port valve Preparations Identify the required capillaries in your capillary kits (“Common capillary kit (5067-4646)” page 164) Use outmost care to avoid any void volumes caused by poor connections. N O T E 1290 Infinity TCC User Manual...
  • Page 132 1 Install the capillaries depending on your application. Following configurations are available for listed applications. Please choose your appropriate configuration from this list: Figure 38 Installing the capillaries for a dual-column selection set-up (column and heat exchanger of the second position are omitted) 1290 Infinity TCC User Manual...
  • Page 133 Flow direction from top to bottom needs switch of connected capillaries at ports 5 and 2. Also column inlet connections needed to be switched with outlet connections. Port 4 to 3 and 6 to 1.) 1290 Infinity TCC User Manual...
  • Page 134 Maintenance Installing the capillaries Figure 39 Installing the capillaries for a sample enrichment set-up 1290 Infinity TCC User Manual...
  • Page 135 Low dispersion heat exchanger or build-in 3 µL/6 µL heat exchanger and 90 mm length capillary to column Pos.1: Connection between ports 1-6 , 4-5, 2-3 , active column 1 = left (enrichment column) Pos. 2: Connection between ports 1-2, 3-4, 5-6 active column 2 = right (analytical colum) 1290 Infinity TCC User Manual...
  • Page 136 Maintenance Installing the capillaries Figure 40 Installing the capillaries for a sample clean-up set-up 1290 Infinity TCC User Manual...
  • Page 137 Low dispersion heat exchanger or build-in 3 µL/6 µL heat exchanger and 90 mm length capillary to column Pos.1: Connection between ports 1-6 , 4-5, 2-3 , active column 1 = left (enrichment column) Pos. 2: Connection between Ports 1-2, 3-4, 5-6 active column 2 = right (analytical colum) 1290 Infinity TCC User Manual...
  • Page 138 Maintenance Installing the capillaries Figure 41 Installing the capillaries for alternating column regeneration (column and heat exchanger of the second position are omitted) 1290 Infinity TCC User Manual...
  • Page 139 Pos.1: Connection between ports 1-10 , 2-3, 4-5, 6-7, 8-9 active column 1 = left / regemerating column = right Pos. 2: Connection between ports 1-2, 3-4, 5-6, 7-8, 9-10 active column 2 = right / regenerating column = left 1290 Infinity TCC User Manual...
  • Page 140 9 Place the capillaries that go to another module or waste into the capillary guides to prevent squeezing them when closing the front cover. 10 Stow any excess lengths of the capillaries. 11 Perform a final leak-check. 1290 Infinity TCC User Manual...

  • Page 141: Correcting Leaks

    2 Use a pipette and tissue to dry the leak sensor area. 3 Observe the capillary connections and the column switching valve for leaks and correct, if required. 4 Re-install the front cover. Figure 42 Possible Leak Areas 1290 Infinity TCC User Manual...

  • Page 142: Replacing Valve Heads

    C A U T I O N Switching the valve to a wrong position can damage the column or bias measurement results. ➔ Fit the lobe to the groove to make sure the valve is switched to the correct position. 1290 Infinity TCC User Manual...
  • Page 143 Always switch off the instrument when replacing the valve head. Switch off the module. Unscrew the valve head. Push the valve head for bringing it to its outer position and unscrew all capillary connections from the valve head. 1290 Infinity TCC User Manual...
  • Page 144 Screw the valve head onto the valve drive using the union lobe fits to the groove. nut. Install all required capillary connections to the valve head. Push the valve head until it snaps in and stays in the rear position. Switch on the module. 1290 Infinity TCC User Manual...

  • Page 145: Preparing The Thermostatted Column Compartment For Transportation

    Transportation Lock Kit (p/n G1316-67001) can be re-ordered. Remove the valve head as described in “Replacing Valve Replace the valve head by the transportation valve head. Heads” on page 142. Bring the transportation valve head to the outer position. 1290 Infinity TCC User Manual...
  • Page 146 Lock plate (p/n G1316-03701) to the heat exchangers to the Transportation valve head (p/n G1316-40002) in in the outer positions of the plate. the central position of the plate. Put the spring washer (not shown) between the screw and the lock plate. 1290 Infinity TCC User Manual...

  • Page 147: Replacing The Module Firmware

    Initial firmware (main A.06.10 and resident) Compatible with All other modules must have firmware revision A.06.1x or B.06.1x or above (main 1100/1200 series and resident). Otherwise the communication will not work. modules Conversion to / emulation 1290 Infinity TCC User Manual...
  • Page 148 Maintenance Replacing the Module Firmware 1290 Infinity TCC User Manual...

  • Page 149: Parts And Materials For Maintenance

    1290 Infinity TCC User Manual Parts and Materials for Maintenance Valve Options Overview Heater and Cooling Devices Column Switching Valve 8 Position-9 Port 2 pos/6 Port Ultra High Pressure Valve Head 2Pos/10Port Ultra High Pressure Valve Head 8Pos/9Port Ultra High Pressure Valve Head...

  • Page 150: Valve Options Overview

    Rotor seal (p/n Stator head (p/n G4231B) pressure (1200 bar) 5068-0008) 5068-0006) valve head (p/n 5067-4117) Valve Head 2 Postion / Rotor Seal, PEEK (p/n Stator head (p/n 6 Port, 600 bar (p/n 0101-1409) 5068-0006) 5067-4137) 1290 Infinity TCC User Manual...
  • Page 151 Method development valves kits include the valve head(s), column, capillaries, manual and instal- lation and familiarization service G4230A contains 2 valve heads 8 pos/9 port valve head low pressure (400 bar) (p/n 5067-4108) kit with stator face and rotor seal 1290 Infinity TCC User Manual...

  • Page 152: Heater And Cooling Devices

    For fittings see Table 20 on page 153 Column clip set, 8 colors (p/n 5042-9918) Carrier for heat exchanger (p/n G1316-89200) Fitting holder assy, includes following items: Fitting fork, fitting clip screws (pack of 4) (p/n G1316-68706) 1290 Infinity TCC User Manual...
  • Page 153 Ferrule front included in kit SST hex head nut with PEEK ferrule, 6/pk (p/n 5067-1540), only pressure tight up to 600 bar included in kit Fitting screw long (p/n 5065-4454) Figure 43 TCC Heater Fittings 1290 Infinity TCC User Manual...
  • Page 154 Parts and Materials for Maintenance Heater and Cooling Devices Figure 44 Heater Devices for G1316C 1290 Infinity TCC User Manual...

  • Page 155: Column Switching Valve 8 Position-9 Port

    8 pos/9 port valve head low pressure (400 bar) 1535-4857 Stator screws 5067-4112 Stator head 3, 4 5067-4113 Stator face/rotor seal 400 bar 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 45 Column Switching Valve Parts (5067-4108) 1290 Infinity TCC User Manual...

  • Page 156: Pos/6 Port Ultra High Pressure Valve Head

    Item p/n Description 5067-4117 2 pos/6 port ultra high pressure (1200 bar) valve head 5068-0006 Stator head 5068-0008 Rotor seal 1535-4857 Stator screws 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 46 Column Switching Valve Parts (5067-4117) 1290 Infinity TCC User Manual...

  • Page 157: 2Pos/10Port Ultra High Pressure Valve Head

    Item p/n Description 5067-4118 2 pos/10 port ultra high pressure (1200 bar) valve head 5068-0011 Stator head 5068-0012 Rotor seal 5068-0019 Stator screws 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 47 Column Switching Valve Parts (5067-4118) 1290 Infinity TCC User Manual...

  • Page 158: 8Pos/9Port Ultra High Pressure Valve Head

    Item p/n Description 5067-4121 8 pos/9 port valve head high pressure (1200 bar) 1535-4857 Stator screws 5068-0001 Stator head 5068-0002 Rotor seal 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 48 Column Switching Valve Parts (5067-4121) 1290 Infinity TCC User Manual...

  • Page 159: 2Pos/6 Port Valve Head 600 Bar

    Description 5067-4137 Valve Head 2 Postion / 6 Port, 600 bar 5068-006 Stator screws, 10/Pk 5068-0006 Stator head 0101-1409 Rotor Seal, PEEK 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 49 Column Switching Valve Parts (5067-4137) 1290 Infinity TCC User Manual...

  • Page 160: 2Pos/10 Port Valve Head 600 Bar

    5067-4144 Micro Valve Head 2 Position / 10 Port, 600 bar 5068-0054 Stator screws, 10/Pk 0101-1421 Stator Head 0101-1415 Rotor Seal, PEEK 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 50 Column Switching Valve Parts (5067-4144) 1290 Infinity TCC User Manual...

  • Page 161: 8Pos/9 Port Valve Head 600 Bar

    8pos/9 port valve head 600 bar Item p/n Description 5067-4107 Valve Head 8 Position/9 Port, 600 bar 1535-4857 Stator screws 5068-0001 Stator head 5067-4111 Rotor Seal 1535-4045 Bearing Ring, (Qty 1, replacement) Figure 51 Column Switching Valve Parts (5067-4107) 1290 Infinity TCC User Manual...

  • Page 162: Accessory Kits

    (0.17 mm i.d., 180 mm) and three capillaries (0.17 mm i.d., 90 mm) G1316-87321 Capillary column-heat exchanger 115 mm lg, 0.17 mm i.d. G1316-87323 Capillary column-heat exchanger 170 mm lg, 0.17 mm i.d. 1290 Infinity TCC User Manual...

  • Page 163: G1316C Capillary System Kit

    Flexible tubing, 280 mm G1156-22401 Fitting Screw long G1316-68706 Fitting holder assy, includes following items: Fitting fork, fitting clip screws (pack of 4) G1316-89200 Carrier for heat exchanger G1316-80003 Heater long-down (0.12 mm i.d., 1.6 µL internal volume) 1290 Infinity TCC User Manual...
  • Page 164 TUBING, FLEX (p/n 0890-1713) Valve to waste Heater long-up (0.12 mm i.d., 1.6 µL internal volume) (p/n G1316-80002) Heater long-down (0.12 mm i.d., 1.6 µL internal volume) (p/n G1316-80003) Carrier for heat exchanger (p/n G1316-89200) 1290 Infinity TCC User Manual...

  • Page 165: Accessories

    You will need this kit to prepare the TCC for transportation. Transportation Lock Kit (p/n G1316-67001) Description G1316-03701 Lock plate 2680-0128 Screw M4 0515-0897 Screw M3x8 (pack of 4) Spring Washer G1316-40002 Transportation valve head 1290 Infinity TCC User Manual...
  • Page 166 Parts and Materials for Maintenance Accessory Kits 1290 Infinity TCC User Manual...

  • Page 167: Identifying Cables

    1290 Infinity TCC User Manual Identifying Cables Cable Overview Analog cables Remote Cables BCD Cables CAN Cable RS-232 Cable Kit Agilent Module to Printer This chapter summarizes information on all cables. Agilent Technologies...

  • Page 168: Cable Overview

    Identifying Cables Cable Overview Cable Overview Never use cables other than the ones supplied by Agilent Technologies to ensure proper N O T E functionality and compliance with safety or EMC regulations. Analog cables Description 35900-60750 Agilent module to 3394/6 integrators...
  • Page 169 It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity TCC User Manual...

  • Page 170: Analog Cables

    The other end depends on the instrument to which connection is being made. Agilent Module to 3394/6 Integrators p/n 35900-60750 Pin 3394/6 Pin Agilent Signal Name module Not connected Shield Analog - Center Analog + 1290 Infinity TCC User Manual...
  • Page 171 Pin BNC Pin Agilent Signal Name module Shield Shield Analog - Center Center Analog + Agilent Module to General Purpose p/n 01046-60105 Pin 3394/6 Pin Agilent Signal Name module Not connected Black Analog - Analog + 1290 Infinity TCC User Manual...

  • Page 172: Remote Cables

    Identifying Cables Remote Cables Remote Cables One end of these cables provides a Agilent Technologies APG (Analytical Products Group) remote connector to be connected to Agilent modules. The other end depends on the instrument to be connected to. Agilent Module to 3396A Integrators...
  • Page 173 5 - Pink Not connected 6 - Yellow 6 - Yellow Power on High 7 - Red 7 - Red Ready High 8 - Green 8 - Green Stop 9 - Black 9 - Black Start request 1290 Infinity TCC User Manual...
  • Page 174 Prepare run 3 - Gray Start 4 - Blue Shut down 5 - Pink Not connected 6 - Yellow Power on High 7 - Red Ready High 8 - Green Stop 9 - Black Start request 1290 Infinity TCC User Manual...

  • Page 175: Bcd Cables

    BCD 4 Black BCD 0 Orange BCD 3 BCD 2 Brown BCD 1 Gray Digital ground Gray Gray/pink BCD 11 Red/blue BCD 10 White/green BCD 9 Brown/green BCD 8 not connected not connected + 5 V 1290 Infinity TCC User Manual...
  • Page 176 Agilent Module to 3396 Integrators p/n 03396-60560 Pin 3396 Pin Agilent Signal Name BCD Digit module BCD 5 BCD 7 BCD 6 BCD 4 BCD0 BCD 3 BCD 2 BCD 1 Digital ground + 5 V 1290 Infinity TCC User Manual...

  • Page 177: Can Cable

    CAN cable, Agilent module to module, 1 m LAN Cables Description 5023-0203 Cross-over network cable, shielded, 3 m (for point to point connection) 5023-0202 Twisted pair network cable, shielded, 7 m (for point to point connection) 1290 Infinity TCC User Manual...

  • Page 178: Rs-232 Cable Kit

    It's also called "Null Modem Cable" with full handshaking where the wiring is made between pins 1-1, 2-3, 3-2, 4-6, 5-5, 6-4, 7-8, 8-7, 9-9. 5181-1561 RS-232 cable, 8 m 1290 Infinity TCC User Manual...

  • Page 179: Agilent Module To Printer

    Agilent Module to Printer Agilent Module to Printer Description 5181-1529 Cable Printer Serial & Parallel, is a SUB-D 9 pin female vs. Centronics connector on the other end (NOT FOR FW UPDATE). For use with G1323 Control Module. 1290 Infinity TCC User Manual...
  • Page 180 Identifying Cables Agilent Module to Printer 1290 Infinity TCC User Manual...

  • Page 181: Appendix

    1290 Infinity TCC User Manual Appendix General Safety Information The Waste Electrical and Electronic Equipment (WEEE) Directive (2002-96-EC) Lithium Batteries Information Radio Interference Sound Emission Solvent Information Agilent Technologies on Internet This chapter provides addition information on safety, legal and web.

  • Page 182: General Safety Information

    C A U T I O N alerts you to situations that could cause loss of data, or damage of equipment. ➔ Do not proceed beyond a caution until you have fully understood and met the indicated conditions. 1290 Infinity TCC User Manual...
  • Page 183 Make sure that only fuses with the required rated current and of the specified type (normal blow, time delay, and so on) are used for replacement. The use of repaired fuses and the short-circuiting of fuse holders must be avoided. 1290 Infinity TCC User Manual...
  • Page 184 When working with solvents please observe appropriate safety procedures (e.g. goggles, safety gloves and protective clothing) as described in the material handling and safety data sheet by the solvent vendor, especially when toxic or hazardous solvents are used. 1290 Infinity TCC User Manual...

  • Page 185: The Waste Electrical And Electronic Equipment (Weee) Directive (2002-96-Ec)

    With reference to the equipment types in the WEEE Directive Annex I, this product is classed as a Monitoring and Control Instrumentation product. Do not dispose off in domestic household waste N O T E To return unwanted products, contact your local Agilent office, or see www.agilent.com more information. 1290 Infinity TCC User Manual...

  • Page 186: Lithium Batteries Information

    Ved udskiftning benyttes kun batteri som anbefalt av apparatfabrikanten. ➔ Brukt batteri returneres appararleverandoren. Bij dit apparaat zijn batterijen geleverd. Wanneer deze leeg zijn, moet u ze niet weggooien N O T E maar inleveren als KCA. 1290 Infinity TCC User Manual...

  • Page 187: Radio Interference

    Appendix Radio Interference Radio Interference Cables supplied by Agilent Technologies are screened to provide optimized protection against radio interference. All cables are in compliance with safety or EMC regulations. Test and Measurement If test and measurement equipment is operated with unscreened cables, or...

  • Page 188: Sound Emission

    This product has a sound pressure emission (at the operator position) < 70 dB. • Sound Pressure Lp < 70 dB (A) • At Operator Position • Normal Operation • According to ISO 7779:1988/EN 27779/1991 (Type Test) 1290 Infinity TCC User Manual...

  • Page 189: Solvent Information

    Chromatographic grade ethers, which can contain peroxides (for example, THF, dioxane, di-isopropylether) such ethers should be filtered through dry aluminium oxide which adsorbs the peroxides, • Solvents containing strong complexing agents (e.g. EDTA), • Mixtures of carbon tetrachloride with 2-propanol or THF. 1290 Infinity TCC User Manual...

  • Page 190: Agilent Technologies On Internet

    Agilent Technologies on Internet For the latest information on products and services visit our worldwide web site on the Internet at: http://www.agilent.com Select Products/Chemical Analysis It will provide also the latest firmware of the modules for download. 1290 Infinity TCC User Manual...
  • Page 191 1290 Infinity TCC User Manual...
  • Page 192 RS-232C bench space cable capillaries and waste tubings 1290 Infinity TCC User Manual...
  • Page 193 WEEE directive status indicator weight synchronization lost system overview installation temperature verification principle temperature calibration description problems procedure temperature verification 1290 Infinity TCC User Manual...
  • Page 194 In This Book The manual contains technical reference information about the Agilent 1290 Infinity Thermostatted Column Compartment. This manual describes the following: • introduction and specifications, • installation, • using and optimizing, • troubleshooting and diagnose, • maintenance, • parts identification, •...

Table of Contents