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Thermo Scientific ISQ EC Manuals
Manuals and User Guides for Thermo Scientific ISQ EC. We have
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Thermo Scientific ISQ EC manuals available for free PDF download: Operating Manual, Preinstallation Manual
Thermo Scientific ISQ EC Operating Manual (232 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 5.84 MB
Table of Contents
Table of Contents
5
Contacting Us
3
Table of Contents
5
1 Using this Manual
9
About this Manual
10
Conventions
11
Safety Messages
11
Special Notices and Informational Notes
11
Typographical Conventions
12
Reference Documentation
14
2 Safety
16
Safety Symbols and Signal Words
17
Safety Symbols and Signal Words in this Manual (Symboles de Sécurité Et Mentions D'avertissement Utilisés Dans Ce Manuel)
17
Observing this Manual
19
Safety Symbols on the Instrument
19
Intended Use
22
Safety Precautions
23
General Safety Information (Consignes Générales de Sécurité)
23
Qualification of the Personnel
24
Personal Protective Equipment
26
Electrical Safety Precautions
28
General Residual Hazards
29
Solvent and Additive Information
37
Compliance Information
38
3 Instrument Overview
39
Mass Spectrometer Operating Principle
40
Overview of an LC/MS or IC/MS Analysis
41
Software Operation
43
4 Unpacking
44
Unpacking
45
Scope of Delivery
49
5 Installation
50
Safety Guidelines for Installation
51
Installing the Mass Spectrometer
53
Site Requirements
55
Workbench
55
Power Considerations
55
Power Cord
57
Condensation
62
Operating Conditions
62
Gas Ventilation
63
Nitrogen Gas Supply
64
Unpacking the Instrument
67
Setting up the Hardware
68
Installing the Foreline Pump
68
Installing the Oil Mist Filter
82
Adding Oil to the Foreline Pump
92
Installing the Solvent Trap
96
Installing the Source Housing Drain Insert and Sweep Cone
98
Switching between HESI and APCI Modes on the ISQ EM Source Housing
103
Installing the Internal Calibration Solution
104
Connecting the IC or LC to the MS Inlet
106
Flushing the Calibration Solution
108
Connecting the System to the PC
110
Summary of Hardware Installation
113
Powering up the System
115
6 Operation
117
Introduction to this Chapter
118
Safety Guidelines for Operation
119
MS Instrument Overview
121
Configuring the MS in Chromeleon
123
User Operation
136
Chromeleon User Interface
136
Running Your First Sample
143
Getting Started
143
Method Editor-Source Settings, Easy View
144
Method Editor-Source Settings, Advanced View
146
Method Editor-Scan Settings
148
Method Editor-Component Mode
150
Method Editor-Scan Mode
152
Method Development
154
MS Instrument Data Signal Channels
156
Custom Variables
156
Chromeleon Audit Trail
156
Shutting down the MS Instrument
157
Short-Term Standby
157
Long-Term Shutdown
158
Venting the Mass Spectrometer
162
Remote Start Cable
164
Vanquish HPLC-Autosampler
164
Ultimate 3000
165
AS-AP Autosampler
165
Integrion Autosampler (no AS-AP)
165
7 Maintenance and Service
167
Introduction to Maintenance and Service
168
Safety Guidelines for Maintenance and Service
169
General Rules for Maintenance and Service
172
Routine and Preventive Maintenance
173
Maintenance Plan
173
Preventive Maintenance Schedule
174
Cleaning or Decontaminating the Instrument
174
Replacing the ESI Probe Capillaries for the ISQ EC and ISQ EM
176
Replacing the APCI Probe Capillaries for the ISQ EM
181
Replacing the APCI Needle
189
Cleaning the Front Optics
190
Removing the Instrument from the System Stack
200
Updating the Mass Spectrometer Firmware
202
8 Troubleshooting
205
General Information about Troubleshooting
206
Troubleshooting Problems with Autotune
208
Troubleshooting Leaky Source Gases
210
9 Specifications
211
Physical Specifications
212
10 Accessories, Consumables and Replacement Parts
213
General Information
214
Ship Kit
215
Accessories, Consumables and Replacement Parts Item
216
Replacement Parts
217
Driver, Phillips
218
Driver, T25
218
Tool, Ion Transfer Tube Removal
218
Tool, Lens 0 Removal
218
Tubing Cutter, 1/16 PEEK
218
Tubing Cutter, 1/8 Plastic
218
Tubing Cutter, Large Hose
218
Hose Adapter, NW25 to 1 in
220
Hose Clamp, 21-38 MM 1R4120-0003
220
O-Ring with Centering Ring, NW25
220
Oil Mist Filter (Connects to Oil Return Kit) 1R76505-0037
220
Oil Return Kit (Connects to Oil Mist Filter) 1R76505-0022
220
Vacuum Hose Clamp NW25
220
11 Appendix
221
Compliance Information
222
Declarations of Conformity
222
WEEE Compliance
223
FCC Compliance
224
Regulatory Compliance
225
Low Voltage Safety Compliance
225
Notice on Lifting and Handling of Thermo Scientific Instruments
225
Notice on the Proper Use of Thermo Scientific Instruments
225
Notice on the Susceptibility to Electromagnetic Transmissions
225
Manual Release History
227
12 Index
228
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Thermo Scientific ISQ EC Preinstallation Manual (56 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 1.25 MB
Table of Contents
Contacting Us
3
Table of Contents
5
1 Using this Manual
7
About this Manual
8
Conventions
9
Safety Messages
9
Special Notices and Informational Notes
9
Typographical Conventions
10
Reference Documentation
12
2 Safety
14
Safety Symbols and Signal Words
15
Safety Symbols and Signal Words in this Manual
15
Observing this Manual
16
Safety Symbols on the Detector
16
Intended Use
18
Safety Precautions
19
General Safety Information
19
Qualification of the Personnel
19
Personal Protective Equipment
20
Electrical Safety Precautions
21
General Residual Hazards
21
Solvent and Additive Information
26
Compliance Information
27
3 Site Preparation
28
Entrance Requirements
29
Workbench and Space Requirements
30
Lighting Requirements
34
Power Requirements
35
Environmental Requirements
40
Gas Requirements
42
Nitrogen Gas Supply
42
Exhaust Requirements
45
Foreline Pump Exhaust
45
Ion Source Exhaust
45
Solvents and Sample Preparation
47
Standard Installation
47
Receiving Requirements
48
3.10 What Happens Next
49
4 Appendix
50
Compliance Information
51
Declarations of Conformity
51
WEEE Compliance
52
FCC Compliance
53
Regulatory Compliance
54
Low Voltage Safety Compliance
54
Notice on Lifting and Handling of Thermo Scientific Instruments
54
Notice on the Proper Use of Thermo Scientific Instruments
54
Notice on the Susceptibility to Electromagnetic Transmissions
54
Manual Release History
56
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