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Thermo Scientific ISQ manual available for free PDF download: User Manual
Thermo Scientific ISQ User Manual (152 pages)
Brand:
Thermo Scientific
| Category:
Laboratory Equipment
| Size: 9 MB
Table of Contents
Table of Contents
3
About Your System
9
Preface
9
Related Documentation
10
Safety and Special Notices
11
Safety Symbols and Signal Words
11
Special Notices
11
System Requirements
11
Hydrogen Safety Precautions
13
Using Hydrogen with ISQ
15
Hydrogen Connection Guidelines
16
Purchasing Hydrogen
17
Properly Storing Hydrogen
18
Hydrogen Safety Codes, Standards and References
19
Biological Hazard Warning Note
20
Hazardous Substances Precautions
20
Contacting Us
21
Venting Toxic Gases
21
Checking Power to the System
23
Confirming Your GC/MS System Is Working
23
Verifying the Carrier Gas Flow Rate
24
Checking Your Carrier Gas Tank Pressure
25
Checking the Vacuum and Temperature
26
Chapter 2 Changing the Column
27
Replacing the Factory Installed Column
29
Connecting the Column to the Transfer Line
35
Tuning the ISQ
45
Accessing ISQ Autotune
46
Tuning the ISQ Mass Spectrometer
46
Creating a Method
55
Creating a Method for the Autosampler
56
Creating a Method for the ISQ Mass Spectrometer
59
Creating a Method for the GC
65
Creating a Method for the TRACE 1300 or TRACE 1310
65
Creating a Method for the TRACE GC Ultra
72
Creating a Method for the FOCUS GC
76
Chapter 5 Running a Sample
83
Preparing Your Sample
83
Running a Sequence
84
Exploring Your Data
97
Optimizing Your Method
107
Changing the Chromatographic Separation
107
Finding the Best Way to Make an Injection
108
Improving the Way You Prepare Samples
108
Changing the Scan Rate
108
Narrowing the Mass Range
108
Adjusting the Transfer Line Temperature
109
Modifying an Automatic Tune
110
Troubleshooting
125
No Ions Present in Scans
126
Checking the ISQ System Firmware
126
How to Know When Your System Needs Maintenance
129
Investigating Baseline Issues
130
Investigating Peak Issues
132
Investigating Results Issues
135
Reconfiguring Your Instrument
137
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