Appendix F: Filtration Efficiency Test Results - Labconco Paramount 69632 Series User Manual

A p p e n
A p p e n
F i l t r a t i
F i l t r a t i
Ductless enclosures require filtration efficiency testing to validate performance.
Independent testing, conducted by a consultant and the University of Kansas,
concluded the tested filtration efficiency for acetone, ethanol, isopropyl alcohol,
toluene and hydrochloric acid was excellent. Filtration capacity is defined as a
percentage of the chemical mass adsorbed compared to the total carbon filter weight.
Utilizing analytical instrumentation, the organic vapor filter and acid vapor filter were
both independently tested for filtration efficiency. The solvents and acids listed below
were evaporated at both low and high evaporation rates. Low evaporation rates are
typical in ductless enclosures in order to maximize useful carbon filter life. Both
ethanol and acetone were specifically tested at low evaporation rates of 14ppm and
22ppm, respectively, to simulate real laboratory conditions of chemicals with low
filter capacities. High evaporation rates of 100-462ppm were used for most of the
organic solvents and mineral acid to accelerate the testing process of chemicals with
higher filtration capacity and determine filter saturation and chemical breakthrough.
The testing was designed to assess the filtration efficiency of the filters. As suggested
by carbon manufacturers, carbon filters usually have a 30 percent to 40 percent
filtration capacity of theoretical values for organic chemicals with higher carbon
affinity. The test results show a filtration efficiency of 33-39 percent for chemicals
with higher affinity for organic vapor carbon and directly in line with the 30-40
percent as suggested by carbon manufacturers. Since ethanol has very low filter
capacity, it is not alarming that the filtration efficiency is 17-19 percent; the test
results prove the practical matter of using low quantities of ethanol or any other
chemical with very lower filter capacity. The mineral acid filtration efficiency of
hydrochloric acid approached 83 percent of theoretical value and is attributed to the
chemisorption process of the treated acid filters. To conclude, the filtration efficiency
test data and charts indicate the ductless enclosure filtration was in line with carbon
manufacturer expectations and will provide a safe working environment for
controlled environments.
Exposure Evaporation No. of
Chemical Limit
Acetone 250 ppm 22 ppm
Ethanol or 1000 ppm 14 ppm
Ethyl Alcohol 1000 ppm 206 ppm
Isopropyl Alcohol 400 ppm 462 ppm
Toluene 100 ppm 155 ppm
37% Hydrochloric 5 ppm 100 ppm
Acid
70
d i x F :
d i x F :
o n E f f i c i e
o n E f f i c i e
3' Paramount
Rate Filters Carbon Filter Mass
4 13500 grams
4 13500 grams
4 13500 grams
4 13500 grams
4 13500 grams
4 18000 grams
of treated carbon
n c y T e s t R
n c y T e s t
Chemical Mass Detected Saturation
Adsorbed Breakthrough Concentration Tested Theoretical Efficiency
153 grams 1-2 ppm
32 grams 6-9 ppm
148 grams 6-9 ppm
824 grams 8-11 ppm
1317 grams 0.5-1 ppm
2529 grams 0.5-1 ppm
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e s u l t s
R e s u l t s
Filtration Capacity
1.1% 2.8%
0.3% 1.6%
1.1% 6.3%
6.1% 17.7%
9.8% 29.7%
14.1% 17.0%
Filtration
39%
19%
17%
34%
33%
83%