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TA Instruments Manuals
Measuring Instruments
Q20
Getting started manual
TA Instruments Q20 Getting Started Manual
Differential scanning calorimeter
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Contents
Table of Contents
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Table of Contents
Important: TA Instruments Manual Supplement
Table of Contents
Notes, Cautions, and Warnings
Regulatory Compliance
Safety Standards
Electromagnetic Compatibility Standards
Safety
Instrument Symbols
Electrical Safety
Handling Liquid Nitrogen
Thermal Safety
Lifting the Instrument
Chapter 1: Introducing the DSC
Overview
DSC System Components
DSC Cell
Cooling Accessories
Finned Air Cooling System (FACS)
Refrigerated Cooling System (RCS)
Quench Cooler
Liquid Nitrogen Cooling System (LNCS)
The DSC Q2000/Q200 Touch Screen
Primary Function Keys
Control Menu
Display Touch Screen Options
The DSC Q1000/Q100 Touch Screens
Primary Function Keys
DSC Control Menu Keys
Display Menu Keys
DSC Auto Q20/Q20/Q10 Keypad
Options and Accessories
Tzero Sample Encapsulating Press
DSC Autosampler
Photocalorimeter Accessory (PCA)
DSC Pressure Cell
Instrument Specifications
DSC Instrument Characteristics
Chapter 2: Installing the DSC
Unpacking/Repacking the DSC
Installing the Instrument
Inspecting the System
Choosing a Location
Connecting Cables and Lines
Ports
Ethernet Switch Setup
Purge Lines
Cooling Gas Line
Base Purge Line
Voltage Configuration Unit
Power Switch
Power Cable
Starting the DSC
Shutting down the DSC
Installing the DSC Cooling Accessories
Installing the Finned Air Cooling System
Installing the Quench Coolers
Quench Cool Accessory for FACS
Quench Cooler
Installation of Additional Items
Installing the Manual Lids
Installing the Autosampler Tray and Dust Cover
Chapter 3: Use, Maintenance, & Diagnostics
Using the DSC
Before You Begin
Calibrating the DSC
Tzero TM
Baseline Slope and Offset Calibration
Enthalpy (Cell) Constant Calibration
Temperature Calibration
Heat Capacity (Q2000/Q1000) Calibration
Heat Capacity (MDSC ® ) Calibration
Pressure Calibration
Autosampler Calibration
Q2000/Q200/Auto Q20 Autosampler Calibration
Q1000/Q100 Autosampler Calibration
Running a DSC Experiment
Experimental Procedure
Loading the Sample
Starting an Experiment
Stopping an Experiment
Maintaining the Instrument
Cleaning the Touch Screen
Cleaning a Contaminated Cell
Cleaning a Contaminated QDSC Standard Cell
Burning off Contamination in a DSC Cell with a FACS Installed
Burning off Contamination in a DSC Cell with an RCS or LNCS
Removing a DSC Q2000/Q1000 Cell
Installing a Cell
Replacing Fuses
Replacing the DSC Fuses
Replacement Parts
Fuses, Cords, and Cables
DSC Cells, Lids, and Accessories
Autosampler Accessories
Tzero Sample Encapsulation Press
DSC Sample Pans, Lids, and Accessories
Calibration/Reference Materials
Index
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DSC
Differential Scanning
Calorimeter
TM
Q Series
Getting Started Guide
Revision N
Issued January 2007
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Summarization of Contents
DSC Introduction and Safety
Introducing the DSC
General introduction to the Differential Scanning Calorimeter (DSC) and its function.
Safety and Compliance
Covers regulatory compliance, safety standards, instrument symbols, and hazard warnings.
DSC System Components and Cooling
DSC Cell Description
Details the DSC cell, its thermal model, and overall system components.
Cooling Accessories Overview
Introduces FACS, RCS, Quench Cooler, and LNCS for DSC temperature control.
DSC User Interfaces
Touch Screen Interfaces
Describes the Q2000/Q200 and Q1000/Q100 touch screen interfaces and keys.
DSC Auto Keypad Interface
Details the keypad interface for DSC models without a touch screen.
Installation Procedures
Instrument Installation and Setup
Covers unpacking, inspection, location selection, and initial instrument installation.
Connections and Configuration
Instructions for connecting cables, ports, purge lines, and voltage configuration.
Cooling Accessory Installation
Guides for installing FACS, Quench Coolers, and related accessories.
DSC Operation and Calibration
Using the DSC and Experiment Setup
Outlines basic usage, preparation steps, and calibration requirements before experiments.
DSC Calibration Procedures
Explains various DSC calibration types like Tzero, baseline, enthalpy, temperature, and heat capacity.
Running and Stopping Experiments
Details the procedures for loading samples, starting, and stopping DSC experiments.
Maintenance and Replacement Parts
Instrument Maintenance
Covers cleaning, contamination removal, cell maintenance, and fuse replacement.
Replacement Parts Catalog
Lists available replacement parts including fuses, cables, cells, pans, and calibration materials.
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