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Related Manuals for Radleys Reactor-Ready Duo
Summary of Contents for Radleys Reactor-Ready Duo
- Page 1 February 2023 Issue 7 Instructions Reactor-Ready Duo ™ Lab Reactor Patent Pending Your local distributor Radleys, Shire Hill, Saffron Walden, Essex, CB11 3AZ. United Kingdom. Tel: +44 1799 513320 Fax: +44 1799 513283 Email: sales@radleys.com Web: www.radleys.com...
- Page 2 Page 21 8. Set-Up and Operation - Continued 8.20 Disconnecting the thermoregulator Page 4 5. Products and Accessories 8.21 Use of Reactor-Ready Duo Hose Tidies Page 5 5. Products and Accessories - Continued Page 22 8. Set-Up and Operation - Continued 8.22 Static...
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Page 3: Warranty
2. Warranty Reactor-Ready Duo includes one year full parts and labour warranty from date of original purchase. Warranty will only be valid if a completed Warranty Email Back is returned within 1 month of date of purchase (see last page). -
Page 4: Safety Information
• Reactor-Ready Duo can be used with a recirculating fluid at a temperature of up to 190˚C, or down to -60°C without damage to the unit. Careful inspection of all fluid connections to Reactor-Ready Duo should be regularly performed when operating at these temperatures. -
Page 5: Products And Accessories
How to order Reactor-Ready Duo Important: The support collar is required to support vessels within the quick-release clamp. Two collars are supplied with each Reactor-Ready Duo Core System, however extra collars can be purchased using the above Cat. No. 1. Select the Reactor-Ready Duo Core: RR213000. - Page 6 Ministat 230-CC NR Important: For custom glassware please contact your local distributor or call our sales HB1030.0001.04 Petite Fleur team on Tel: +44-1799-513320 or E-mail: sales@radleys.co.uk HB1030.0001.04ET Petite Fleur with 4 Litre Expansion Tank RR139005 Condenser Liebig 250mm B29 + GL14 + fittings HB1000.0001.05...
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Page 7: Component Guide
Reactor-Ready Duo - Lab Reactor 6. Component Guide Reactor-Ready Duo Core System Adjustable Feet HDPE Drip Tray Aluminium Base Support Rod Bosses Support Rods Hose Tidies Safety Stop Collars Vessel Support Collars Vessel Support Clamps 10. T-Beam Support Brace 11. Stirrer Support Bosses 12. - Page 8 Pt100 PTFE Temperature Probe PTFE Temperature Probe Adapter E. PTFE Temperature Probe Adapter Vessel Compatibility Tables Use the tables below to ensure Reactor-Ready Duo will accept your chosen vessels in parallel... Standard Vessel, Single Jacketed Standard Vessel, Vacuum Jacketed 250ml...
- Page 9 Reactor-Ready Duo - Lab Reactor 7. Quick Start Guide 7.1 Identify a clear unobstructed site within your fume- hood. You will require a power supply for your thermo- regulator/s and for your overhead stirrers. Reactor- Ready Duo should not be moved after assembly so take care to locate it in its final position.
- Page 10 Reactor-Ready Duo - Lab Reactor 7. Quick Start Guide - Continued 7.10 Position the Stirrer Guide in the central lid port and 7.11 7.10 hand tighten the red (Rodaviss) screw cap fitting to secure. Slide the stirrer shaft into the Stirrer Guide...
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Page 11: Setup And Operation
5 feet are squarely positioned. Check that all feet are contacting the fumehood surface and that the Reactor-Ready Duo unit is level. Adjustments can be made to individual feet by screwing in or out to achieve this. Locate the Drip Tray in the base. - Page 12 Important, Important, Important, Important, 8.4 Assembling the Manifolds 8.4.1 Reactor-Ready Duo offers a choice of configurations for circulating manifolds, dependant on the application. The single circulator manifold configuration allows both jacketed reaction vessels to be controlled from a single thermoregulator. Thermofluid flow is split equally for each vessel. Both vessels will be controlled at the same temperature and temperature profile.
- Page 13 Reactor-Ready Duo - Lab Reactor 8. Set-Up and Operation - Continued 8.5 Assembling Single Circulator Manifolds 8.5.1 8.5.1 For single circulator manifold configuration slide the Lower Supply Manifold down the central Support Rod. Tighten the locking knob to secure the Manifold to the Support Rod.
- Page 14 Reactor-Ready Duo - Lab Reactor 8. Set-Up and Operation - Continued 8.6 Assembling Double Circulator Manifolds 8.6.2 8.6.3 8.6.1 For double circulator manifold configuration firstly identify each of the 4 separate manifolds. 8.6.2 A. Left Hand Upper Return Manifold with Vent Valve B.
- Page 15 8.7. Locating the support braces 8.7.1 8.7.1 The Reactor-Ready Duo core includes four Safety Stop Collars that limit the downward movement of the Stirrer Support Boss and Vessel Support Clamp. One collar is positioned and secured under each of the two Stirrer Support Bosses and two collars under the Vessel Support Clamp.
- Page 16 100ml to 5000ml in either single jacket or vacuum jacket format. Important Note - Reactor-Ready Duo clamp assembly is NOT designed to accept Important, Important, reactors from other manufacturers. The vessel neck, flange and lid geometry are...
- Page 17 Reactor-Ready Duo - Lab Reactor 8. Set-Up and Operation - Continued 8.9. Assembling the vessel lid, stirrer guide and probe 8.9.2 8.9.1 Before attaching the lid to the reaction vessel the stirrer assembly must be mounted in the lid. 8.9.2 Position the Stirrer Guide in the central B24 lid port. Hand tighten the central red (Rodaviss) screw cap to secure.
- Page 18 Reactor-Ready Duo - Lab Reactor 8. Set-Up and Operation - Continued 8.10 Assembling the thermofluid hoses 8.10.1.A 8.10.1.A 8.10.A Single Circulator Manifold configuration 8.10.1.A Using the Single Circulator Manifold configuration (as set-up in 8.5), attach a Quick Release insulated hose to each of the ports on either side of the Lower Supply Manifold.
- Page 19 8.12.10 Switch on power to the overhead stirrer, and start stirrer motor slowly, to check that smooth coupling of stirrer pins has been achieved. The maximum operating speed for Reactor-Ready Duo is 500rpm for continuous operation and 800rpm for short periods.
- Page 20 8.15.1 8.15 Connecting the thermoregulator 8.15.1 The Reactor-Ready Duo manifolds are supplied with M24 fittings as standard. Please check the fittings on the hoses you are using and if they are not M24, then a suitable adapter will be required (please see Page 5 for a full list of suitable adapters).
- Page 21 Closed 8.19. Draining thermofluid from Reactor-Ready Duo 8.19.1 If the reaction vessel needs to be removed from the Reactor-Ready Duo framework for cleaning, or to replace it with another vessel, the thermofluid in the jacket must first be drained. 8.19.2 Ensure that the thermoregulator is switched off and thermofluid allowed to cool to a safe temperature.
- Page 22 The hose connector should be sealed at this point with the use of a red (Rodaviss) sealing cap (supplied with the hose) or with Reactor-Ready Duo Hose Tidies to prevent dripping of thermofluid residues.
- Page 23 Reactor-Ready Pilot - Lab Reactor 8. Set-Up and Operation - Continued 8.22 Static Static can be generated in any circulating fluid system. This is not a ‘fault’ with the equipment, but an unfortunate and accepted occasional side effect of the methodology. The following is provided for your information only and is not intended to be a concise guide of necessary actions in the case of static build up.
- Page 24 50K. 9.4 Temperature Range Standard jacketed vessels with the Radleys V4 Zero Dead Space Stopcock, are suitable for use from -60°C to +190°C. Important Note - At temperatures below -50°C there may be some weeping from the Important, Important, stopcock.
- Page 25 9.8 V4 Zero Dead Space Stopcock (V4 ZDS) 9.8.1 All Reactor-Ready Duo Vessels feature the V4 ZDS. This zero dead volume stopcock minimises the dead space at the bottom of the reaction vessel during reactions. The stopcock also minimises hold up of reaction contents after draining the reactor.
- Page 26 Important, Important, Important, Important, Important, Important, Important Note - The FEP O-rings may not suit all applications, therefore alternative Important, Important, O-ring seals are available. Please contact Radleys for technical advice. Important, Important, Important, Important, Important, Important, Important, Important, Important, Important, Warning - Risk of injury due to broken glass.
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Page 27: General Specifications
800rpm for short periods 11. Routine Maintenance 10.1 To maintain your Reactor-Ready Duo system in prime condition it is important that care is taken to check all moving parts and seals regularly. 10.2 Moving parts should be kept clean and free from any obstructions or surface contamination. - Page 28 Page 27...
- Page 29 Warranty – Email Back sales@radleys.com To qualify for your warranty please complete, scan and email this form to Radleys Product Name/Model Product Batch or Serial No. (If shown) Date of purchase Supplier’s name and address Organisation name First name Last name...