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Analytik Jena SPECORD 200 Manual

Uv vis spectrophotometer
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SPECORD
PC
200 / 205 / 210 / 250
UV VIS Spectrophotometer

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Summary of Contents for Analytik Jena SPECORD 200

  • Page 1 ® SPECORD 200 / 205 / 210 / 250 UV VIS Spectrophotometer...
  • Page 2 + 49 (0) 3641 77 74 07 Fax: + 49 (0) 3641 77 74 49 E-Mail: service@analytik-jena.de General information about Analytik Jena AG on the internet: http://www.analytik-jena.de Copyrights and Trademarks Microsoft, Windows XP, Windows NT, Windows 2000, MS Excel are registered trademarks of Microsoft Corp.

  • Page 3: Table Of Contents

    Changing the deuterium lamp ................35 8.3.4 Changing the halogen lamp ................37 Changing the desiccator ..............39 Changing fuses ...................39 Disposal .................41 Index to Illustrations .............43 Index to Overviews............43 ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 1 Analytik Jena AG...

  • Page 5: Introduction

    ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 3 Analytik Jena AG...

  • Page 6: Notes On The User's Manual

    • Every illustration has its own caption. • Steps of operation are numbered. • Cross-references are marked by an arrow (e.g. →Intended use of the SPECORD p.3) ® Page 4 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 7: Safety Notes

    For that, the knowledge of the information provided by this manual is indispensable and taken for granted. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 5 Analytik Jena AG...
  • Page 8 Avoid exposing the sample compartment to strongly corrosive substances! For the analysis of such samples, use vapor-tight stoppered cells. After the measurement, do not leave the samples unnecessarily long in the sample compartment of the device! ® Page 6 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...
  • Page 9 • DIN EN 61010-1 (IEC 1010-1) • 73/23/EC • 89/336/EC. ® The SPECORD meets the requirements as per Protection Type IP 20. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 7 Analytik Jena AG...

  • Page 11: Technical Data Of The Spectrophotometers

    ≤ 0.05%T Baseline noise at 500nm ≤ 0.00015 (RMS) Long-term stability at 500nm ≤ ± 0.001 Scanning speed up to 6000nm/min allowing for tolerances of used standard ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 9 Analytik Jena AG...
  • Page 12 0.5; 1; 2; 4 nm 0.5; 1; 2; 4 nm bandwidth Toluene / hexane > 2.1 > 1.7 > 2.1 > 2.1 resolution ® Overview 3-1 Technical data of SPECORD ® Page 10 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 13: General Technical Data Of Specord

    1 x RS–232 for the connection of an external PC PC requirements for software: Pentium processor 133 MHz, 16 MB RAM, WinASPECT Windows 2000 or higher ® Overview 3-2 General technical data of SPECORD ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 11 Analytik Jena AG...

  • Page 15: Device Description And Operating Principle

    Spectrometer system The spectrometer system is protected against extraneous light and dust by cover. The desiccator regulates the humidity inside the system. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 13 Analytik Jena AG...

  • Page 16: Design Of Subassemblies

    200 / 205 / 210 Halogen lamp in protective housing E lamp compartment Reflecting mirror Toric illuminating mirror Setscrew for mirror adjustment ® Fig. 4-2 Lamp compartment of SPECORD 200/205/210 ® Page 14 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...
  • Page 17 (Fig. 4-2, 5). On the SPECORD® 250, the holographic grating of the premonochromator takes the place of the toric illuminating mirror (Fig. 4-4, 4). ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 15 Analytik Jena AG...

  • Page 18: Spectrometer System And Photometer Section

    Cell Detector Halogen lamp Quartz-coated toric mirrors Swivel mirror Toric illuminating mirror on SPECORD 200/205/210 or premonochromator grating on SPECORD 250 ® Fig. 4-4 Optical diagram of SPECORD The spectrometer system with the optical elements illustrated above – filter wheel, concave grating and slit assembly –...

  • Page 19: Sample Compartment

    Two openings in the front of the device cover (12) are provided for the aspiration tubes of the super sipper system. The illustration below shows the geometrical dimensions of the sample compartment. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 17 Analytik Jena AG...
  • Page 20 ® SPECORD Device description and operating principle Design of subassemblies Fig. 4-6 Dimensions of sample compartment ® Page 18 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 21: Installation And Transport Conditions

    For transport and storage, the following ambient conditions must be complied with: • Temperature range in transport: -40...+70 °C • Relative humidity in transport: up to 95 % ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 19 Analytik Jena AG...

  • Page 23: Installation And Start-Up

    Power ON indicator LED (green) E lamp ON indicator LED (yellow) Halogen lamp ON indicator LED (red) Fig. 6-2 Display elements on front panel ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 21 Analytik Jena AG...
  • Page 24 In normal operation, this opening should be closed with the black cover provided to prevent the entry of extraneous light, which would distort the analysis results. ® Page 22 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 25: Removing The Transport Lock

    The transport lock screw is not removed from the device, but is left in its holder in the ® SPECORD If the device must be transported again or returned for repair to Analytik Jena AG, lock the transport lock again. Releasing the transport lock Using a screwdriver turn the transport lock screw anti-clockwise as far as it will go.

  • Page 26: Connecting The Specord

    SPECORD® and the PC to power outlets that are connected to the same phase of the line power supply (multiple socket outlet, if possible). ® Page 24 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 27: Start-Up

    Activate the menu command Measurement / Set Parameters to open the window of the device driver SPECORD xxx ..® Fig. 6-8 Dialog box of SPECORD 250 device driver • Click on the Device tab. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 25 Analytik Jena AG...

  • Page 28: Switching The Device Off

    If you have finished the measurements on the SPECORD but want to analyze the ® obtained results on the PC, you can also switch off the SPECORD without shutting down the computer before. ® Page 26 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 29: Accessories

    Fill the sample into the cell up to a level of at least 20 mm. Insert the cell so it rests against the right-hand support surface of the cell holder. Correct Fig. 7-2 Inserting the cell ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 27 Analytik Jena AG...

  • Page 30: Receptacle For Cells With Turbid Samples

    After the measurement is finished, make sure to cover the cell receptacles again with the foamed-plastic caps. If you fail to do so, extraneous light might be incident on the detector and distort the results of the measurements. ® Page 28 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 31: Additional Accessories

    PTC 100, Peltier temperature-controlled cell holder • PTC 600, Peltier temperature-controlled 6-cell changer • SMA fiber connector • 8-cell changer (non-thermostatted, water-thermostatted or Peltier thermostatted) • Combination of 2 x 8-cell changers ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 29 Analytik Jena AG...

  • Page 33: Care, Maintenance, Lamp Change

    Care and maintenance ® The SPECORD is largely free of maintenance. To ensure your laboratory certification with device validation, Analytik Jena AG offers you a service/maintenance agreement. User care and maintenance is limited to the following operations: • Cleaning of sample compartment and device casing •...

  • Page 34: Changing Lamps

    Remove the flap of the lamp compartment by lifting it from below by 1 to 2 mm and then pulling it off to the left. Flap of lamp compartment Lock Fig. 8-1 Opening the flap of the lamp compartment ® Page 32 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...
  • Page 35 Knurled screw for protective cover of halogen lamp Protective cover of deuterium lamp Top part of protective cover of deuterium lamp Desiccator Fig. 8-2 Lamp compartment of SPECORD®, opened ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 33 Analytik Jena AG...
  • Page 36 Put the flap of the lamp compartment from the left straight onto the bottom of the spectrometer. Slide the flap to the right until the clips snap in. Fasten the lock by folding it back to the flap. ® Page 34 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 37: Changing The Deuterium Lamp

    Disconnect the three-pole plug-and-socket connection (4) by compressing the lateral straps and pulling the connection apart. Loosen the knurled screws (1) and pull the deuterium lamp out of its holder. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 35 Analytik Jena AG...
  • Page 38 Finally, close the flap of the lamp compartment. Note Please note that the deuterium lamp needs a warm-up of one hour after ignition to reach full thermal stability. ® Page 36 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 39: Changing The Halogen Lamp

    Rear part of protective cover of halogen lamp Knurled screws Holder of halogen lamp Adjusting screws for halogen lamp holder Halogen lamp Fig. 8-1 Changing the halogen lamp ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 37 Analytik Jena AG...
  • Page 40 200/205/210. For that, the ideal wavelength is 500 nm. Note Please note that the halogen lamp needs a warm-up of about one hour after switch on to reach full thermal stability. ® Page 38 SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Analytik Jena AG...

  • Page 41: Changing The Desiccator

    Close the fuse holder again. ® Reconnect the power cable to the power input connector of the SPECORD and the power outlet. ® Switch the SPECORD on again. ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 39 Analytik Jena AG...

  • Page 43: Disposal

    When the service life of the device is over, dispose of the device with its electronic components as electronic scrap observing the relevant regulations. ® You can also return the SPECORD to Analytik Jena AG for disposal. Please contact our Technical Service. ® SPECORD 200/205/210/250 User's Manual –...

  • Page 45: Index To Illustrations

    Changing the deuterium lamp ............... 35 Index to Overviews ® Overview 3-1 Technical data of SPECORD 200 ............10 ® Overview 3-2 General technical data of SPECORD ..........11 ® SPECORD 200/205/210/250 User's Manual – Edition 04/2005 Page 43 Analytik Jena AG...

This manual is also suitable for:

Specord 205Specord 210Specord 250

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