CETAC LSX-213 Operator's Manual
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CETAC LSX-213 Operator's Manual

Laser ablation system
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CETAC
LSX-213 Laser Ablation System
Operator's Manual
Manual Part Number 480141 Rev 2e

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Summary of Contents for CETAC LSX-213

  • Page 1 CETAC LSX-213 Laser Ablation System Operator’s Manual Manual Part Number 480141 Rev 2e...
  • Page 2 Phone (402) 733-2829 (402) 733-1932 E-mail custserv@cetac.com CETAC Technologies strives to provide the REVISIONS scientific community with an unparalleled combination of effective technology and continuing value. Modular upgrades for existing instruments will continue to be a prime consideration as designs progress.

  • Page 3: Table Of Contents

    Preparing for Installation ....................14 Ventilation ........................14 Establishing Optimal Operating Conditions ............15 Using the LSX-213 Laser Ablation System ........... 15 Creating the Lab Environment ................16 Replacing Laser Ablation System Components ..........17 Connecting the Laser Ablation System............... 18 Purchasing Supplies ....................
  • Page 4 CETAC LSX-213 Operator’s Manual Contents What’s New ..........................29 Using the DigiLaz III Software ................29 Software Overview ......................29 Installing the DigiLaz III Software ................30 ™ Running the DigiLaz III Software ................31 ™ Essential Tasks ........................32 Emergency Stop......................
  • Page 5 Laser Controller Interlocks ..................79 No Laser Output ......................80 Carrier Gas System ......................82 Low Laser Efficiency ....................81 Returning the Product to CETAC for Service ............83 Contamination ......................82 Shipping the Product ....................83 Product Warranty Statement ................. 83 Returned Product Procedures .................
  • Page 6 CETAC LSX-213 Operator’s Manual Contents CDRH Laser Product Regulations................89 Coolant ..........................90 Ventilation ........................90 Power Cord Set Requirements ................90 Power Cord Safety Maintenance ................90 Mains Disconnect ......................90 Cleaning Instructions ....................91 Operating Environment .................... 91 Avertissements en Français ....................

  • Page 7: Overview

    1 Introduction Overview The CETAC LSX-213 Laser Ablation System is the next generation UV laser ablation system from CETAC Technologies. The LSX-213 system features a high-energy 213nm laser, with improved viewing optics and an improved version of the operating software, DigiLaz™ III.

  • Page 8: Principles Of Operation

     Sample image and image map save, retrieval, and export The LSX-213 system provides a means of rapid, direct analysis of solid samples without dissolution and with minimal sample preparation. Ablation may be performed on samples of electrically conductive or non-conductive materials.

  • Page 9: Laser Ablation System

    Q-switch. The pulse repetition rate varies from 1–20 Hz. The LSX-213 sampling cell is mounted on an X-Y-Z translation stage, with a step size of 0.25 m. The translation stage provides X-Y positioning control for laser targeting on the sample and is under computer control.

  • Page 10: Laser Head And Optics

    The laser system used for the LSX-213 system uses a liquid chiller which maintains a constant temperature on the optical plate whether the unit is running at 100% or idle.

  • Page 11: Viewing Optics And Video System

    CETAC LSX-213 Operator’s Manual Chapter 1: Introduction  High intensity reflected and/or transmitted light illumination Viewing Optics and Video System  Computer controlled focusing  5X, 40 mm focal length UV achromatic lens  Computer controlled polarizers for transmitted and reflected light ...

  • Page 12: System Characteristics

     Custom designed sampling cells, oversize cell, document cell, core cell, small sample cell. Inquire about custom designs  The LSX-213 system has built in safety interlocks to disable the laser in the Laser and High Voltage Safety Features event the cover is opened or the front door is opened during operation.

  • Page 13: Who Should Use This Product-Operator Qualifications

    New versions of this manual may be available under “Service and Support” on CETAC’s Web site: www.cetac.com In addition to the LSX-213 Laser Ablation System Operator’s Manual, you can refer to the following resources for citation material or for further information:  “Safe Use of Lasers" (Z136.1)

  • Page 14: Preparing For Installation

     "Performance Standards for Laser Products" United States Code of Federal Regulations 21 CFR 1040.10(d) and 1040.11.  The CETAC LSX-213 Laser Ablation System Service Manual.  CETAC Technologies Customer Service and Support: Phone: 1 (800) 369-2822 (USA only) 1 (402) 733-2829 Fax: 1 (402) 733-1932 E-mail: custserv@cetac.com...

  • Page 15: Establishing Optimal Operating Conditions

    2 Using the LSX-213 Laser Ablation System The LSX-213 system is both reliable and easy to use. Before using the LSX-213 system, however, ensure that your lab environment provides operating conditions that will prolong the life of the LSX-213 system. Once the proper operating conditions are met, you can load samples and perform analysis with the laser ablation system.

  • Page 16: Creating The Lab Environment

     Avoid rough handling of the LSX-213 system. Do not expose the laser ablation system to vibration or shock.  Protect the LSX-213 system from long-term exposure to condensation, corrosive materials, solvent vapor, standing liquids, liquid spills into the electrical equipment or operation inside an acid hood or glove box.

  • Page 17: Replacing Laser Ablation System Components

    CETAC LSX-213 Operator’s Manual Chapter 2: Using the LSX-213 Laser Ablation System The following LSX-213 system components wear out, or become contaminated Replacing Laser Ablation System Components under normal use, and must be replaced periodically.  System Tubing  Chiller water ...

  • Page 18: Connecting The Laser Ablation System

    Two people are required to lift the unit. Lifting should be done with a WARNING person situated on either side of the instrument. Assuming that the LSX-213 has been installed by a qualified CETAC Connections to the Host Computer representative, the electronic connections from the host computer to the LSX- 213 should already be in place.

  • Page 19: Connections To The Power Supply/Cooler

    CETAC LSX-213 Operator’s Manual Chapter 2: Using the LSX-213 Laser Ablation System Video from LSX-213 USB-Video to PC USB-Mouse and Keyboard USB-Video to PC RS232 Serial Data 52-Pin Control Cable Figure 2-2 Host Computer Likewise, all connections between the Laser and the power supply should be in...

  • Page 20: Using The Laser Ablation System

    ICP to the “Argon” port on the back of the LSX-213. For the helium connection, use the supplied fittings to connect 1/8” tubing from the source to the push fitting on the rear of the laser.

  • Page 21: Starting The Laser Ablation System

    LSX-213 system is ready to begin operation under computer control until the programmed sampling procedure is completed. Do not start the LSX-213 system unless the front door and top cover of the WARNING LSX-213 system are completely closed and all covers and safety interlocks To start the laser ablation system, complete the following steps: are in place and operating.

  • Page 22: Methods Of Analyses

    O-ring.) Slide the translation stage back to the home position and close the LSX-213 system door. The translation stage will latch in place when returned to the home position, as will the LSX-213 system door.

  • Page 23: Optimization

    Optimization The host ICP or ICP-MS is optimized in concert with each laser ablation program. The LSX-213 laser ablation parameters can be optimized using the following general procedures. Place a homogeneous reference material (such as the NIST 612 glass which is supplied) in the ablation cell.

  • Page 24: Bulk Analysis

    For example, use integration times or dwell times that will collect data for 1-2 minutes of sample ablation. Set up the LSX-213 in one of the methods that sample a large area (either grid of spots, scanning area or line scan) that will be about 30-60 seconds longer in duration to allow the laser ablation system to equilibrate.

  • Page 25: Depth Profiling

    Applications that benefit the most from using this laser method are those that have the ICP-MS detection ability to gather many data points very quickly (e.g. TOF ICP-MS). The LSX-213 system can be setup to perform large spot sizes at low repetition rates in order to facilitate analyte measurement with fine spatial resolution.

  • Page 26: Sample Preparation

    Sample Size calculated to be large enough for practically all potential applications for the LSX-213 system. Sample sizes ranging from a fraction of an inch to 2 inches (52 mm) in diameter can be placed directly into the sampling cell without further preparation.
  • Page 27 CETAC LSX-213 Operator’s Manual Chapter 2: Using the LSX-213 Laser Ablation System press that is adequate for the application. 13 mm or 31 mm stainless dies are most commonly used.  For best results the powder should be ground as finely as possible. Grain sizes of less than 1-5 µm provide the best results for pressed pellets.

  • Page 28: Shutting Down The Laser Ablation System

    Choose File > Exit to shut down the DigiLaz III software. Turn the main power off. The switch is located on the back of the LSX-213 system. NOTE: Keeping the laser power supply/chiller on for long periods of time does not hurt the system.

  • Page 29: What's New

    3 Using the DigiLaz III Software Use the DigiLaz III™ software to control the operation of a CETAC LSX-213 or LSX-500 laser ablation system. DigiLaz III allows you to draw method patterns on the screen while simultaneously recording all method parameters and coordinates into a sequence page.

  • Page 30: Installing The Digilaz Iii

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Point, Depth Profile, and Multi-Line Scan. Laser parameter control and modes of operation are accessed by "point and click" usage. The platform is designed for maximum method flexibility by using a drawing mode of displaying a method patterns on the screen while simultaneously recording all method parameters and coordinates into a sequence page.

  • Page 31: Software

    Use the menu on the left to select your laser hardware. Use the menu on the right to select the aperture wheel you have. By default, CETAC LSX systems come with a (10, 25, 50, 100, 150, 200, Square) aperture wheel.

  • Page 32: Essential Tasks

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Essential Tasks Emergency Stop  Press the stop button on the power supply pendant (control pod), or Stopping the Laser Quickly  Turn off the power switch on the back of the laser ablation system.

  • Page 33: Operating Software

    Exit from the DigiLaz III software and shutdown the computer (if desired) Choose File > Exit to shut down the DigiLaz III software. Turn the main power off. The switch is located on the back of the LSX-213 system. NOTE Keeping the laser power supply/chiller on for long periods of time does not hurt the system.
  • Page 34 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-3 Manual Laser Control menu Table 3-1 Laser Controls Control What it does Spot size (Microns) Spot size selection Laser Energy (%) Energy Level Selection Laser Shot Frequency (Hz)
  • Page 35 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Table 3-2 Video Modes Mode What it does Target This selection allows the user to navigate the sample with simple mouse clicks on the graphical interface screen. When a mouse click is made the stage will move such that the graphics screen (or center of the crosshairs) is centered on that point.
  • Page 36 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-5 Method Selection drop-down menu Sequence Operations: Here the user can start and stop a method or sequence. When the “Start Ablation” button is pressed, the Sequence Run Information window will open.

  • Page 37: Gas Management

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-6 Sequence Run Information window The Gas Management section consists of four sections: Helium Flow Control, Gas Management Gas Management State, Purge Time, and Cancel Purge. Figure 3-7 Gas Management menu Helium Flow Control: This section allows a value to be designated for the desired Helium carrier gas flow rate.
  • Page 38 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software This allows the sample cell to be opened for sample changes without extinguishing the plasma. (See Figure 3-9.) As soon as the interlock is closed (by closing the sample compartment door or closing the upper enclosure), the valves switch to “Purge”...
  • Page 39 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-9 Bypass gas management state Figure 3-10 Purge gas management state...

  • Page 40: Video Operations

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-11 Argon-only gas management state (no He flow) The Video Operations section consists of five sections: Video Stream, Video Operations Crosshairs, Lines, Media, and Sample Map. Figure 3-12 DigiLaz III™ Software Video Operations Section in the Main Toolbar Video Stream, Crosshairs, &...
  • Page 41 CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Figure 3-13 Graphic color selection button Media: This section allows a sample image and/or video to be recorded. To “Video Snap Shot” button can be pressed to capture and save a sample image.

  • Page 42: Light Controls

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software construct the map and specify the location around which the map will be built (either “Center” of the sample cell or “Current Location”). The “File Operations” menu contains buttons used to save, open, or clear a sample map.

  • Page 43: Using The Sequence Editor

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Using the Sequence Editor The Sequence Editor opened by clicking Launch Sequence Editor in the General Operations tab of the main window. The Sequence Editor automatically stores all drawn method pattern coordinates and associated parameters such as spot size, pulse repetition rate, scan rate, etc.

  • Page 44: General

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software The General tab includes two groups of commands: File Operations and Print General Operations. This group contains buttons which allow you to create a new sequence, File Operations open/save a sequence, and export/import a sequence to and from Microsoft Excel.

  • Page 45: Sequence

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software This tab allows features for easily editing various aspects of the sequence. Editing Figure 3-19 DigiLaz III™ Sequence Editor “Editing” menu These features can either be accessed in the Editing tab by clicking each button individually or by right clicking the mouse.

  • Page 46: Drawing And Editing Method Graphics

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Displays the total time required to complete the entire sequence. Total Sequence Run Time Sequence editor Help is not enabled at this time, but you may access help Help through the Help button in the main DigiLaz III™...

  • Page 47: Deleting A Method Graphic

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Click on the sample image to define the starting point of the method. Continue clicking to set intermediate or end points. See "Software Methods" beginning on page 51 for details.

  • Page 48: Triggering And Timing

    The DigiLaz III software can be used to designate when an external trigger signal will be sent to initiate data acquisition by the host instrument. Depending on how the host instrument is configured, the LSX-213 can use contact closure to synchronize start and delays between the LSX-213 and host ICP.

  • Page 49: Gas Blank

    CETAC LSX-213 Operator’s Manual Chapter 3: Using the DigiLaz III Software Time that occurs before the laser begins to fire onto the sample. Gas Blank Gas Blank includes the Shutter Delay time, so it must be greater than or equal to the Shutter Delay value.

  • Page 50: Service Calibration Tools

    As such, these functions are described in another document only available from the CETAC service department. These tools should only be accessed on request of the CETAC service engineer.

  • Page 51: Spot Scan

    4 Software Methods Each of the pictures shown are taken from the main software screen. Each method can be “drawn” using the graphical interface, as indicated in these pictures, or, by entering the sample coordinates into the sequence editor. On- screen graphical method drawing is useful because one can see exactly where the ablation spot, line or area is going to take place.

  • Page 52: Parameters

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Example Line Scan Single line scan allows the laser to move incrementally across a sample in a Description straight line. Energy, shot frequency, and spot size can all be set. The scan rate, expressed in Parameters µm/sec, automatically calculates the time per scan and the X and Y distances...

  • Page 53: Segmented Line Scan

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Click anywhere on the sample image to set the start point. Click again to set the end point. Multiple repetitions of the line scan, delay between scans and gas blank can all be set in the sequence editor to allow optimal integration with ICP software.

  • Page 54: How To Draw

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods How to Draw Select the Segmented Line Scan method. Click anywhere on the sample image to set the start point. Click again to end a segment and begin the next one. Left-click and select Mark Last Segment to set the end point.

  • Page 55: Line Raster

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Line Raster In the line raster, the laser follows a line of discreet spots. By drawing a line on Description the sample image to indicate the area of interest, the software automatically calculates the number of spots which will fit on the space provided, given the spot size and distance between spots.

  • Page 56: Scanning

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Example Scanning Here, the user defines an area using the mouse. This area is then divided up Description automatically given the distance between lines and the spot size. Energy, shot frequency, and spot size may be set. The number of lines,...

  • Page 57: Example

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Set the method parameters. Click anywhere on the sample image to set the start point. Click again to set the end point. Example...

  • Page 58: Area Raster

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Area Raster Area raster is analogous to line raster except it covers a defined area in the Description same way that the area scan does. Enter the spot size and distance between spots. Energy, shot frequency, and Parameters number of shots per spot may also be set.

  • Page 59: Example

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Example...

  • Page 60: Depth Profiling

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Depth Profiling Depth profiling is a method which moves the Z stage at specific increments and times to compensate for the "drilling" effect of the laser into the sample. Normally, continuously ablating a single spot will result in the laser getting out of focus as the hole gets deeper.

  • Page 61: Example

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Open the Sequence Editor and select the Depth Profiling tab to set the per-step parameters. Click anywhere on the sample image to set the location. Example...

  • Page 62: Multiple Method Drawing

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Multiple Method Drawing DigiLaz III allows a number of different methods to be combined into a sequence. As shown above, all eight methods can be drawn on the sample image simultaneously and ablated in order. Parameters can be changed for the...

  • Page 63: Sequence Editor

    CETAC LSX-213 Operator’s Manual Chapter 4: Software Methods Sequence Editor All drawn method graphic coordinates and associated parameters are automatically stored in the sequence editor. All method parameters can be changed at any time. The “Run Sequence” button can be used to run all methods or individual rows can be highlighted to run select methods from the sequence.

  • Page 65: Safety Systems/Maintenance Schedule

    Safety Systems/Maintenance Schedule The LSX-213 Laser Ablation System is designed, as a Class 1 laser product, to contain all hazardous laser radiation during normal operation, as required by the U.S. Department of Health and Human Services. Normal operation of the LSX-213 shall not be allowed unless all safety systems are operational.

  • Page 66: Safety System Inspection

    Q-Switch and Laser Safe from Power Supply Figure 5-1 Rear View of the LSX-213 Cooling System Maintenance Changing the laser cooling system coolant is the primary maintenance tasks that will be performed. Other items should also be checked periodically to maintain the cooling system properly.

  • Page 67: Periodic Checks Of The Cooling System

    If the back light is not on, follow the steps below to fill the reservoir to proper levels. Before shipping the laser, a CETAC Technologies technician drains the coolant Filling and Draining the Power Supply from the coolant reservoir. In order to use the Cooling Group Unit, the customer must fill the coolant reservoir with about 1.5 liters of distilled water.
  • Page 68 CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System Disconnect the umbilical coolant lines from the ICE450 and drain the water from the reservoir (follow the steps described in Step 4). Then, disconnect the umbilical coolant lines from the laser head and reconnect the red fitting to the ICE450.

  • Page 69: Ionizing Cartridge Maintenance (Inline Filter)

    CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System The ICE450 cooler/power supply can provide years of reliable performance De-Ionizing Cartridge Maintenance (Inline Filter) given proper handling and some minor routine maintenance. Visually inspect your ICE450 monthly for coolant leaks, abnormal noises or damage to connectors and coolant ports.

  • Page 70: Ionizing Cartridge Maintenance (Internal Filter)

    CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System The ICE450 cooler/power supply can provide years of reliable performance De-Ionizing Cartridge Maintenance (Internal Filter) given proper handling and some minor routine maintenance. Visually inspect your ICE450 monthly for coolant leaks, abnormal noises or damage to connectors and coolant ports.
  • Page 71 CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System Loosen the screw holding the DI cartridge access cover in place. The cover will then swing open 90 degrees. After opening the cover 90 degrees, remove it from the back of the ICE450 by pulling it away from the rear of the unit.
  • Page 72 CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System Figure 5-8 DI Cartridge Extraction Orient the extracted DI cartridge assembly, and the new DI cartridge, as indicated in Figure 5-9. Note the direction of the FLOW arrow on the side of the cartridges.
  • Page 73 CETAC LSX-213 Operator’s Manual Chapter 5: Maintaining the Laser Ablation System Figure 5-10 Re-Insertion of the DI Cartridge Pull the cartridge back out slightly with the latch until the metal tube and the right-angle fitting lines up with the internal mating fitting. Use the latch to push the metal tube into the internal mating fitting, as shown in Figure 5-11.

  • Page 74: Internal Tubing Replacement

    In the event the sample gas/valve assembly tubing becomes contaminated, it must be replaced. A spare parts kit can be obtained from CETAC. In lieu of purchasing the kit, the tubing can be changed with stock Tygon tubing. All the Tygon tubing is 1/4”...

  • Page 75: Troubleshooting The Laser Ablation System

    Software limits have been factory selected to protect the laser system against electrical and optical damage. If you determine the problem is in the LSX-213, check the AC power transformer, the communications interface, the safety interlocks, or the laser head to find the cause of the problem and resolve it.

  • Page 76: Power System Problems

    LSX-213 or it may not be getting to the power supply/chiller. If this is the case, the READY indicator (green LED) on the front of the laser module is off and all of the LEDs on the front of the power supply are off.

  • Page 77: Fuses

    Fuses The only fuses in the LSX-213 are in the laser power supply. The laser module has no replaceable fuses. The power supply/chiller has one fuse which can be checked in the event that it does not operate despite taking the actions outlined above.

  • Page 78: Interface Problems

    If the cables are connected properly and the laser ablation system is still not Software Configuration Problems communicating with the control computer, ensure that the software is configured correctly. To do so, complete the following steps: Run the LSX-213 software, or the stepper control program, to ensure that the computer is functioning properly.

  • Page 79: Safety Interlock Problems

    Safety Interlock Problems There are seven safety interlocks in the LSX-213 Laser Ablation System to protect personnel from accidental UV laser beam and high voltage exposure, and to protect the laser from overheating.

  • Page 80: Laser Problems

    150 F (65 Laser Problems A malfunction of the LSX-213 laser can indicate a problem with the laser electronics unit, laser-pumping energy, the cooling system, or with the laser flashlamp. The following sections explain how to troubleshoot these problems.

  • Page 81: Low Laser Efficiency

    Given this information, consult your CETAC service representative who will provide further guidance.

  • Page 82: Carrier Gas System

    The carrier gas is the medium that delivers the ablated sample to the ICP-MS. The carrier gas for the LSX-213 is helium and is controlled by the helium mass flow controller via computer. Argon from the host ICP is used as a make-up gas which is mixed downstream of the sample cell before exiting the sample out port on the LSX-213.

  • Page 83: Returning The Product To Cetac For Service

    CETAC LSX-213 Operator’s Manual Chapter 6: Troubleshooting the Laser Ablation System Returning the Product to CETAC for Service Refer to the following information if you need to return the product to CETAC Technologies for service. Follow these guidelines when shipping the product: Shipping the Product ...

  • Page 84: Returned Product Procedures

    CETAC reserves the right to change or improve the design of any unit without assuming any obligation to modify any unit previously manufactured.

  • Page 85: Returned Product Warranty Determination

    CETAC LSX-213 Operator’s Manual Chapter 6: Troubleshooting the Laser Ablation System After CETAC’s examination, warranty or out of warranty status will be Returned Product Warranty Determination determined. If a warranted defect exists, the product will be repaired at no charge and shipped prepaid back to the buyer. If the buyer desires an air freight return, the product will be shipped collect.
  • Page 86 CETAC LSX-213 Operator’s Manual Chapter 6: Troubleshooting the Laser Ablation System This page is intentionally blank.

  • Page 87: Characteristics

    CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information 7 Safety and Regulatory Information Review this product and related documentation to familiarize with safety markings and instructions before you operate the instrument. Characteristics Environmental Characteristics Operating Temperature +10° C to +30° C (+50° F to +85° F) Non-Operating Temperature +0°...
  • Page 88 CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information Power requirements Cooler/Power Input: Supply AC Voltage, Frequency, and Current 100-250 V AC ± 10% ~ 47-63 Hz Installation Category: CAT II (Line voltage in appliance and to wall outlet) Output: 28 V DC, 4.6 A...

  • Page 89: Safety Notices

    CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information Safety Notices If the equipment is used in a manner not specified by CETAC Technologies, WARNING Repair or service that this not covered in this manual should only be the protection provided the equipment may be impaired.

  • Page 90: Coolant

    CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information The cooling system, located in the laser power supply, is filled with DISTILLED Coolant WATER. Do not fill with any other type of fluid. The cooling system should contain a sufficient amount of distilled water. The fault light will come on if the coolant is in interlock mode.

  • Page 91: Cleaning Instructions

    To reduce the risk of fire hazard and electrical shock, do not expose the unit to rain or humidity. To reduce the risk of electrical shock, do not open the cabinet. All maintenance is to be performed by an Authorized CETAC Service Provider.

  • Page 92: Explanation Of Caution And Warning Notices

    CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information Explanation of Caution and Warning Notices Warning symbol marked on equipment. This symbol means “Attention! Refer to the manual.” The WARNING notice denotes a hazard. It calls attention to a procedure,...

  • Page 93: Avertissements En Français

    CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information Avertissements en Français This section provides French translations of notices which may appear on the instrument or on other instruments used as part of the measurement system. AVERTISSEMENT POUR UNE PROTECTION CONTINUÉ CONTRE LES RISQUES D’INCENDIE, REMPLACER UNIQUEMENT PAR DES FUSIBLES...

  • Page 94: Electromagnetic Interference

    The FCC requires the user to be notified that any changes or modifications made to this device that MODIFICATIONS are not expressly approved by CETAC Technologies may void the user's authority to operate the equipment. Connections to this device must be made with shielded cables with metallic RFI/EMI connector CABLES hoods to maintain compliance with FCC Rules and Regulations.

  • Page 95: Explanation Of Regulatory Marks

    In the event a supplier cannot be reached, contact CETAC Technologies customer service department at 1 (800) 369 2822. The CE mark is a registered trademark of the European Community. This CE mark shows that the product complies with all the relevant European Legal Directives.
  • Page 96 CETAC LSX-213 Operator’s Manual Chapter 7: Safety and Regulatory Information This page is intentionally blank.

  • Page 97: Glossary

    Flat Top Energy Profile: Beam profile of the UV Nd:YAG laser at 266 nm producing superior pit morphology. He: Helium. Used as the sample carrier gas. Host Computer: The computer that controls operation of the LSX-213 laser ablation system. Typically, this computer also controls the analytical instrument.
  • Page 98 CETAC LSX-213 Operator’s Manual Chapter 8: Glossary LED: Light-Emitting Diode. LSX-213: The CETAC LSX-213 Laser Ablation System. Macro: The software in the electronics module which intercepts and acts upon autosampler commands. Nd:YAG: Neodymium: Yttrium Aluminum Garnet. Refers to the type of laser used in the LSX-213.
  • Page 99 Index area raster, 58 methods, 51 avertissements, 93 drawing, 46 avis Canadien, 95 online state, 37 bulk analysis, 24 operator qualifications, 13 burst, 34 pollution degree, 87 bypass state, 37 powder samples, 26 characteristics power electrical, 88 requirements, 88 laser, 10 power cord, 90 cleaning, 91 purge state, 38...
  • Page 100 480141 Manual Part Number Rev 2e Printed in USA...

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