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CETAC ASXpress Operator's Manual

Rapid sample introduction system
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ASX
CETAC
Rapid Sample Introduction System
Operator's Manual
Manual Part Number 480166 Rev 4
PRESS

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  • Page 1 PRESS CETAC Rapid Sample Introduction System Operator’s Manual Manual Part Number 480166 Rev 4...
  • Page 2 480166 Rev 4 , April, 2010 materials, infectious agents, or any other materials and/or conditions that could constitute a health or injury hazard to CETAC All rights reserved. Reproduction or REPRODUCTION employees. Call Customer Service and...
  • Page 3 Contents...

  • Page 4: Table Of Contents

    Preparing for Installation .................. 16 2.1.1 Space Requirements .................. 16 2.1.2 Liquid Waste Routing Requirements ..........16 2.2 Unpacking the ASXpress Rapid Sample Introduction System ....17 2.1.3 Power Requirements................. 17 3.1 Prepare the CETAC Autosampler ................ 21 Installing the ASX Rapid Sample Introduction System ....
  • Page 5 7.2 Interface Problems ....................106 7.2.1 RS-232 Cable Problems ................. 106 7.2.2 USB cable Problems ................106 7.3 Returning the Product to CETAC for Service ..........109 7.2.3 Software Configuration Problems ............ 106 7.3.1 Shipping the Product ................109 7.3.2 Product Warranty Statement .............
  • Page 6 ASXpress Rapid Sample Introduction System Operator’s Manual Preface 10.5 Explanation of Regulatory Marks ............132 11 Index ........................134...
  • Page 7 Introduction...

  • Page 8: Overview

    • Windows-based software to allow the configuration of the system The ASX system is connected to, powered, and controlled by a CETAC • autosampler. The ASX system is operated by the autosampler executing a macro automatically when the probe is placed into the sample. The macro PRESS ends when the probe is lifted out of the rinse station.
  • Page 9 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 1: Introduction “Load Sample” Cycle Diagram Figure 1-1 “Inject/Rinse” Cycle Diagram Figure 1-2...

  • Page 10: Rapid Sample Introduction System Standard Components

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 1: Introduction 1.1 Rapid Sample Introduction System Standard Components The ASX Rapid Sample Introduction System module cases are made of a high-strength aluminum alloy with an epoxy powder coating finish. The 6-...
  • Page 11 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 1: Introduction The following standard components are located on the ASX system and are shipped with the system. Each lettered item listed below corresponds with a feature in Figure 1-3. PRESS A. Vacuum Pump “Out” Port B.
  • Page 12 PRESS station will be included in the kit, as this version rinse station MUST be used. (The CETAC ASX-520HS includes a large-bowl rinse station, which must be replaced with the standard-bowl unit which is included in the upgrade version of the ASX system, as mentioned above.)

  • Page 13: Optional Accessories/Components

    Note Please refer to the ASX Rapid Sample Introduction System PRESS Accessories and Supplies Catalog or contact CETAC Technologies if you need additional accessories not listed, need added features to integrate the ASX Rapid Sample Introduction System into your PRESS analytical system, or have unique requirements.

  • Page 14: About This Book

    The ASX The software manual for the ICP/ICP-MS instrument you are using • Quick Installation Guide PRESS The operator’s manual for the CETAC autosampler you are using • The CETAC Technologies Website: www.cetac.com • CETAC Technologies Customer Service and Support: •...
  • Page 15 Preparing for Installation...

  • Page 16: 2.1 Choosing A Location

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 2: Preparing for Installation 2 Preparing for Installation Installing the ASX system requires preparation. Before you install the Rapid Sample Introduction System, you should evaluate the physical arrangement of the laboratory to choose a suitable location which allows...

  • Page 17: Unpacking The Asxpress Rapid Sample Introduction System

    The ASX system is intended to operate from DC power supplied PRESS through the CETAC autosampler, which is provided power through an AC WARNING power source that will not apply more than 240VAC between the supply conductors and ground. A protective ground connection by way of the grounding connector in the autosampler power cord is required for safe operation.
  • Page 18 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 2: Preparing for Installation...
  • Page 19 Installing the Rapid Sample Introduction System...

  • Page 20: Installing The Asx

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3 Installing the ASX Rapid Sample PRESS Introduction System The ASX Rapid Sample Introduction System is designed for easy installation. Installation consists of two parts: preparing the autosampler and...

  • Page 21: Prepare The Cetac Autosampler

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1 Prepare the CETAC Autosampler A CETAC ASX-520, ASX-520HS, or ASX-260 autosampler may be used with the system. If the autosampler and ASX Rapid Sample Introduction...

  • Page 22: Install The Auxiliary I/O Connector Card And Processor (Rabbit) Module

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1.1 Install the Auxiliary I/O Connector Card and Processor The proper processor module (with ASX functionality firmware pre- (Rabbit) Module loaded) and auxiliary board (daughter board) with female I/O connector are...
  • Page 23 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Figure 1-5 Front view of ASX-260 Autosampler. 2. Remove the two Kynar thumbscrews from the Y-axis home block (Figure 1-6). Figure 1-6 View of Y-axis home block with Kynar thumbscrews (ASX-260...
  • Page 24 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3. Remove the entire Z-drive assembly from the Y-arm by pulling the Z- drive assembly forward and off of the autosampler arm as shown (Figure 1-7 and Figure 1-8).
  • Page 25 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 4. Once the Z-drive assembly is removed, remove the rinse station (Figure 1-9/Figure 1-10). Turn the rinse station ¼ turn counter- clockwise while pulling it upward. Also, the tubing located at the bottom of rinse station will have to be disconnected from the pump at the rear of the autosampler.
  • Page 26 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 5. The autosampler tray should then be removed. Lift up the tray and pull out (Figure 1-11). Figure 1-11 Removing the tray (ASX-520).
  • Page 27 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 6. Next, the front cover is to be removed. Remove the four corner screws (Figure 1-12/Figure 1-13). Figure 1-12 Front view of ASX-520 Autosampler showing front cover screws.
  • Page 28 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 7. The front cover is removed by lifting it slightly and pulling forward (Figure 1-14/Figure 1-15). Figure 1-14 View of ASX-520 Autosampler with the front cover being removed.
  • Page 29 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 8. The screws that hold the inner shield must be removed. Move the Y- axis assembly all the way to the left (Figure 1-16/ Figure 1-17 shows screw locations).
  • Page 30 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 9. The inner shield can be removed by lifting it up while pulling forward (Figure 1-18/Figure 1-19). Removal of inner shield (ASX-520). Figure 1-18 Figure 1-19 Removal of inner shield (ASX-260).
  • Page 31 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System To complete I/O board/rabbit module installation for CETAC ASX-520/ ASX-520HS/EXR-8 autosamplers, continue on the next page (32). To complete I/O board/rabbit module installation for the CETAC ASX-260 autosampler,...

  • Page 32: Continuation Of I/O Board And "Rabbit" Module Installation For Cetac Autosampler Asx-520/Asx-520Hs

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1.2 Continuation of I/O board and “Rabbit” module installation for CETAC autosampler ASX-520/ASX- 520HS AUXILIARY BOARD INSTALLATION (ASX-520/520HS) 1. Remove the Auxiliary cover plate and discard the plate and hardware (Figure 1-20).
  • Page 33 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Figure 1-22 Note the location of the pin array marked “P7” utilized to mate to the I/O board (ASX-520). Note: It may be necessary to loosen screws that secure the main circuit board to the case to facilitate positioning/installation of the I/O board.
  • Page 34 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Figure 1-23 I/O board being placed into position to mated to the main board pin array (ASX-520) Figure 1-24 Main and Daughter board installed (ASX-520).
  • Page 35 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 4. Install Jackscrews through the autosampler case and into the 37-pin connector ears, threading and then fully tightening with a 3/16” nut driver to securely attach daughter board to the chassis (Figure 1-25).
  • Page 36 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System PROCESSOR (RABBIT) MODULE INSTALLATION (ASX-520/ASX-520HS) 5. Remove the existing Rabbit processor module from the main board (See Figure 1-26 for location of Rabbit module) by pulling straight upward and firmly on the Rabbit module, gripping it by the sides.
  • Page 37 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 6. Insert Rabbit module processor (supplied in the upgrade kit) in the same position/orientation as the removed unit had been installed. Be sure to align all pins to the proper socket hole location, using care to insert the module fully and securely.

  • Page 38: Cetac Asx-260 Autosampler

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1.3 Continuation of I/O board and “Rabbit” module installation for CETAC ASX-260 autosampler 1. Remove the blue ribbon cable from the carriage assembly by first bending the retaining clamp out of the way, then grasp the cable firmly and give a sharp tug (Figure 1-28).
  • Page 39 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 2. Loosen the guide shaft set screws at each end of the guide shaft (Figure 1-29) Figure 1-29 Loosening of guide shaft set screws (ASX-260).
  • Page 40 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3. Remove the three mounting screws for the right end plate (Figure 1-30). Two are counter sunk and one is a round head. The round head screw is used on the back of the chassis when re-assembled.
  • Page 41 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 4. Remove right end plate (Figure 1-31). It may be necessary to lightly tap with a small hammer or mallet as the fitting is sometimes quite snug.
  • Page 42 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 6. Remove the voltage regulator heat sink using a 1/4” nut driver (Figure 1-32). Set this aside for re-assembly. Figure 1-32 Removing the voltage regulator heat sink (ASX-260).
  • Page 43 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 7. Remove the four stand-offs with the 1/4” nut driver (Figure 1-33). Set these aside for re-assembly. Figure 1-33 Removing the four stand-offs (ASX-260). 8. Remove the 6 Phillips head screws holding the board in place (Figure 1-34).
  • Page 44 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 9. Remove the board by pulling forward from the top (Figure 1-35). Figure 1-35 Removing the main board. Rabbit processor is the small board in the top left corner (ASX-260).
  • Page 45 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 11. Remove stand-off with 1/4” nut driver and discard (Figure 1-37). Remove the spacer located under the stand-off and place with the other two spacers received with the installation kit.
  • Page 46 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 13. Install the daughter board on the three studs. Secure to the bottom two posts with the 5/16” head nuts provided in the kit. Secure to the top post with the 3/8”...
  • Page 47 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 14. Install the main board in the chassis. Ensure the 10 pin connector on the back of the board is seated correctly in the connector of the communications interface board mounted behind it (Figure 1-40).
  • Page 48 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System belt in place. PROCESSOR (RABBIT) MODULE INSTALLATION (ASX-260) 1. Remove existing Rabbit processor module from the main board (See Figure 1-41 for location of Rabbit module) by pulling straight outward and firmly on the Rabbit module, gripping it by the sides.

  • Page 49: Increase The Peristaltic Pump Speed Setting

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Mainboard shown with rabbit module removed Figure 1-42 Proceed to the “Increase the Peristaltic Pump Speed” section of this manual (Do not replace covers, etc., at this time).
  • Page 50 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Figure 1-43 Jumper position utilized to increase pump speed (ASX-520) Note: ASX-520/ASX520HS main boards of differing eras/versions may have varying orientation of jumper positions. Follow the nomenclature present on the circuit board for proper jumper positioning.

  • Page 51: Internal Work Is Complete; Replace All Covers, Etc

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System When all interior work has been completed as outlined in the previous 3.1.5 Internal work is complete; replace all covers, etc. sections: • Reinstall all shields •...

  • Page 52: Install The Standard-Bowl Rinse Station And Modified Rinse Tubing Arrangement

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1.6 Install the Standard-Bowl Rinse Station and Modified A Standard-Bowl Rinse Station (Figure 1-45) and associated modified tubing Rinse Tubing Arrangement arrangement is required to accommodate the design requirements of the system.
  • Page 53 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Rinse Tubing and Y-Connection Assembly Installed on Peristaltic Pump and Rinse Station (ASX-520) Figure 1-46 To retrofit the rinse station on an ASX-520HS with existing Large Bowl Rinse Station to the Standard Bowl version, complete the following: 1.
  • Page 54 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Rinse Tubing Diagram Figure 1-47 To retrofit the rinse station plumbing on an ASX-520 or ASX-260, complete the following: 1. Gently pull the existing rinse station away from the autosampler rinse block.
  • Page 55 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System of tubing may be cut to accommodate your specific position/arrangement. 5. Gently push the Standard Bowl Rinse Station into place onto the rinse station holder block (mounted on the autosampler front cover) as shown in place in Figure 1-45.

  • Page 56: Install The 1.0Mm Id Sample Probe On The Autosampler

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.1.7 Install the 1.0mm ID Sample Probe on the A 1.0mm ID sample probe (Figure 1-48) is provided for use with the CETAC Autosampler autosampler for proper operation with the ASX system.

  • Page 57: System

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.2 Connect the ASX system Once the autosampler is prepared for use, the ASX system should be PRESS connected to the host instrument and autosampler, and the autosampler should be connected to the host instrument’s computer.
  • Page 58 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Valve/Pump Module Tubing Connections Figure 1-49 PRESS To make the plumbing connections to the ASX (Figure 1-49), perform the following: PRESS 1. Remove the protective cover from the 6-port valve.
  • Page 59 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 6. Connect the 14” length of 0.030” x 0.062” tubing (which is pre-installed to the green connector at port #6 of the 6-port valve) to the ICP / ICP-MS peristaltic pump.

  • Page 60: Connect The Electronics Module To The Valve/Pump Module

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.2.2 Connect the Electronics Module to the Valve/Pump The ASX system is comprised of two main components which include the Module electronics module and valve/pump module (Figure 3-47). The separate...

  • Page 61: Connect The Asx Press

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System The ASX valve/pump module connects to the electronics module via its integrated cable with DIN style connector as shown in Figure 3-48. To connect the electronics module to the valve/pump module, simply plug the PRESS valve/pump module’s cable connector into the electronics module’s jack...

  • Page 62: Connect The Autosampler To The Host Computer

    Valve/Pump Module to ASX autosampler Figure 1-49 PRESS Connect the CETAC autosampler to the host computer and power source as 3.2.4 Connect the Autosampler to the Host Computer directed in the CETAC Autosampler Operator Manual. When interconnecting any computing devices, keep communications cables...
  • Page 63 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.3 Install the ASX Software The Xpress Configuration Tool Program is used to enable/disable and PRESS configure the autosampler and its control of the ASX...
  • Page 64 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Xpress Config Installation Wizard Figure 1-51 The License Agreement appears. Click the “I accept the terms in the license agreement” radio button. Then click the “Next” button (Figure 3-52).
  • Page 65 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Readme information window Figure 1-53 The “Destination Folder” window appears. Click the “Change” button to modify the folder name or location, or click “Next” to select the default location as depicted in Figure 3-54.
  • Page 66 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System “Ready to Install the Program” window Figure 1-55 The “InstallShield Wizard Completed” window appears (Figure 3- 56). Select the “Launch the program” box and then click the “Finish”...
  • Page 67 This process reads the parameters that are stored on the rabbit processor residing within the CETAC autosampler (the default settings will be read the first time the Query is performed), and displays them in the Configuration Tool parameter fields.
  • Page 68 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Configuration Tool software window (post-query) Figure 1-58 Note the appearance of the Config Tool software window after querying (Figure 3-58). Clicking on the double arrow box in the...
  • Page 69 ASX firmware, or to upgrade PRESS firmware to subsequent versions as CETAC advances its technology. To perform this procedure, all covers should be removed to access the interior of the autosampler as is outlined in section 3.1.1 of this manual.

  • Page 70: Upgrade The Firmware On The Autosampler

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.4 Upgrade the Firmware on the Autosampler The CETAC autosampler requires a firmware version which is compatible with the ASX system. The ASX full system versions are shipped with the firmware pre-loaded onto the Rabbit module which is pre-installed inside the autosampler.
  • Page 71 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Note: Main boards of different versions may have varying locations/positions/quantities of available jumper positions. Follow nomenclature present on the board for proper jumper positioning. Figure 1-60 Jumpers on board in normal mode (ASX-520).

  • Page 72: Load The Firmware Upgrade, Via The Rabbit Field Utility (Rfu) Program, From The Cd Provided

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3. On the ASX-260 board, move jumper JP2 to JP4 and leave JP3 in place (Figure 3-61 shows jumpers). Jumpers on board in normal position (ASX-260) Figure 1-61 3.4.2 Load the Firmware Upgrade, via the Rabbit Field...
  • Page 73 Note: For additional instructions on using HyperTerminal, refer to the Guide to Operating a CETAC Autosampler using HyperTerminal located at the end of this manual. If your computer does not have HyperTerminal configured already, please refer to this section now.
  • Page 74 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System Figure 1-62 Rabbit Field Utility Application • When the Rabbit Field Utility has opened, select “Setup”, and then “Communications”.
  • Page 75 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System • On the Communications Options window (Figure 3-63), in the “Comm Port” field, select the COM port on the computer that is connected to the autosampler.
  • Page 76 Note: The .bin file name in Figure 3-65 (i.e. ASXpress_1_19) will vary depending on which era ASXpress FW is being loaded. CETAC Technologies makes every effort to update the firmware as needed to ensure that the most beneficial functionality is provided to the customer.
  • Page 77 ASXpress_HS_1_19) will vary depending on which era ASX FW is PRESS being loaded. CETAC Technologies makes every effort to update the firmware as needed to ensure that the most beneficial functionality is provided to the customer. As of December 2009, the most current firmware version file name is “ASXpress_1_19”...
  • Page 78 ASXpress_HS_1_19) will vary depending on which era ASX FW is PRESS being loaded. CETAC Technologies makes every effort to update the firmware as needed to ensure that the most beneficial functionality is provided to the customer. As of December 2009, the most current firmware version file name is “ASXpress_1_19”...
  • Page 79 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 3: Installing the Rapid Sample Introduction System 3.4.2.4 Return the Autosampler to Normal (Non-Programming Mode) Configuration Turn off the autosampler. On the ASX-520/520HS board, move jumper JP5 and JP6 back to JP3...
  • Page 80 Chapter 3: Installing the Rapid Sample Introduction System 3.4.2.5 Verification of Firmware Upgrade Start HyperTerminal. (For instructions on using HyperTerminal, refer to the Guide to Operating a CETAC Autosampler using HyperTerminal). In HyperTerminal type VERSS. The system should respond with the new firmware version.
  • Page 81 Verifying Installation/ Function Overview...

  • Page 82: Verifying Installation/ Function Overview

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 4: Verifying Installation/ Function Overview 4 Verifying Installation/ Function Overview Once installation of the ASX Rapid Sample Introduction System is complete, it is important to verify that you have installed it correctly, so that it functions as intended.

  • Page 83: To Test The Communications Interface, Complete The Following Steps

    Click on the “Load” button (Figure 4-3); doing so will position the 6-port valve into the mode which loads the sample loop, and PRESS will illuminate the “Load” Led on the front panel of the ASXpress electronics module (no autosampler operation takes place at this time).
  • Page 84 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 4: Verifying Installation/ Function Overview timing parameters. Click on the “Inject” button (Figure 4-3); doing this so will position the 6-port valve into the mode in which sample injection into the PRESS ICP takes place (via the Peristaltic pump on the ICP), and will illuminate the “Inject”...
  • Page 85 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 4: Verifying Installation/ Function Overview Figure 1-52 Xpress Configuration Tool—Expanded Window Note: At any time that parameter changes are made within the Xpress Configuration Tool software, the user must save those settings by clicking the “Save to ASX”...

  • Page 86: Operation Controls

    4.3 Operation Controls Enable ASXpress operation for normal operation. 4.3.1 Enable ASXpress Operation Disable ASXpress operation if you want to test how the autosampler would respond to commands without the ASX system. (Note that a different tubing arrangement is required to run the autosampler without the ASX system.) This setting does not affect the rinse timeout.

  • Page 87: Additional Xpress Configuration Tool Features

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 4: Verifying Installation/ Function Overview When the vacuum pump timeout is not enabled, the vacuum pump will 4.3.2 Enable Vacuum Pump Timeout continue running indefinitely after sampling has stopped. This introduces wear which can reduce the lifespan of the vacuum pump. Enable the vacuum Pump Timeout to specify a limit for how long the vacuum pump should continue running.

  • Page 88: Regular Inspection Of Asx Components

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 4: Verifying Installation/ Function Overview To save the notes: The notes will be saved to a predefined file. 1. Click the floppy disk icon at the top of the Notes window. 4.5 Regular Inspection of ASX...
  • Page 89 Using the Rapid Sample Introduction System...

  • Page 90: 5.1 Establishing Optimal Operating Conditions

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 5: Using the Rapid Sample Introduction System 5 Using the Rapid Sample Introduction System The ASX Rapid Sample Introduction System is both reliable and easy to use. Before using it, however, ensure that your lab environment provides...

  • Page 91: Replacing Rapid Sample Introduction System Components

    When you need to purchase additional supplies, it is extremely important that 5.1.3 Purchasing Supplies you choose the appropriate sizes and materials. To order additional supplies, refer to the CETAC Accessories and Supplies Catalog for the ASX Rapid Sample Introduction System.

  • Page 92: Starting The Asx Press Rapid Sample Introduction System

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 5: Using the Rapid Sample Introduction System 5.1.4 Starting the ASX Rapid Sample Introduction PRESS System To start the Rapid Sample Introduction System, complete the following steps: PRESS Ensure that the ASX...

  • Page 93: Rapid Sample Introduction System

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 5: Using the Rapid Sample Introduction System 5.2 Shutting Down the ASX Rapid Sample PRESS Introduction System To shut down the ASX Rapid Sample Introduction System, complete the following steps: PRESS 1. Drain the system by removing the rinse solution uptake tubing from the rinse solution sources (autosampler and ICP/ICP-MS).

  • Page 94: Flushing The Rinse Station And Flow Path

    Config software, utilizing the time settings for Loop Load, Probe Wash, Rinse Station Fill and Rinse Timeout that are normal operating parameters specific to your own process. Click on the “Query ASXpress Params” button, and then click on the “Manual Cycle” button. This will run the ASX system through a PRESS complete cycle of operation, including “load”...
  • Page 95 Maintaining the Rapid Sample Introduction System...

  • Page 96: Press

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System 6 Maintaining the ASX Rapid PRESS Sample Introduction System Routine maintenance of the ASX Rapid Sample Introduction System consists of daily and weekly cleaning of specific components. Routine...
  • Page 97 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System Note: It is recommended to clean the 6-port valve every 20,000 cycles. However, the frequency of cleaning interval will vary depending on application. Materials required:...
  • Page 98 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System Figure 6-1 6-port valve assembly – exploded view of components...

  • Page 99: Checking For Leaks

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System 6.2 Checking for Leaks The tubing has a finite lifespan, and will wear out under normal use. Standard maintenance procedures require that you periodically check for leaks. To do...

  • Page 100: 6-Port Valve Replacement Or Reorientation

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System 6.4 6-Port Valve Replacement or Reorientation The 6-Port valve Assembly has a finite lifespan that is dependent upon the conditions/sample media to which it is exposed. Exposure to higher sample solids levels reduces the valve lifespan.
  • Page 101 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System No gap Hex screw Figure 6-2 Reseating the 6-Port Valve 12 Tighten the hex screw. 13 Repeatedly cycle the actuator via the software “Load” and “Inject”...
  • Page 102 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 6: Maintaining the Rapid Sample Introduction System...
  • Page 103 Troubleshooting the Rapid Sample Introduction System...

  • Page 104: Troubleshooting The Rapid Sample Introduction System

    This chapter explains how to troubleshoot ASX Rapid Sample Introduction System problems. If you cannot solve a problem using the steps given in this chapter, you should contact CETAC Technologies Customer Service and Support. PRESS 7.1 Power System Problems A possible cause of ASX Rapid Sample Introduction System malfunction is a problem in the power system.
  • Page 105 ASXpress Rapid Sample Introduction System Operator’s Manual Troubleshooting the Rapid Sample Introduction System Check the external power supply (autosampler). The green LED on the power supply should be illuminated. a. If the power supply LED is not illuminated, check the wall ...

  • Page 106: Interface Problems

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 7: Troubleshooting the Rapid Sample Introduction System 7.2 Interface Problems Operation of the ASX system is directed by the host computer and autosampler. A malfunction of the ASX Rapid Sample Introduction System...
  • Page 107 ASXpress Rapid Sample Introduction System Operator’s Manual Troubleshooting the Rapid Sample Introduction System system. To do so, verify proper operation of all manual functions by completing the following steps: PRESS With the ASX system connected to the autosampler/ICP/ICP-MS systems, Operate manual features of the Xpress Config Tool software.
  • Page 108 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 7: Troubleshooting the Rapid Sample Introduction System Ensure that ICP software is not conflicting with ASX system PRESS Disable ICP software and run the ASX system from host computer. If operation. conflict is no longer present, troubleshoot ICP software per its own troubleshooting procedure.

  • Page 109: Returning The Product To Cetac For Service

    ASXpress Rapid Sample Introduction System Operator’s Manual Troubleshooting the Rapid Sample Introduction System 7.3 Returning the Product to CETAC for Service Refer to the following information if you need to return the product to CETAC Technologies for service. Follow these guidelines when shipping the product: 7.3.1 Shipping the Product...

  • Page 110: Returned Product Procedures

    Manual. The warranty does not cover any unit that has been altered or modified so as to change its intended use. Any attempt to repair or alter any CETAC unit by anyone other than by CETAC authorized personnel or agents will void this warranty.

  • Page 111: Returned Product Warranty Determination

    ASXpress Rapid Sample Introduction System Operator’s Manual Troubleshooting the Rapid Sample Introduction System After CETAC’s examination, warranty or out of warranty status will be 7.3.4 Returned Product Warranty Determination determined. If a warranted defect exists, the product will be repaired at no charge and shipped prepaid back to the buyer.
  • Page 112 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 7: Troubleshooting the Rapid Sample Introduction System This page is intentionally blank.
  • Page 113 Glossary...

  • Page 114: Glossary

    ® FEP: Fluorinated Ethylene Propylene. Host Computer: The computer that controls operation of the ICP / ICP-MS instrument to which the CETAC autosampler is attached, and through which the ASXPRESS PLUS is controlled. Hz: Hertz I/O Auxiliary Port: The connector used for establishing communication and power between the ASX system and the autosampler.
  • Page 115 Guide to Operating a CETAC Autosampler Using a Terminal Program...

  • Page 116: Guide To Operating A Cetac Autosampler Using A Terminal Program

    Windows 2000 and later. (recommended) HyperTerminal. This program was supplied with versions of the Windows operating system through Windows XP. This chapter explains how to operate a CETAC autosampler using either of the two programs. 9.1 Using C-Term™...

  • Page 117: Configuring C-Term

    By default, C-Term attempts to open COM1 the first time it is executed. If the 9.1.3 Configuring C-Term COM port that the CETAC device is connected to is not the default (COM1), then it will be necessary to configure C-Term to use the desired port.

  • Page 118: Setting Preferences

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal The default communications configuration is appropriate for use with the vast Program majority of CETAC devices. Exceptions are the ASX-8000 which requires a baud rate change and the AS300 emulator which uses non-printing characters are part of its command protocol.

  • Page 119: Using Hyperterminal

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal Program Figure 9-5 Preferences Window To change the Scrollback Buffer Length, either type the new value in the field or use the arrows adjust the value up or down.
  • Page 120 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal Program Figure 9-6 “Connection Description” Window In the Connect To window, set Connect Using to COM 1, then click OK. Figure 9-7 “Connect To” Window In the Properties window, set Bits per second to 9600 and Flow control to None.
  • Page 121 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal Program “COM1 Properties” Window Figure 9-8 The HyperTerminal window will open. Click OK. Figure 9-9 “Com 1 Hyperterminal” Window 7. On the File menu, click Properties.
  • Page 122 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal Program 8. On the Settings tab, click ASCII Setup “Com 1 Properties” Window Figure 9-10 Click ASCII Setup. 10 Enable “Echo typed characters locally” and “Append line feeds to incoming line ends,”...

  • Page 123: Autosampler Commands

    Moves z-axis to upper most postion. Table 9-1 Autosampler Commands You can use these commands to determine if the CETAC autosampler is communicating and functioning properly. If more assistance is needed, please contact CETAC customer service.
  • Page 124 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 9: Guide to Operating a CETAC Autosampler Using a Terminal This page is intentionally blank. Program...
  • Page 125 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information Safety and Regulatory Information...

  • Page 126: Safety And Regulatory Information

    See page 10 for information on chemical compatibility. 10.1.2 Electrical Characteristics 10.1.2.1 Power requirements Electronics Module Input: Power is provided by the CETAC autosampler through the power/signal cable which is attached to the electronics module. DC Voltage and Current 24 V 2.5 A...
  • Page 127 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information 10.1.2.2 Input and output connectors All terminals allow a maximum current of 500MA @ 24VDC, unless otherwise noted. Auto Sampler Power and signal connection to a CETAC autosampler.

  • Page 128: Safety Notices

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information 10.2 Safety Notices If the equipment is used in a manner not specified by CETAC Technologies, the protection provided the equipment may be impaired. WARNING Repair or service that this not covered in this manual should only be performed by qualified personnel.

  • Page 129: Cleaning Instructions

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information For additional cleaning information, see “cleaning” in the index. 10.2.2 Cleaning Instructions To clean the exterior surfaces of the instrument, complete the following steps: Shut down and unplug the instrument.
  • Page 130 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information Warning symbol marked on equipment. This symbol means “Attention! Refer to the manual.” The WARNING notice denotes a hazard. It calls attention to a procedure, practice, or the like, that, if not correctly performed or adhered to, could WARNING result in personal injury.

  • Page 131: Avertissements En Français

    ASXpress Rapid Sample Introduction System Operator’s Manual Chapter 10: Safety and Regulatory Information 10.3 Avertissements en Français This section provides French translations of notices which may appear on the instrument or on other instruments used as part of the measurement system.

  • Page 132: Electromagnetic Interference

    The FCC requires the user to be notified that any changes or modifications made to this device that MODIFICATIONS are not expressly approved by CETAC Technologies may void the user's authority to operate the equipment. Connections to this device must be made with shielded cables with metallic RFI/EMI connector CABLES hoods to maintain compliance with FCC Rules and Regulations.
  • Page 133 Index...
  • Page 134 ASXpress Rapid Sample Introduction System Operator’s Manual Chapter : Index 11 Index 6-port valve power valve. See requirements, 17, 126 avertissements, 131 power-off procedure, 93 chemical compatibility, 10 power-on procedure, 92 cleaning, 96, 129 probe commands 1.0mm, 12, 56 autosampler, 123 carbon fiber, 56 condensation.
  • Page 136 480166 Manual Part Number Rev 4 Printed in USA...

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