Related Manuals for Ankom 2000
Summary of Contents for Ankom 2000
- Page 1 Operator’s Manual Rev 05/12/21 2052 O’Neil Rd, Macedon NY 14502 Telephone: (315) 986-8090 Fax: (315) 986-8091 www.ankom.com...
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Page 3: Table Of Contents
Instrument Description ..............................7 Safety Precautions ..............................10 Instrument Installation ............................... 11 Fiber Analysis Support Items ............................12 2000 Analysis Options using the ANKOM Fiber Analyzer ....................12 ADF Analysis ................................13 NDF Analysis ................................19 Crude Fiber Analysis ..............................25 Flush Procedure ................................ - Page 4 This page intentionally left blank...
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Page 5: Introduction
Filter Bags ANKOM Technology filter bags (part # F57 and F58) are designed to produce precision and accurate fiber results. The F57 bags should be used when grinding samples using a cutter type mill with a 1 mm screen which is typically referenced by the approved methods. -
Page 6: Contact Information
At ANKOM Technology we are committed to your total satisfaction and therefore always available to help you get the most from your ANKOM products. We are also very interested in any comments or suggestions you may have to help us improve. -
Page 7: Instrument Description
Process temperatures are precisely controlled while providing proper agitation to ensure a uniform flow of chemical solutions and rinses across each sample. 2000 Below are detailed views of the ANKOM Fiber Analyzer. Display... - Page 8 Operator’s Manual Port A – Used for Crude Fiber Acid solution and ND solution Vent Tube Water Supply Fitting Water Filter Line to Hot Water Supply Drain Hose Left Side View Port B – Used for Crude Fiber Base solution, AD solution, and Diluted Amylase Temperature Controller Domestic:...
- Page 9 Operator’s Manual Internal Components Valve B Pressure Transducer (part # 6121) Valve A A2000 Computer Check Valve & (part # A09) (part # A19 B) Assembly (part # A19 A) Fitting Assembly (part # A25) SICK Fiber Optic Module - for Instruments Analog Level delivered...
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Page 10: Safety Precautions
WARNING: Attempts to override safety features or to use this instrument in a manner not specified by ANKOM Technology voids the warranty and may result in serious injury or even death. This system is designed to meet and/or exceed the applicable standards of CE, CSA, NRTL and OSHA. -
Page 11: Instrument Installation
Fiber Analyzer you will need the following: • Adjustable wrench • 2000 Water supply located within 6 feet (3 meters) of the ANKOM and capable of heating water to 50°C for Crude Fiber and 70°C for ADF/NDF analyses • Adequate power (see “Operating Environment” section) •... -
Page 12: Fiber Analysis Support Items
ADF, NDF, or Crude Fiber analyses using custom digestion and rinse time settings. 2000 For maintenance purposes, the ANKOM also provides the capability to flush the solution lines. 2000 The following sections provide the information you will need to use and maintain the ANKOM Fiber Analyzer. pg. 12 Rev 05/12/21... -
Page 13: Adf Analysis
ADF Sample Preparation Procedure To prepare samples for fiber analysis, follow the procedure detailed below. 2000 When using the ANKOM Fiber Analyzer for ADF analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss. - Page 14 If your samples contain soybean products or >5% fat: 2000 Before doing the ADF analysis in the ANKOM , you will need to do a pre- extraction. For samples containing non-roasted soybean or >5% fat, follow the pre-extraction steps below: 1.
- Page 15 Fiber Analyzer If you are following the acid detergent procedure with an acid detergent lignin, you can find the lignin procedure on our website at www.ankom.com. To perform ADF analysis on prepared samples, follow the procedure detailed below. If you are changing from one analysis type to another, flush the system before running.
- Page 16 Operator’s Manual Press ENTER on the Keypad and follow the prompts on the Display to set up the instrument for ADF analysis. Close the Vessel Lid and tighten it by turning the Vessel Clamp Handle. If you do not want to use the Cubitainers to automatically add your solutions, you can manually fill the vessel for each procedure.
- Page 17 Blank bag correction (running average of final oven-dried weight divided by original blank bag weight) If you are following the acid detergent procedure with an acid detergent lignin, you can find the lignin procedure on our website at www.ankom.com. Rev 05/12/21 pg. 17...
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Page 19: Ndf Analysis
NDF Sample Preparation Procedure To prepare samples for fiber analysis, follow the procedure detailed below. 2000 When using the ANKOM Fiber Analyzer for NDF analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss. - Page 20 If your samples contain soybean products or >5% fat: 2000 Before doing the NDF analysis in the ANKOM , you will need to do a pre- extraction. For samples containing non-roasted soybean or >5% fat, follow the pre-extraction steps below: 1.
- Page 21 Operator’s Manual 2000 NDF Analysis Procedure using the ANKOM Fiber Analyzer To perform NDF analysis on prepared samples, follow the procedure detailed below. • If you are changing from one analytical method to another, flush the system before running. See the “Flush Procedure” section of this manual for more information.
- Page 22 Operator’s Manual 11. Press the arrow keys on the Keypad until you see “Select NDF” on Select NDF the Display. v <Enter> The NDF analysis will use the following default settings: • 75 minute digestion • four 5 minute rinses If you want to run a custom NDF analysis that allows you to set the digestion time and the number of rinses, press the arrow keys until you see “Select Custom”...
- Page 23 Operator’s Manual 20. Remove the bags from the beaker and place them on a wire screen to air-dry. – Do NOT place bags in an oven until all acetone has Hazardous Materials evaporated. 21. Place air-dried bags in the oven and heat at 102°C ± 2° for 2 – 4 hours (depending on the oven). When running a lignin procedure or a sequential (NDF/ADF or NDF/ADF/Lignin) with F57 Filter Bags it is important not to dry the bags overnight after the NDF or ADF procedure.
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Page 25: Crude Fiber Analysis
Crude Fiber Sample Preparation Procedure To prepare samples for fiber analysis, follow the procedure detailed below. 2000 When using the ANKOM Fiber Analyzer for Crude Fiber analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss. - Page 26 For all samples you will need to do a pre-extraction of fat. 2000 Before doing a Crude Fiber analysis in the ANKOM , follow the pre- extraction steps below: 1. Place the filter bags with sample into an appropriately sized container.
- Page 27 Operator’s Manual 2000 Crude Fiber Analysis Procedure using the ANKOM Fiber Analyzer To perform Crude Fiber analysis on prepared samples, follow the procedure detailed below. If you are changing from one analysis type to another, flush the system before running. See the “Flush Procedure” section of this manual for more information.
- Page 28 Operator’s Manual Close the Vessel Lid tightening it by turning the Vessel Clamp Handle. 10. Press START on the Keypad. Solution will flow first into the vessel through Port A. Once the analysis begins, digestions and rinses occur automatically, with the analyzer Display providing information about the process time remaining, the temperature, and the pressure.
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Page 29: Flush Procedure
Operator’s Manual Flush Procedure The Flush procedure allows you to clean the system with water. This procedure should be used when changing from one procedure to another (e.g., when preparing to do an ADF analysis after completing an NDF analysis) or when doing an NDF procedure after a previous NDF procedure with more than two hours between procedures, or before storing the instrument. - Page 30 Operator’s Manual This page intentionally left blank pg. 30 Rev 05/12/21...
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Page 31: Periodic Maintenance
Operator’s Manual Periodic Maintenance Initial Maintenance (after 10 hours of operation) After the first 10 hours of operation, follow the procedure below: Maintenance Alert Collector Packing Nut Remove the back panel of the instrument. Inspect the Maintenance Alert Collector. Clean any residue from the collector. Unscrew the filter body (the fixture on the outside of the instrument that attaches to the water supply). - Page 32 Operator’s Manual Replace the Fuses (as needed) 2000 To replace the fuses in the ANKOM Fiber Analyzer, follow the procedure detailed below. Turn off the instrument power and unplug the Power Cord from the outlet. Using a flat blade screwdriver, twist the slot on the fuse holders counterclockwise ¼...
- Page 33 Operator’s Manual Check the Agitation System The agitation system should be checked every three to six months or if fiber values are higher than normal or inconsistent. To check the agitation system, follow the steps below. Poor agitation will cause higher analysis values and poor repeatability. Check the function of the agitator motor.
- Page 34 (Place the thermometer near the probe at the bottom of the vessel.) Thermometer c. The temperature shown on the display. _______˚C Temperature Probe If these three temperatures are not within ½ degree of each other, contact ANKOM Technology for assistance. Send results to service@ankom.com. pg. 34 Rev 05/12/21...
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Page 35: Troubleshooting & Replacement Parts
Concave Tray Troubleshooting & Replacement Parts The ANKOM Technology web site has the most current troubleshooting and replacement parts information. 2000 Therefore, if you have any questions about the operation of your ANKOM Fiber Analyzer, or if you need replacement parts, please visit our web site at www.ankom.com. -
Page 36: Appendix A - Analytical Procedures
The inclusion of at 2000 each sample to ensure uniformity of extraction (ANKOM least one blank bag in each run is mainly used as an indicator with 65rpm agitation, ANKOM Technology). - Page 37 Vessel and place the Bag Suspender Weight on top of the empty 9 tray to keep the Bag Suspender submerged. 2000 13. Follow the instructions on the ANKOM display: Select ADF. Close the Vessel Lid. Confirm hot water is on (>70°C).
- Page 38 O (premixed chemical solution available from acetone into the container to cover the bags and secure the ANKOM Technology). Check that pH is from 6.9 to 7.1. Agitate top. Shake the container 10 times and pour off the acetone. and heat to aid solution.
- Page 39 Once agitation begins, close the Vessel Lid and follow the rest of the procedure from step 13 to the end. 2000 12. Follow the instructions on the ANKOM display: Select NDF. (Wait to close the Vessel Lid.) Confirm hot water is on (>70°C).
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Page 40: Appendix B - Wiring Diagrams (1 Of 4)
Operator’s Manual Appendix B – Wiring Diagrams (1 of 4) pg. 40 Rev 05/12/21... - Page 41 Operator’s Manual Appendix A – Wiring Diagrams (2 of 4) Rev 05/12/21 pg. 41...
- Page 42 Operator’s Manual Appendix A – Wiring Diagrams (3 of 4) pg. 42 Rev 05/12/21...
- Page 43 Operator’s Manual Appendix A – Wiring Diagrams (4 of 4) Rev 05/12/21 pg. 43...
- Page 44 Automation saves time and money! ANKOM Technology is an international company with products that include… FLEX Analyte Extractor • Simplifies fat-soluble vitamin and cholesterol analysis • Crude and total fat analysis capability coming soon • Eliminates chemical handling to improve safety •...
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