Ankom ANKOM200 FIBER ANALYZER Operator's Manual

Ankom ANKOM200 FIBER ANALYZER Operator's Manual

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Operator's Manual
Rev 1/24/20
2052 O'Neil Rd, Macedon NY 14502
Telephone: (315) 986-8090
Fax: (315) 986-8091
www.ankom.com

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  • Page 1 Operator’s Manual Rev 1/24/20 2052 O’Neil Rd, Macedon NY 14502 Telephone: (315) 986-8090 Fax: (315) 986-8091 www.ankom.com...
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  • Page 3: Table Of Contents

    Instrument Description ..............................7 Safety Precautions ................................ 9 Instrument Installation ............................... 10 Fiber Analysis Support Items ............................11 Analysis Options using the ANKOM Fiber Analyzer ....................11 ADF Analysis ................................13 NDF Analysis ................................19 Crude Fiber Analysis ..............................23 Periodic Maintenance ..............................
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  • Page 5: Introduction

    Filter Bags ANKOM Technology filter bags (part # F57 and F58) are designed to produce precision and accurate fiber results. The F57 bags should be used when grinding samples using a cutter type mill with a 1 mm screen which is typically referenced by the approved methods.
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  • Page 7: Instrument Description

    Process temperatures are precisely controlled while providing proper agitation to ensure a uniform flow of chemical solutions and rinses across each sample. Below are descriptions of specific features and functions of the ANKOM Fiber Analyzer.
  • Page 8 Operator’s Manual Internal Components (Rear View) Packing Maintenance Alert Collector (part # F27) External Components (Rear View) Maintenance Alert Reservoir pg. 8 Rev 1/24/20...
  • Page 9: Safety Precautions

    WARNING: Attempts to override safety features or to use this instrument in a manner not specified by ANKOM Technology voids the warranty and may result in serious injury or even death. This system is designed to meet and/or exceed the applicable standards of CE, CSA, NRTL and OSHA.
  • Page 10: Instrument Installation

    Operator’s Manual Instrument Installation Site Requirements To install and operate the ANKOM Fiber Analyzer you will need the following: • Adjustable wrench • Water supply and capability of heating water to 50°C for Crude Fiber and 70°C for ADF/NDF analyses •...
  • Page 11: Fiber Analysis Support Items

    Analysis Options using the ANKOM Fiber Analyzer The ANKOM Fiber Analyzer can be used for ADF, NDF, and Crude Fiber analyses. The following sections provide the information you will need to use and maintain the ANKOM Fiber Analyzer. Rev 1/24/20 pg. 11...
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  • Page 13: Adf Analysis

    ADF Sample Preparation Procedure To prepare samples for fiber analysis, follow the procedure detailed below. IMPORTANT: When using the ANKOM Fiber Analyzer for ADF analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss.
  • Page 14 IMPORTANT: If your samples contain soybean products or >5% fat… Before doing the ADF analysis in the ANKOM , you will need to do a pre- extraction. For samples containing non-roasted soybean or >5% fat, follow the pre-extraction steps below: Place the filter bags with sample (up to 23) into a container with a top.
  • Page 15 Fiber Analyzer If you are following the acid detergent procedure with an acid detergent lignin, you NOTE: can find the lignin procedure on our website at www.ankom.com. To perform the ADF analysis on prepared samples, follow the procedure detailed below. IMPORTANT: The Vessel must be at room temperature before beginning an ADF analysis.
  • Page 16 Operator’s Manual 16. When the Timer sounds, the rinse is complete. Slowly open the Exhaust Valve to drain the hot water. 17. Repeat steps 12 - 16 to accomplish the second rinse. HEAT 18. Make sure that the button is off (not lit) so that pH can be checked after the third rinse. 19.
  • Page 17 Blank bag correction (running average of final oven-dried weight divided by original blank bag weight) If following the acid detergent procedure with an acid detergent lignin, the procedure NOTE: can be found on our website at www.ankom.com. Rev 1/24/20 pg. 17...
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  • Page 19: Ndf Analysis

    To prepare samples for fiber analysis, follow the procedure detailed below. IMPORTANT: When using the ANKOM Fiber Analyzer for NDF analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss. A running average of the blank bag weights is used in the fiber calculation as the C correction factor.
  • Page 20 If your samples contain soybean products or >5% fat… IMPORTANT: Before doing the NDF analysis in the ANKOM , you will need to do a pre- extraction. For samples containing non-roasted soybean or >5% fat, follow the pre- extraction steps below: Place the filter bags with sample (up to 23) into a container with a top.
  • Page 21 Operator’s Manual NDF Analysis Procedure using the ANKOM Fiber Analyzer To perform NDF analysis on prepared samples, follow the procedure detailed below. IMPORTANT: The Vessel must be at room temperature before beginning an NDF analysis. Verify that the Exhaust Hose is connected to the instrument and securely positioned in the drain.
  • Page 22 Operator’s Manual 20. With your hands, gently press out excess water from the bags into the beaker and pour off the water from the beaker. 21. With the bags in a beaker, add enough acetone to cover them. Let the bags soak in acetone for 3 - 5 minutes.
  • Page 23: Crude Fiber Analysis

    To prepare samples for fiber analysis, follow the procedure detailed below. IMPORTANT: When using the ANKOM Fiber Analyzer for Crude Fiber analysis, at least one blank filter bag should be included with the sample set as an indicator of particle loss.
  • Page 24 IMPORTANT: For all samples you will need to do a pre-extraction of fat before doing a Crude Fiber analysis in the ANKOM . Follow the pre-extraction steps below: Place the filter bags with sample into an appropriately sized container.
  • Page 25 Operator’s Manual Crude Fiber Analysis Procedure using the ANKOM Fiber Analyzer To perform Crude Fiber analysis on prepared samples, follow the procedure detailed below. IMPORTANT: The Vessel must be at room temperature before beginning a Crude Fiber analysis. Verify that the exhaust hose is connected to the instrument and securely positioned in the drain.
  • Page 26 Operator’s Manual 19. Press the HEAT AGITATE buttons on the front of the instrument so they are lit. Look in the Vessel to confirm agitation. 20. Close the Vessel Lid. 21. On the Timer/Clock, set the Timer to 40 minutes and press the Start/Stop button. 22.
  • Page 27 Operator’s Manual 39. Remove one filter bag from the Desiccant Pouch. Flatten the pouch to remove ambient air. To prevent moisture from settling on the filter bags, it is important to keep ambient air out of the Desiccant Pouch while weighing the bags. This can be done by holding IMPORTANT: the pouch flat or zipping it shut after removing filter bags.
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  • Page 29: Periodic Maintenance

    Operator’s Manual Periodic Maintenance Initial Maintenance (after 10 hours of operation) Follow the procedure below: After every 3 hours of use check the Maintenance Alert Reservoir for any fluid accumulation. If any fluid is present, unscrew the Reservoir bottle and empty the fluid.
  • Page 30 Re-install the fuse holder into the instrument. Fuse Reset/replace the Circuit Breaker in a 220V instrument To reset/replace the circuit breaker in a 220V ANKOM Fiber Analyzer, follow the procedure detailed below. Turn off the instrument power and unplug the Power Cord from the outlet.
  • Page 31 Operator’s Manual Check the Agitation System The agitation system should be checked every three to six months or if fiber values are higher than normal or inconsistent. To check the Agitation System, follow the procedure detailed below. IMPORTANT: Poor agitation will cause higher analysis values and poor repeatability. Check the function of the agitator motor.
  • Page 32 3. Open the Vessel Lid. Vessel 4. Place approximately 1800ml of room temperature water (about 20˚C) in the empty ANKOM digestion vessel, leaving the Bag Suspender out of the Vessel. 5. Press the red HEAT and blue AGITATE buttons on the front of the HEAT instrument so that they are lit.
  • Page 33 AAc.01l on Display 2. 11. Press 12. Press on the controller to save the calibration. The ANKOM controller is now calibrated. The instrument will boil water at the calibrated temperature and maintain the proper temperature throughout an assay. Rev 1/24/20...
  • Page 34: Storage

    Operator’s Manual Check the Bag Suspender he Bag Suspender should be checked every three to six months or if fiber values are higher than normal or inconsistent. To check the Bag Suspender, follow the procedure detailed below. Verify that you are using the version of the Bag Suspender Trays.
  • Page 35: Troubleshooting & Replacement Parts

    Operator’s Manual Troubleshooting & Replacement Parts The ANKOM technology web site has the most current troubleshooting and replacement parts information. Therefore, if you have any questions about the operation of your ANKOM Fiber Analyzer, or if you need replacement parts, please visit our web site at www.ankom.com.
  • Page 36: Appendix A - Wiring Diagram

    Operator’s Manual Appendix A – Wiring Diagram pg. 36 Rev 1/24/20...
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  • Page 38 Automation saves time and money! ANKOM Technology is an international company with products that include… TDF Dietary Fiber Analyzer • Automates AOAC 991.43, 985.29, 2009.01, and 2011.25 (and associated AACC methods) • IDF/SDF and TDF values • Faster, Technician-free Filtering •...

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