Related Manuals for Cannon PolyVISC SPS
Summary of Contents for Cannon PolyVISC SPS
- Page 1 CANNON® PolyVISC® SPS Solution Preparation System PolyVISC® SPS Operators Manual P/N 67.9995...
- Page 3 PolyVISC® SPS Operators Manual Cannon Instrument Company® 2139 High Tech Road State College, PA 16803...
- Page 4 PolyVISC SPS Operators Manual Copyright Copyright © 2018 Cannon Instrument Company®. All rights reserved. Trademarks CANNON®, the CANNON® logo, and Cannon Instrument Company® are registered trademarks of CANNON Instrument Company®. VISCPRO® and the VISCPRO® logo are registered trademarks of Cannon Instrument Company. Contact...
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Page 5: Table Of Contents
PolyVISC SPS Operators Manual Contents Overview........................... 1 Related Documents ........................1 Specifications / Compliances ......................2 Notes/Cautions/Warnings ......................4 Safety Precautions ........................4 Unpacking and Installation ....................7 Unpack and Inspect ........................7 Setup the Solution Preparation System ..................9 Physical Arrangements ...................... - Page 6 PolyVISC SPS Operators Manual Specifications........................28 Warranty ........................30 Products limited warranty ......................30 Reagent and chemical warranty ....................30 Returning a product to CANNON ....................31 Required information ......................31 Hazardous materials ....................... 31 Shipping notification ....................... 32 Replacement Parts List .....................33 List of Figures Figure 1 —...
- Page 7 Table 11 — Advanced settings ......................22 Table 12 — Mettler Toledo XS204 Precision Balance* ..............28 Table 13 — TITRONIC® 300 Piston Burette* ................... 29 Table 14 — TITRONIC® universal Piston Burette* ................29 Table 15 — PolyVISC SPS replacement parts ................... 33...
- Page 8 PolyVISC SPS Operators Manual...
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Page 9: Overview
PolyVISC. This system consists of a titrator for dispensing solvent, a scale for measuring the prepared solution, and the CANNON SPS software on a Windows® PC for managing the operation. Using a gravimetric method of measurement, the SPS achieves an accurate concentration measurement within ±... -
Page 10: Specifications / Compliances
50% at 40 °C , non-condensing, Installation Category II, Pollution Degree 2 Compliance CE Mark: EMC Directive (2004/108/EC); Low Voltage Directive (2006/95/EC) * Specifications provided for convenience. Refer to manufacturer’s specifications and Declaration of Conformance for official specifications. Polyvisc SPS Operators Manual... -
Page 11: Table 4 - Titronic® Universal Piston Burette
50% at 40 °C , non-condensing, Installation Category II, Pollution Degree 2 Compliance CE Mark: EMC Directive (2004/108/EC); Low Voltage Directive (2006/95/EC) * Specifications provided for convenience. Refer to manufacturer’s specifications and Declaration of Conformance for official specifications. CANNON Instrument Company® | Overview... -
Page 12: Notes/Cautions/Warnings
Please observe the following general safety precautions for proper and safe operation of the equipment. • Only qualified personnel should operate the CANNON SPS. • Make sure that you read and understand all operating instructions and safety precautions listed in this manual before installing or operating your unit. If you have questions regarding instrument operation or documentation, contact Cannon Instrument Company. - Page 13 Never operate the equipment with a damaged MAINS AC power cable. Use only the manufacturer-supplied MAINS AC power cable. This cable must be inserted into a receptacle with a protective earth ground. symbol indicates the OFF position for the electrical switches for your unit. CANNON Instrument Company® | Overview...
- Page 14 Polyvisc SPS Operators Manual...
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Page 15: Unpacking And Installation
PolyVISC SPS Operators Manual Unpacking and Installation Unpack and Inspect Unpack and inspect all CANNON PolyVISC SPS components and accessories as soon as you receive them. Caution: Many components are fragile. Use caution when moving and handling the SPS and accessories. -
Page 16: Table 6 - Packing List
67.0459 Serial cable gender changer 67.0467 Top glass plate, single solvent 67.0470 Top glass plate, dual solvent 67.0471 Dispensing tube, dual tip 67.1025 Titrator to titrator cable 67.1027 Solvent filter, 20 Micron 65.0047 StaticMaster Bar 67.1029 Polyvisc SPS Operators Manual... -
Page 17: Setup The Solution Preparation System
Figure 1 shows an arrangement with 2 titrators. Titrator 1 Computer Balance Titrator 2 Figure 1 — Arrangement of solution preparation system CANNON Instrument Company® | Unpacking and Installation... -
Page 18: Communication Cables Setup
5. Connect the Mini-DIN-4 on the balance cable to the RS2 port on either titrator #1 (single titrator system) or titrator #2 (dual titrator system). 6. Connect the serial cable gender changer to the serial port on the balance. 7. Connect the DB9 on the balance cable to the balance. Polyvisc SPS Operators Manual... -
Page 19: Figure 2 - Communication Setup: Single Titrator System
Figure 2 — Communication setup: single titrator system Figure 3 — Communication setup: dual titrator system (Titronic 300) Note: On Titronic Universal titrators, the RS1 port is on top Refer to Figure 4 and Figure 5. CANNON Instrument Company® | Unpacking and Installation... -
Page 20: Figure 4 - Universal Titrator Communication Setup - Single Titrator
Figure 4 — Universal Titrator Communication Setup – single titrator Figure 5 — Universal Titronic Cable Connection Setup – dual titrators Polyvisc SPS Operators Manual... -
Page 21: Solvent Hose Setup
7. Connect a solvent hose from the top of the burette to port 2 on the titrator. 8. Connect a solvent hose from port 3 on the titrator to the dispensing tube. 9. Place the StaticMaster Bar on the metal scale of the balance. CANNON Instrument Company® | Unpacking and Installation... -
Page 22: Figure 6 - Hose Setup: Single Titrator System
Figure 6 — Hose setup: single titrator system Figure 7 — Hose setup: dual titrator system Note: Dual titrator systems require two P61.5085 fittings and two P61.5086 fittings. Polyvisc SPS Operators Manual... -
Page 23: Install Sps Software
Install SPS software Note: If you purchased a computer from Cannon Instrument Company, the SPS software will be pre-installed at the factory. Software installation simply loads the program onto the computer and creates shortcuts. No configuration settings are entered during software installation. -
Page 24: Sps Software Configuration
PolyVISC SPS Operators Manual SPS Software Configuration Before attempting to prepare solutions, you must set the configuration options for the PolyVISC SPS software. Software configuration options only need to be set when the SPS system is initially installed and when changes are made to the system, for example, when a different balance is used or when different solvents are used. -
Page 25: Table 9 - Hardware Settings
600, 1200, 2400, 4800, 9600 Must match the baud rate, parity, Parity None, add, even and bit of titrator #1. 8 Bit / 7 Bit Radio buttons 4. Click to save your changes. CANNON Instrument Company® | SPS Software Configuration... -
Page 26: Configure Method
/ g Solvent Radio buttons Selects test method (weight-to-weight, g / g Solution weight-to-volume, etc.) g / mL Solution Units in Percent Check box Divides target value by 100 Dissolution Volume Change (active only for g/mL Solution) Polyvisc SPS Operators Manual... - Page 27 0 to 100 with 2 Percent purity of polymer solute decimal precision (impurities are treated as insoluble) Export Blank ARV Factor Solvent 1/Solvent 2 Single Dose Radio buttons Single Dose dispenses solvent in a Titration single dose. CANNON Instrument Company® | SPS Software Configuration...
- Page 28 .001 to 1000 with 3 Density of solvent at test temperature decimal precision Percentage (%) 0 to 100 with 2 Percent of the solvents used relative decimal precision to the total solvent used. Set to 100% for single solvent system Polyvisc SPS Operators Manual...
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Page 29: Equations
( polymer mass × polymer purity ) + solvent mass concentration solvent mass � � � + � � Actual solvent� = solvent mass polymer mass × polymer purity density solvent test density polymer density CANNON Instrument Company® | SPS Software Configuration... -
Page 30: Configure Advanced Settings
Maximum time period acceptable for a communication Increment Balance (s) response to the controlling software from the balance during the titration cycle. 4. Click to save your changes. Polyvisc SPS Operators Manual... -
Page 31: Using The Label Printer
Select the label printer from the drop-down list, and use the spin controls to choose the desired number of labels to be printed for the solution. Then click OK to close the Print window and print the solution label. CANNON Instrument Company® | SPS Software Configuration... -
Page 32: Preparing Solutions
PolyVISC SPS Operators Manual Preparing Solutions The SPS sample preparation process is a semi-automatic process that uses a sophisticated computer program to calculate and dispense quantities of solvent to prepare the desired concentration of solution. The user is responsible for adding solute to the sample vial in the correct proportions when prompted by the computer. -
Page 33: Preparing A Solution
2. To select solution preparation procedures to run, click the R column to display a “+”. 3. If this is the first sample that you are running, click the Start button. For any remaining solution, click the button. CANNON Instrument Company® | Preparing Solutions... -
Page 34: Saving Solution Preparation Data
If you are using the miniPV or miniPV-HX Automatic Viscometer from CANNON, this file can be used to import solution concentration data directly into the VISCPRO II database. Samples tested with the miniPV or miniPV-HX must be assigned the same numeric Sample ID as the SPS-generated Sample ID in order for the import to be successful. -
Page 35: Recalling Solution Data
100 mL capacity. Additional information on burette operation is also available in the Operating Instructions, including installation, troubleshooting, maintenance, serial communication, and order information for replacement parts. CANNON Instrument Company® | Preparing Solutions... -
Page 36: Specifications
PolyVISC SPS Operators Manual Specifications Table 12 — Mettler Toledo XS204 Precision Balance* Specifications Details Model XS204 Maximum capacity 220 g Readability 0.1 mg Power supply 100 to 240 V , 50/60 Hz, 30 VA Operating conditions 5 °C to 40 °C, max. relative humidity 80% at 31 °C linearly decreasing to 50% at 40 °C , non-condensing, Installation... -
Page 37: Table 13 - Titronic® 300 Piston Burette
50% at 40 °C , non-condensing, Installation Category II, Pollution Degree 2 Compliance CE Mark: EMC Directive (2004/108/EC); Low Voltage Directive (2006/95/EC) * Specifications provided for convenience. Refer to manufacturer’s specifications and Declaration of Conformance for official specifications. CANNON Instrument Company® | Specifications... -
Page 38: Warranty
Company. Reagent and chemical warranty Cannon Instrument Company® (“the Company”) warrants all reagents and chemicals sold by the Company and delivered to and retained by their original purchasers to conform to the weight, specifications and standards stated on the package. The Company will, at its sole option, either... -
Page 39: Returning A Product To Cannon
Returning a product to CANNON Before returning a CANNON product for repair or service, make every attempt to identify the problem. If, after careful checking, the problem remains unidentified or unsolved, telephone Cannon Instrument Company (or the local service agent) to consult with a product specialist. If the specialist cannot recommend a simple solution or repair, CANNON will authorize the return of the product through the issuance of a Return Authorization number (RA). -
Page 40: Shipping Notification
Shipping notification Products returned without prior notification (by either telephone or fax), or without Cannon’s authorization, will not be accepted. The customer may be billed a testing fee if a product is returned to CANNON and found to be working properly. -
Page 41: Replacement Parts List
PolyVISC SPS Operators Manual Replacement Parts List Table 15 — PolyVISC SPS replacement parts Description Part Number TITRONIC® 300 Piston Burette 67.0475 Titrator cable 67.0461 Mettler Toledo XS204 Precision Balance 67.0555 PolyVISC® SPS Software 67.9997 PolyVISC® SPS Operator’s Manual 67.9995 Dispenser assembly, single tip 67.0450... - Page 42 Polyvisc SPS Operators Manual...
- Page 43 CANNON Instrument Company® 2139 High Tech Road State College, PA 16803...
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