Analytik Jena SPECORD 200 PC Operating Manual
  1. Manuals
  2. Brands
  3. Analytik Jena Manuals
  4. Measuring Instruments
  5. SPECORD 200 PC
  6. Operating manual

Analytik Jena SPECORD 200 PC Operating Manual

Uv vis spektralphotometer
Hide thumbs
Table of Contents

Advertisement

Quick Links

UV VIS Spektralphotometer
SPECORD
SPECORD
SPECORD
Analytik Jena AG
   
200
   
205
   
210
Operating Manual
PC
PC
PC

Advertisement

Table of Contents
loading
Need help?

Need help?

Do you have a question about the SPECORD 200 PC and is the answer not in the manual?

Questions and answers

Related Manuals for Analytik Jena SPECORD 200 PC

Summary of Contents for Analytik Jena SPECORD 200 PC

  • Page 1 UV VIS Spektralphotometer     SPECORD     SPECORD     SPECORD Operating Manual Analytik Jena AG...
  • Page 2 Hotline: + 49 (3641) 77-7401 Fax: + 49 (3641) 77-7449 E-Mail: service@analytik-jena.de General information about Analytik Jena AG on the internet: http://www.analytik-jena.de Copyrights and Trademarks Microsoft, Windows 98, Windows NT, MS Word, MS Excel are registered trademarks of Microsoft Corp.

  • Page 3: Table Of Contents

    Note on the service life of lamps ................36 9.3.2 Opening the flap of the lamp compartment............. 36 9.3.3 Changing the deuterium lamp ................38 9.3.4 Changing the halogen lamp ................... 41 ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 1 Analytik Jena AG...
  • Page 4 ® Contents SPECORD Changing the desiccator ..................43 Changing fuses ...................... 44 Index to Illustrations Index to Overviews ® Page 2 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 5: Introduction Conventions

    For easier navigation within the manual, the manual uses the following system: • Chapters and illustrations are numbered consecutively. • Every illustration has its own caption. ■ This symbol denotes a step of operation. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 3 Analytik Jena AG...

  • Page 6: Intended Use Of The Specord

    ® Page 4 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 7: Safety Notes

    Emergency stop! ® In the case of emergency, disconnect the SPECORD and its components from line power by removing the power plug from the power outlet. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 5 Analytik Jena AG...
  • Page 8 Heat accumulation might result in overheating and faults on the device. ® Make sure not to cover the ventilation slots of the SPECORD ® Before you switch on the SPECORD , remove its dust cover! ® Page 6 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 9 • DIN EN 61010-1 (IEC 1010-1) • 73/23/EC • 89/336/EC. ® The SPECORD meets the requirements as per Protection Type IP 20. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 7 Analytik Jena AG...
  • Page 10 ® Safety notes SPECORD ® Page 8 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 11: Disposal

    When the service life of the device is over, dispose of the device with its electronic components as electronic scrap observing the relevant regulations. ® You can also return the SPECORD to Analytik Jena AG for disposal. Please contact our Technical Service. ® SPECORD 200/205/210 User's Manual –...
  • Page 12 ® Disposal SPECORD ® Page 10 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 13: Technical Data Of The Spectrophotometers

    1 / 2 / 4 nm, variable 1.4 nm 0.5 / 1 / 2 / 4 nm, variable Toluene / hexan > 2.1 > 1.7 > 2.1 resolution ® Overview 4-1 Technical data of SPECORD ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 11 Analytik Jena AG...

  • Page 14: General Technical Data Of Specord

    Data interface RS-232 port PC requirements for software: MS Windows 2000 operating system or higher Aspect Plus and WinASPECT ® Overview 4-2 General technical data of SPECORD ® Page 12 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 15: Device Description And Operating Principle Mechanical Design Of Specord

    Spectrometer The spectrometer system is protected against system extraneous light and dust by cover . The desiccator regulates the humidity inside the system. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 13 Analytik Jena AG...
  • Page 16 ® the SPECORD 200/210. Device control The device control computer coordinates the interaction computer of the subassemblies involved in the measurement processes. ® Page 14 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 17: Design Of Subassemblies

    To obtain the maximum possible energy of the deuterium lamp for the measurement, you can sensitively adjust the setscrew for mirror adjustment ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 15 Analytik Jena AG...

  • Page 18: Spectrometer System And Photometer Section

    1, 2, 4 nm ® SPECORD 1.4 nm ® SPECORD 0.5, 1, 2, 4 nm. The imaging grating disperses the incident light and spreads it out into a spectrum. ® Page 16 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 19: Sample Compartment

    Mount for cell holder Reserve connector Conduit for sample drain hose Stopper for optical fiber of measuring probe Conduits for sample-aspirating hoses (sipper) Conduits for coolant hoses ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 17 Analytik Jena AG...
  • Page 20 Two openings in the front of the device cover are provided for the aspiration tubes of the super sipper system. The illustration below shows the geometrical dimensions of the sample compartment. ® Page 18 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 21 ® SPECORD Device description and operating principle Design of subassemblies Fig. 5-5 Dimensions of sample compartment Front side of sample compartment Detector side ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 19 Analytik Jena AG...
  • Page 22 ® Device description and operating principle SPECORD Design of subassemblies ® Page 20 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 23: Installation Requirements

    Do not expose the device to direct sunlight or the radiation of heaters. • Temperature range: + 15 ... + 35 °C • Humidity: up to 90 % (at + 30 °C) ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 21 Analytik Jena AG...
  • Page 24 ® Installation requirements SPECORD ® Page 22 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 25: Installation And Start-Up

    E lamp ON indicator LED (yellow) Halogen lamp ON indicator LED (red) ® The LEDs light when the SPECORD has been switched on and the lamps are on. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 23 Analytik Jena AG...
  • Page 26 Fig. 7-3 Connectors on right-hand side panel RS 232 port for PC Connector for xyz autosampler USB port for PC Connector for control of Peltier temperature-controlled cell holder ® Page 24 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 27: Removing The Transport Lock

    The transport lock screw is not removed from the device, but is left in its holder in ® the SPECORD If the device must be transported again or returned for repair to Analytik Jena AG, lock the transport lock again. Releasing the transport lock...

  • Page 28: Connecting The Specord

    Spare fuses 5 x 20 T 3.15 A L ® • User's Manuals for the SPECORD , the accessories and the ® WinASPECT control and analysis software. ® Page 26 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 29 (multiple socket outlet, if possible). Note When required, align the lamps following the instructions given in Section 9.3 Changing lamps, p. 36 after start-up. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 27 Analytik Jena AG...

  • Page 30: Start-Up

    COM port for the SPECORD – PC connection: Activate the menu command < Measurement I Set Parameters > to open the window of the device driver SPECORD xxx ..® Page 28 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 31 Please note that the SPECORD reaches thermal stability only after a warm-up time of one hour. Therefore, you should not start precision measurements unless the device has warmed up. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 29 Analytik Jena AG...

  • Page 32: Switching The Device Off

    If you have finished the measurements on the SPECORD but want to analyze the ® obtained results on the PC, you can also switch off the SPECORD without shutting down the computer before. ® Page 30 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 33: Accessories

    The beam transmits the cells at a height of approximately 5 to 15 mm above the support of the cell holder. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 31 Analytik Jena AG...

  • Page 34: Receptacle For Cells With Turbid Samples

    (Fig. 5-4 (8) p.17). The receptacles can accommodate standard cells of 10 mm pathlength. Remove the foamed-plastic caps covering the cell receptacles and insert the cells for the analysis. ® Page 32 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 35: Additional Accessories

    • 75-mm integrating sphere for transmission and diffuse reflectance • PTC 100, Peltier temperature-controlled cell holder • PTC 600, Peltier temperature-controlled 6-cell changer • SMA fiber connector ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 33 Analytik Jena AG...
  • Page 36 ® Accessories SPECORD Additional accessories ® Page 34 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 37: Care, Maintenance, Lamp Change

    Care, maintenance, lamp change Care and maintenance The SPECORD is largely free of maintenance. To ensure your laboratory certification with device validation, Analytik Jena AG offers you a service/maintenance agreement. User care and maintenance is limited to the following operations: •...

  • Page 38: Changing Lamps

    Remove the flap of the lamp compartment by lifting it from below by 1 to 2 mm and then pulling it off to the left. ® Page 36 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 39 Fig. 9-2 Open lamp compartment Protective cover of halogen lamp Protective cover of deuterium lamp Knurled screw of halogen lamp sleeve Top part of deuterium lamp cover ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 37 Analytik Jena AG...

  • Page 40: Changing The Deuterium Lamp

    The performance of the lamp will deteriorate by contamination. Before you can change the lamp, remove the top part of the protective cover ( Fig. 9-2 ) by pulling it upward. ® Page 38 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 41 Screw down the deuterium lamp by means of both quick-lock nuts. Fasten the connector to the lamp. Finally, reattach the top part of the protective cover. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 39 Analytik Jena AG...
  • Page 42 Finally, close the flap of the lamp compartment. Note Please note that the deuterium lamp needs a warm-up of one hour after ignition to reach full thermal stability. ® Page 40 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...

  • Page 43: Changing The Halogen Lamp

    Do not touch the glass bulb of the new halogen lamp! Any contamination will impair the lamp performance. Reattach the protective cover of the halogen lamp and refasten it. ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 41 Analytik Jena AG...
  • Page 44 In this case, the ideal wavelength is 500 nm. Note Please note that the halogen lamp needs a warm-up of about one hour after switch on to reach full thermal stability. ® Page 42 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 45 Used up desiccators can be reused after heating them up for five hours in a drying oven. New desiccators are available from our Service Department (→ for the address, refer to the inside cover page). ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 43 Analytik Jena AG...
  • Page 46 Close the fuse holder again. ® Reconnect the power cable to the power input connector of the SPECORD the power outlet. ® Switch the SPECORD on again. ® Page 44 SPECORD 200/205/210 User's Manual – Edition 03/2003 Analytik Jena AG...
  • Page 47 Lamp protective cover partly removed............... 39 Index to Overviews ® Overview 4-1 Technical data of SPECORD 200.............. 11 ® Overview 4-2 General technical data of SPECORD ............12 ® SPECORD 200/205/210 User's Manual – Edition 03/2003 Page 45 Analytik Jena AG...

This manual is also suitable for:

Specord 205 pcSpecord 210 pc

Table of Contents