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Related Manuals for Analytik Jena compEAct S
Summary of Contents for Analytik Jena compEAct S
- Page 1 Operating instructions compEAct S / compEAct S Sulfur Analyzer...
- Page 2 Phone + 49 3641 77 7407 + 49 3641 77 7449 Email service@analytik-jena.com http://www.analytik-jena.com General Information compEAct is a trademark of Analytik Jena AG registered in Germany. Copyrights and The identification with ® or TM is omitted in this manual. Trademarks 11-0205-003-23 Documentation number 01.17...
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Page 3: Table Of Contents
Gas supply ......................... 26 4.1.4 Device layout and space requirements ..............26 Supply and control connections ................28 Installing the compEAct S with sample introduction module ........30 4.3.1 Setting up and connecting the compEAct S ............... 30 4.3.2 Connecting the autosampler LS ................31 4.3.3... - Page 4 6.8.2 Checking and replacing the filter ................49 6.8.3 Replacing the pneumatic seal ................... 51 Opening and closing the side panel of the compEAct S ..........52 6.10 Replacing the deuterium lamp (UVFD) ..............53 6.11 Replacing the chemical ozone decomposer (compEAct S only) ......
- Page 5 Solvent and waste containers of the LS ............24 Fig. 14 Electrical connections of the LS ..............24 Fig. 15 Installation diagram for the compEAct S with autosampler LS ....27 Fig. 16 Connections on the rear of the compEAct S ..........28 Fig. 17 USB port and hose bridge in the gas path behind the front door ....
- Page 6 Figures compEAct S...
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Page 7: Basic Information
These operating instructions provide information about the design and operation of the compEAct S and provide operating personnel the necessary know-how for the safe handling of the compEAct S and its components. Furthermore, the operating instructions include information on the maintenance and servicing of the device as well as hints on potential causes of malfunctions and their correction. -
Page 8: Intended Use
PC. The software EAvolution advanced can be accessed remotely and provides the option to control the device remotely. For this purpose, the compEAct S must be connected to a local network or directly to the Internet. -
Page 9: Warranty And Liability
use of the device other than intended improper commissioning, operation and servicing of the device modifications of the equipment without prior consultation with Analytik Jena operation of the device with faulty safety equipment or improperly fitted safety and protection equipment ... -
Page 10: Safety Instructions
References to potential dangers do not replace the work protection regulations which must be observed. Safety markings on the compEAct S Warnings and information symbols have been attached to the compEAct S. These must be observed under all circumstances. Damaged or missing warnings and information symbols can cause incorrect actions... -
Page 11: Requirements For The Operating Personnel
Requirements for the operating personnel The compEAct S may only be operated by qualified specialist personnel instructed in the use of the device. The personal instruction also includes conveying the contents of these operating instructions. -
Page 12: Safety Instructions For Operation
2.5.1 General instructions Each time before starting up the compEAct S, the operator must make sure that the device and its safety equipment is sound condition. This applies in particular after each modification or extension of the device or its repair. -
Page 13: Safety Instructions For Compressed Gas Containers And Systems
S Safety instructions Before opening the compEAct S the device must be switched off using the mains switch and the mains plug must be disconnected from the power outlet! Work on the electronics may only be carried out by the customer service of Analytik Jena and specially authorized technicians. -
Page 14: Safety Instructions - Service And Repair
"Maintenance and care" on page 38. The exterior of the compEAct S may only be cleaned with a piece of cloth wetted with water but not dripping, after the device has been switched off. -
Page 15: Safety Equipment / Behavior During Emergencies
Observe the following notes: In case of hazardous situations or accidents and if there is no immediate risk of injury, switch off the compEAct S and the connected system components immediately using the mains switch (behind the front door) and/or disconnect the mains plugs from the power outlets, if possible! ... -
Page 16: Function And Layout Of The Compeact S
Function and layout of the compEAct S Principle of operation The compEAct S is a compact elemental analyzer for determining sulfur contents in liquid samples. The separately available LPG module 2.0 allows feeding the analyzer with pressurized liquefied gas samples (LPG). The combined GSS/LPG module allows feeding the analyzer with both LPG samples and pressurized gaseous samples. -
Page 17: Layout Of The Compeact S
UV fluorescence detector Sample introduction system All components of the compEAct S to be operated or serviced by the user can be reached via the front door and the opening at the top of the device. Fig. 3... -
Page 18: Fig. 4 Combustion Tube
950 °C and 1100 °C. A combustion tube has been inserted into the combustion furnace of the compEAct S which is used for all standard applications. The combustion tube is made of quartz glass. -
Page 19: Fig. 6 Auto-Protection Assembly
S Function and layout of the compEAct S downstream membrane dryer and the detector against soot particles and solid pyrolysis products in case of incomplete combustion. The filter also retains condensed water and other aerosols; only water vapor passes through. -
Page 20: Fig. 8 Membrane Dryer
Fig. 8 Membrane dryer The compEAct S uses a UV fluorescence detector. The UV radiation of a deuterium Detector lamp stimulates the fluorescence of the analysis gas which contains SO . The intensity of the fluorescence is determined with a photomultiplier (PMT). -
Page 21: Fig. 9 Gas Flow Diagram Of The Compeact S And Compeact Smpo
S Function and layout of the compEAct S Gas flow diagram Fig. 9 Gas flow diagram of the compEAct S and compEAct S... -
Page 22: Type Plate
Function and layout of the compEAct S compEAct S Type plate The rating plate is located on the rear of the compEAct S next to the mains connection and contains the following information: Manufacturer address / logo Trading name ... -
Page 23: Autosamplers Ls 1 And Ls 2
S Function and layout of the compEAct S 3.4.2 Autosamplers LS 1 and LS 2 The autosampler LS is an automatic sampler for liquid samples. It is available in 2 versions. The LS 1 is intended for small series with up to 18 samples. The samples are arranged in a linear sequence on the fixed sample rack. -
Page 24: Fig. 13 Solvent And Waste Containers Of The Ls
The electrical connections and interfaces of the LS are located on the rear panel of the device. The connections for the serial interface and power supply are effected via terminals on the rear panel of the compEAct S. ON/OFF switch... -
Page 25: Installation And Commissioning
Only use the supplied power cord with protective ground conductor to connect the compEAct S to the power supply. The protective effect must not be invalidated by the use of an extension line which does not have a protective conductor. -
Page 26: Gas Supply
The ventilation slits at the bottom and rear side of the device must not be obstructed by any objects. The auto-injector AI or the autosampler LS are mounted to the top of the compEAct S. Therefore, the required height is the sum of the height of the compEAct S and the height of the sample introduction module that is connected. -
Page 27: Fig. 15 Installation Diagram For The Compeact S With Autosampler Ls
S Installation and commissioning Fig. 15 Installation diagram for the compEAct S with autosampler LS... -
Page 28: Supply And Control Connections
The electrical connections and connections for the gas supply are located on the rear panel of the device. Fig. 16 Connections on the rear of the compEAct S Fan for furnace chamber and electronics Mains connection Connection for oxygen (O... -
Page 29: Fig. 18 Location Of The Switch On The Compeact S
Mains switch for emergencies or servicing ON/OFF switch The mains switch is used to disconnect or to connect the compEAct S from the electric Switch functions mains. In normal operation the mains switch remains switched on. It only needs to be switched off for maintenance works or in case of emergencies (→... -
Page 30: Installing The Compeact S With Sample Introduction Module
4.3.1 Setting up and connecting the compEAct S WARNING The compEAct S may only be set up, assembled and installed by the customer service department of Analytik Jena or by specialist personnel authorized and trained by Analytik Jena! Any unauthorized intervention in the compEAct S can endanger the user and the operational safety of the equipment and limits or completely invalidates any warranty claims. -
Page 31: Connecting The Autosampler Ls
S! 1. Put the cover onto the opening above the combustion tube of the compEAct S. 2. Screw on the attachment angles provided with the autosampler LS to the compEAct S. -
Page 32: Connecting The Auto-Injector Ai
1. Remove the cover above the combustion tube of the compEAct S. 2. Place the auto-injector AI onto the opening at the top of the compEAct S. When doing so, move the base plate until the ring-shaped seating fits onto the injection port of the combustion tube. - Page 33 3. Establish the electrical connections between the auto- injector AI and the compEAct S: Power supply (1) Communication interface (2) 4. Plug in the mains cable to the compEAct S (3). The installation of the compEAct S and the auto-injector AI is now complete. ...
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Page 34: Operation
The device system starts up and the EAvolution software is started. The method that was activated before switching the device off is loaded. 1. Switch off the compEAct S using the ON/OFF switch. Alternatively, select the item Switching off using the ▸ P in the EAvolution menu. -
Page 35: Measuring With Auto-Injector Ai
S Operation Measuring with auto-injector AI CAUTION Risk of injury when handling the cannula The cannula of the syringe has a very sharp tip. Do not touch the syringe by the cannula. This could result in injuries or contamination of the cannula. -
Page 36: Measuring With Ls 1 Or Ls 2
Operation compEAct S Measuring with LS 1 or LS 2 CAUTION Risk of injury when handling the cannula! The cannula of the syringe has a very sharp tip. Do not touch the syringe by the cannula. This could result in injuries or contamination of the cannula. - Page 37 S Operation 4. Fill the solvent container (2) with a maximum of 30 ml of solvent. 5. Empty and clean the waste container (1). 6. Assemble the containers and attach them to the bracket of the LS. Attention Proceed with care when inserting the...
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Page 38: Maintenance And Care
Maintenance intervals Analyzer Maintenance task Maintenance interval Check system tightness If the EAvolution software reports any leaks Clean and maintain the compEAct S Weekly Check hose connections for tight fit Weekly Replace membrane dryer In case of soiling or damage... -
Page 39: Cleaning The Compeact S And Its System Components
Smaller leaks can be detected if the control flow in the system drops when applying additional counter pressure. The flow monitoring set which is provided with the compEAct S can be helpful for finding leaks. The set is assembled as follows (→Fig. 19):... -
Page 40: Adjusting The Auto-Injector Ai
Proceed as follows to start the device and the gas supply: 1. Open the gas supply to the compEAct S. 2. Switch on the compEAct S (→ "Switching the compEAct S on and off" p. 34). 3. Make sure that the pneumatic seal on the auto-protection assembly is closed. To do this, move the toggle switch (1) down. -
Page 41: Adjusting The Autosampler Ls
If the depth position of the needle is not yet centered in the combustion tube loosen the LS attachment at the rear of the compEAct S and move the LS to the required depth position. After that, retighten the screw connection (→ "Connecting... -
Page 42: Combustion Furnace Maintenance
1. First switch off the compEAct S from the ON/OFF switch and then, after the system has been shut down completely, from the mains switch (→ "Switching the compEAct S on and off"... - Page 43 S Maintenance and care 3. Open the pneumatic seal on the auto-protection assembly. Move the toggle switch up. This releases the combustion tube and it can now be pulled out of the auto-protection valve assembly. 4. Pull hose 3 (a, blue), and hose 4 (b, gray) out of the FAST connectors.
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Page 44: Replaceing Quartz Wool Plug
Replaceing quartz wool plug ATTENTION Only use the pure quartz wool supplied by Analytik Jena. Contaminated quartz wool may damage the combustion tube and clog the filter. Make sure that the quartz wool plug is correctly positioned. When the plug is not in correct position the sample does not vaporize evenly. -
Page 45: Inserting The Combustion Tube
S Maintenance and care 6.6.3 Inserting the combustion tube WARNING Risk of explosion or carbonization! The gas hoses on the combustion tube must not be mixed up. CAUTION Risk of burns and possible damage of the auto-protection assembly! Only install when the device is cold. -
Page 46: Replacing The Membrane Dryer
13. Assemble the sampler module: Auto-injector AI: Place the auto-injector AI on the combustion tube. Autosampler LS: Place the cover over the opening to the combustion tube. The compEAct S is ready for operation and can be switched on from the mains switch. - Page 47 The connectors are particularly sensitive. Make sure that the connectors are not twisted during installation. 1. First switch off the compEAct S from the ON/OFF switch and then, after the system has been shut down completely, from the mains switch (→ "Switching the compEAct S on and off"...
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Page 48: Servicing The Auto-Protection Assembly
Only remove the auto-protection assembly (APB) when the device is cold or allow the device to cool down sufficiently! 1. First switch off the compEAct S from the ON/OFF switch and then, after the system has been shut down completely, from the mains switch (→ "Switching the compEAct S on and off"... -
Page 49: Checking And Replacing The Filter
S Maintenance and care 5. Remove the heat guard in front of the auto-protection assembly. 6. Unscrew the union nut from the gas connection between the membrane dryer and the auto-protection assembly. Whilst doing so, hold the connections at the membrane dryer from the yellow shrink tubes to prevent it from twisting. - Page 50 Maintenance and care compEAct S 3. Look into the opening of the seal and inspect the filter for carbonization, other contamination or cracks. If the filter is OK, re-install the auto-protection assembly. If the filter needs replacing, follow the remaining instructions.
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Page 51: Replacing The Pneumatic Seal
S Maintenance and care 6.8.3 Replacing the pneumatic seal 1. Remove the combustion tube (→ "Removing and cleaning the combustion tube", p. 42). 2. Remove the auto-protection assembly (→ "Removing and installing the auto- protection assembly", p. 48). 3. Unscrew the 4 screws attaching the pneumatic seal to the auto- protection valve assembly. -
Page 52: Opening And Closing The Side Panel Of The Compeact S
Opening and closing the side panel of the compEAct S WARNING Danger of electric shock! Before opening the side panels, switch off the compEAct S using the mains switch behind the front door and pull the mains plug from the connection on the rear panel of the compEAct S. -
Page 53: Replacing The Deuterium Lamp (Uvfd)
6.10 Replacing the deuterium lamp (UVFD) WARNING Danger of electric shock! Before replacing the deuterium lamp, switch off the compEAct S using the mains switch behind the front door and pull the mains plug from the connection on the rear panel of the compEAct S. - Page 54 1. First switch off the compEAct S from the ON/OFF switch and then, after the system has been shut down completely, from the mains switch (→ "Switching the compEAct S on and off" p. 34). Pull the mains plug at the rear of the device out of the connection.
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Page 55: Replacing The Chemical Ozone Decomposer (Compeact Smpo Only)
Risk of burns on the furnace! Only remove when the device is cold! 6.12.1 Removing the combustion furnace 1. First switch off the compEAct S from the ON/OFF switch and then, after the system has been shut down completely, from the mains switch (→ "Switching the compEAct S on and off"... - Page 56 Open the side panel, pull the functional grounding off the side panel and safely put the side panel aside (→ "Opening and closing the side panel of the compEAct S" p. 52). Unscrew the knurled head screw.
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Page 57: 6.12.2 Installing The Combustion Furnace
The furnace is completely removed. 6.12.2 Installing the combustion furnace 1. Check that the compEAct S is not connected to the mains! 2. Open and unhook the front door. 3. Insert the furnace into the furnace space. 4. Plug the connectors for the furnace heating and thermocoupler (orange cable) into the connections under the furnace at the rear of the furnace space. - Page 58 Open the side panel, pull the functional grounding off the side panel and safely put the side panel aside (→ "Opening and closing the side panel of the compEAct S" p. 52). At the inside wall of the electronics chamber attach the furnace with the knurled head screw.
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Page 59: Troubleshooting
S Troubleshooting Troubleshooting Troubleshooting according to software messages Error message 100002 Communication with companion chip is disturbed. Cause Remedy The communication with the companion chip is Inform the customer service department. disturbed. 101001 Main mfm defective Cause Remedy The flow meter is defective. - Page 60 Troubleshooting compEAct S 101760 Gas flow in Main-O₂ insufficient Cause Remedy The required gas flow could not be achieved with the Check gas supply and connections. Main-O₂ flow controller. Inform the customer service department. 101764 Hardware error in flow sensor Main-O₂...
- Page 61 S Troubleshooting 102210 Sampler error Cause Remedy A general sampler error has occurred (zero). Inform the customer service department. 102211 Error in sampler x-axis Cause Remedy The drive of the sampler on the X axis does not move Inform the customer service department.
- Page 62 The communication with the S-UVFD is disturbed. Inform the customer service department. 105202 Communication with S-UVFD+ is disturbed. Cause Remedy For compEAct S : The communication with the S- Inform the customer service department. UVFD+ is disturbed. 105230 S-UVFD: deuterium lamp defective...
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Page 63: Equipment Faults And Analytical Problems
S Troubleshooting 201200 Service septum in 300 injections Cause Remedy The maintenance interval for the septum is due after Replace the injection port with septum in due course. 300 additional injections. 203001 Automatic backup success Cause Remedy The automatic backup was completed successfully. -
Page 64: Equipment Faults
Troubleshooting compEAct S 7.2.2 Equipment faults Error Possible cause Remedy Furnace does not heat Temperature set incorrectly in the Check temperature configuration in the software method No method loaded Load method Malfunction in power supply Switching the device on ... -
Page 65: Analytical Problems
Excessively high results Incomplete combustion Clean or replace contaminated parts TN interferences Analyze the sample with compEAct S Carryover Insufficient rinsing of the metering Rinse metering syringes adequately prior to syringes in AI or LS... -
Page 66: Transport And Storage
2. Remove the sample rack and the sample containers. 3. Remove the metering syringe from the injector head and pack it separately. 4. Detach the electrical connections on the rear panel of the compEAct S and the autosampler LS. 5. Put the autosampler LS into its original packaging. -
Page 67: Packing The Auto-Injector Ai
13. Pull off the black skirting towards the front of the device. 14. Take the carrying handles from the bracket on the rear panel of the compEAct S and screw them hand-tight into the lateral openings at the base of the device. -
Page 68: Transporting The Compeact S
The device may only be lifted by the carrying handles. 1. Shut down the compEAct S using the ON/OFF switch. Wait 30 min. until the fans no longer rotate and the door LED goes out. Then switch off the mains switch behind the door. -
Page 69: Storage
Transport and storage For installation at the new location observe the notes in section “Installation conditions” p. 25. Fig. 20 compEAct S with screwed-in carrying handles Storage Attention Environmental influences and condensate formation can destroy individual components of the device! The device may only be stored in air-conditioned rooms. -
Page 70: Disposal
S Disposal At the end of its service life the compEAct S and all its electronic components must be disposed of as electronic waste in accordance with the applicable regulations. The chemical ozone decomposer contains metal oxides. Used cartridges must be... -
Page 71: Specification
S Specification Specification 10.1 Technical data 10.1.1 Technical data of the compEAct S General characteristics Designation/type compEAct S / compEAct S Dimensions (width x height x depth) 54 x 51 x 53 cm Mass approx. 30 kg Procedural data... -
Page 72: 10.1.2 Technical Data Of The Auto-Injector Ai
Connection with 24 V 2.0 A 10.2 Guidelines and standards The compEAct S is classified as protection class I. The casing is protection type IP 20. Safety class and safety type The compEAct S complies with the safety standards Device safety ... - Page 73 S Specification The compEAct S is designed and tested in accordance with standards meeting the EU directives requirements of EU directives 2014/35/EU, 2014/30/EU and 2011/65/EU. The device leaves the factory in a sound condition as far as technical safety is concerned.
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