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Summary of Contents for Analytik Jena SPEKOL 2000
- Page 1 ® SPEKOL 2000 UV VIS Spectrophotometer...
- Page 2 Hotline: + 49 (3641) 77-7407 Fax: + 49 (3641) 77-7449 e-mail: service@analytik-jena.de General information about Analytik Jena AG on the internet: http://www.analytik-jena.de Copyrights and Trademarks Microsoft, Windows are registered trademarks of Microsoft Corp. Publication No.: 210:021.23 Edition – January 2008...
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Page 3: Table Of Contents
Contents Contents Introduction ..............3 Intended use of SPEKOL 2000 .............3 SPEKOL 2000 warning labels...............3 Practical notes for working with this Manual .........4 Safety notes ..............5 Technical data ..............7 Connectors and display elements .........9 Installation and start-up..........11 Installation conditions................11 Connecting the SPEKOL 2000............12 Care, maintenance &... - Page 4 Contents ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 5: Introduction
Introduction Intended use of SPEKOL 2000 Introduction Intended use of SPEKOL 2000 ® The SPEKOL 2000 is a compact, computer-controlled two-beam spectral photometer to measure the transmission, extinction, concentration and energy level of liquid samples. It is designed to perform measurement within the spectral range of 190 nm to 1100 nm. Its optical system ensures genuine real-time operation, so even variations in the absorption of a reference sample can be compensated while measurement is going on. -
Page 6: Practical Notes For Working With This Manual
Every illustration has its own caption. • Working steps are numbered. • Cross-references to other sections are marked by an arrow (e.g. → Practical Notes for Working with this Manual p. 4) ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... -
Page 7: Safety Notes
Operation of the device with any other operating voltage than that specified may result in the destruction of the device. Only use fuses of the specified type. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 8 Avoid exposing the sample compartment to strongly corrosive substances! For the analysis of such samples, use vapor-tight stoppered cells. After the measurement, do not leave the samples unnecessarily long in the sample compartment of the device! ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 9: Technical Data
2x T 4 AH Line fuses Temperature range +15°C … +35°C Humidity < 85% Weight 22 kg Dimensions (W x H x D) 410 x 275 x 656 mm Power consumption 200 VA ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 10 Technical data ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 11: Connectors And Display Elements
Lid of sample compartment Lid for extended sample compartment Status indicator LEDs ® Fig. 1 SPEKOL 2000 overall view RS 232 port (PC) ® Fig. 2 SPEKOL 2000 PC terminals on left-hand side panel ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... -
Page 12: Fig. 3 Spekol ® 2000 Rear-Side Terminals
Two windows are provided to protect the photometer space from dust and exposure to reagents. The holder pocket for th e measuring cell (2) is located in front-left position and that for the reference cell in back-right position (1). ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... -
Page 13: Installation And Start-Up
Based on its specified overall dimensions plus an extra 100 mm stripe of clearance on ® all sides, the SPEKOL 2000 requires a minimum footprint area of 610 x 765 mm ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... -
Page 14: Connecting The Spekol 2000
Installation and start-up Connecting the SPEKOL 2000 Connecting the SPEKOL 2000 Observe correct position of device! ® Move the SPECORD only in upright position (observe label on transport case). Do not turn the device upside down. Electric shock Check that the nameplate specification for operating voltage is in agreement with the ®... -
Page 15: Care, Maintenance & Replacement Of Lamps
Danger! Electric shock! ® Use main power switch to turn electric supply to the SPEKOL 2000 off and detach line power cable from power inlet of the SPEKOL 2000 before you replace a fuse. ® Disconnect line power cable from SPEKOL 2000. -
Page 16: Replacement Of Lamps
Screws Lamp cover ® Fig. 6 Lamphouse cover at the bottom of the SPEKOL 2000 Turn out both screws (1) and remove lamphouse cover (2) on the bottom side. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... -
Page 17: Fig. 7 Spekol ® 2000 Lamphouse With Cover Removed
Loosen knurled thumb screws for fixing of halogen lamp feed wires (5 in Fig. 7) and remove cables from their clamping points. Unscrew fixing screw (3 in Fig. 7) of halogen lamp holder, then cautiously retrieve the holder from the inner space. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... -
Page 18: Fig. 8 Holder Base Of Halogen Lamp
Fix connector (4 in Fig. 7). Close lamphouse cover (2 in Fig. 6) and fix cover with both screws (1 in Fig. 6). ® Turn the SPEKOL 2000 cautiously around into working position. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... -
Page 19: Measurement Parameters For Spectrophotometers Of Spekol Series
Measurement / Set Parameters. Fig.7-1 Device driver dialog box The dialog box contains a toolbar with labeled buttons as well as four tabs (Settings, Device, Mode) for the selection of measurement parameters. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 20 WinASPECT manual). Printer Opens the dialog box for selecting printer-specific options. Setup Preview Opens a dialog box with a preview of the printout. Print Starts the printout of measurement parameters. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 21: Spekol: Settings Tab
In the Number textbox, type the number of repeat measurements to be run. In the Interval time textbox, enter the desired time interval between successive measurement starts within a measurement series in seconds. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 22 This registration of reference data is performed using the same measurement parameters as in the following sample measurement. In most cases, distilled water or the solvent of the sample is used as reference. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 23: Spekol: Device Tab
Depending on the selected measurement mode the appearance of the bottom part of the Mode tab changes and shows only those options (textboxes, list boxes and buttons) that are necessary for this mode. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... -
Page 24: Measuring Mode: Scan Mode
Measuring mode: Time Scan In this mode, you may measure a sample repeatedly at a fixed, preselected wavelength. Fig.7-5 Mode tab – Activated Time Scan Parameter Description Wavelength [nm] Wavelength to be used. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... - Page 25 Note When you select the Time Scan mode, a cycle mode (automatic, time controlled) previously selected on the Settings tab will be deactivated. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG...
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Page 26: Measuring Mode: Wavelengths
Note The system accepts wavelengths with one decimal. If you enter wavelengths with more than one decimal, the software will round the wavelength up or down to one decimal. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG... -
Page 27: First Measurement With Spekol
Cycle Mode None Display Absorbance Min. Max. Correction Reference Device tab Lamp change at 325* ® COM Port COM port of your PC to which the SPEKOL been connected. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 28 The sample measurement is immediately being started. The results of the measurement appear in a separate document window. You can learn more about the properties of document windows in Section "Properties and functions of document windows" in ® WinASPECT manual. ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 29: Disposal
Disposal must be as required under valid legislation and local regulations. ® On expiry of its service life, the SPEKOL 2000, including related electronic components, must be disposed as electronic waste under relevant legal provisions. ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG... - Page 30 Disposal ® Issue 01/2008 Manual SPEKOL 2000 Analytik Jena AG...
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Page 31: Table Of Figures
- Device tab..21 Fig.7-4 Mode tab - Activated Scan Mode ............22 Fig.7-5 Mode tab – Activated Time Scan ............22 Fig.7-6 Mode tab – Activated Wavelengths mode ......... 24 ® Manual SPEKOL 2000 Issue 01/2008 Analytik Jena AG...
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